• 제목/요약/키워드: Micro porous structure

검색결과 116건 처리시간 0.023초

마이크로 부동액막을 이용한 착상방지에 관한 실험적 연구 (An Experimental Study on the Frost Prevention using Micro Liquid Film of an Antifreezing Solution)

  • 장영수;윤원남
    • 설비공학논문집
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    • 제17권5호
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    • pp.459-467
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    • 2005
  • The effect of anti freezing solution liquid film on the frost prevention is experimentally investigated. It is desirable that the antifreezing solution spreads widely on the heat exchanger surface forming thin liquid film to prevent frost nucleation and reduce the thermal resistance across the film. A porous layer coating technique is adopted to improve the wettedness of the anti freezing solution on a parallel plate heat exchanger. The antifreezing solution spreads widely on the heat exchanger surface with 100 $\mu$m thickness by the capillary force resulting from the porous structure. It is observed that the antifreezing solution liquid film prevents a parallel plate heat exchanger from frosting. The reductions of heat and mass transfer rate caused by thin liquid film are only $1\~2\%$ compared with those for non-liquid film surface.

팔라듐 합금 수소 분리막의 전처리에 관한 연구 (A Study on the Surface Pre-treatment of Palladium Alloy Hydrogen Membrane)

  • 박동건;김형주;김효진;김동원
    • 한국표면공학회지
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    • 제45권6호
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    • pp.248-256
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    • 2012
  • A Pd-based hydrogen membranes for hydrogen purification and separation need high hydrogen perm-selectivity. The surface roughness of the support is important to coat the pinholes free and thin-film membrane over it. Also, The pinholes drastically decreased the hydrogen perm-selectivity of the Pd-based composite membrane. In order to remove the pinholes, we introduced various surface pre-treatment such as alumina powder packing, nickel electro-plating and micro-polishing pre-treatment. Especially, the micro-polishing pretreatment was very effective in roughness leveling off the surface of the porous nickel support, and it almost completely plugged the pores. Fine Ni particles filled surface pinholes with could form open structure at the interface of Pd alloy coating and Ni support by their diffusion to the membrane and resintering. In this study, a $4{\mu}m$ surface pore-free Pd-Cu-Ni ternary alloy membrane on a porous nickel substrate was successfully prepared by micro-polishing, high temperature sputtering and Cu-reflow process. And $H_2$ permeation and $N_2$ leak tests showed that the Pd-Cu-Ni ternary alloy hydrogen membrane achieved both high permeability of $13.2ml{\cdot}cm^{-2}{\cdot}min^{-1}{\cdot}atm^{-1}$ permation flux and infinite selectivity.

Microsotructure Designed Porous Apatite Ceramics Prepared by Hydrothermal Method

  • Ioku, Koji;Fukuhara, Michiko;Fujimori, Hirotaka;Goto, Seishi
    • The Korean Journal of Ceramics
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    • 제5권2호
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    • pp.162-164
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    • 1999
  • Microsotructure designed porous ceramics of calcium hydroxyapatite $(Ca_{10}(PO_4)_6(OH)_2)$ were prepared by hydrothermal method. The particle size, shape, and the micro-pore size of the porous hydroxyapatite ceramics could becontrolled. The hydroxyapatite was non-stoichiometric apatite with calcium deficient compositions (Ca/P ratio < 1.67). The composition of non-stoichiometric hydroxyapatite ceramics could be controlled from 1.50 to 1.63 in Ca/P ratio. The hydroxyapatite ceramics preparedc at $105^{\circ}C$ under the saturated vapor pressure for 20h were composed of rod-shaped crystals with about 10$\mu\textrm{m}$ in length with the mean aspect ratio of 40. The porous ceramics of calcium deficient hydroxyapatite had about 45% porosity with the inter-connecting pore structure. Porous hydroxyapatite ceramics prepared hydrothermally had the compressive strength of about 10 to 30 MPa. In addition, porous ceramics of $\beta$-tricalcium phosphate ($\beta-Ca_3(PO_4)_2$) were prepared from the calcium deficient hydroxyapatite.

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지구물질의 마이크로미터 단위의 삼차원 공극 구조 규명: 핵자기공명 현미영상 연구 (3-Dimensional ${\mu}m$-Scale Pore Structures of Porous Earth Materials: NMR Micro-imaging Study)

  • 이범한;이성근
    • 한국광물학회지
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    • 제22권4호
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    • pp.313-324
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    • 2009
  • 지표-지각환경을 구성하는 지질매체의 구조와 성질의 정량적-체계적 이해를 위한 예비연구로, 매질을 구성하는 입자의 모양, 크기, 충전 밀도가 공극 구조의 특성과 매질의 성질에 미치는 영향을 알아보기 위해 입자의 모양이 구형인 글래스 비드와 모양이 불규칙한 실리카 젤을 이용하여 입자 크기와 공극률이 서로 다른 다양한 다공성 매질을 준비하였고, 핵자기공명 현미영상을 이용하여 약 $50\;{\mu}m$의 분해능으로 삼차원 영상을 획득하였다. 분석 결과, 지름 약 0.2~1.3 mm 크기의 입자로 구성된 다공성 매질의 비표면적은 2.5부터 $9.6\;mm^2/mm^3$, 공극률은 0.21에서 0.38, 투수율은 11.6에서 892.3 D이며, 이는 일반적인 미고결 샌드가 갖는 값의 범위에 해당된다. 비표면적, 공극률, 투수율의 관계는 Kozeny 식에서 예상된 경향과 비교적 일치하였다. 상자집계 프랙탈 차원은 공극률, 비표면적과의 관련성이 높으며, 공극률이 0.29~0.38일 때 비표면적이 약 2.5부터 $6.0\;mm^2/mm^3$까지 증가할수록 프랙탈 차원이 2.6에서 3.0까지 선형으로 증가하며, 공극률이 0.21~0.28일 때 비표면적이 약 2.5부터 $9.6\;mm^2/mm^3$까지 증가할수록 프랙탈 차원이 2.5에서 3.0까지 선형으로 증가한다. 실제 다공성 사암에 포함된 유체의 삼차원 구조를 핵자기공명 현미영상으로 영상화하였고, 이에 대한 비표면적은 $0.33\;mm^2/mm^3$, 공극률은 0.017, 투수율은 30.9 mD, 상자 집계 프랙탈 차원은 1.59로 계산되었다. 본 연구에서 제시된 것과 같이 핵자기공명 현미영상은 다양한 다공성 매질의 삼차원 공극 구조를 영상화할 수 있고, 삼차원 공극 구조에 대한 상자집계 프랙탈 차원은 본 연구에서와 같이 다양한 공극 구조에 대해 분석이 가능하며, 다공성 매질의 이동 특성을 나타내는 매개 변수들과 지진파 감쇠 등에 대한 조절 인자로 사용될 수 있을 것으로 기대된다.

UV 레이저응용 마이크로 다공성 EPP 기판의 치과용 핸드피스 흡음성능에 관한 기초연구 (Fundamental study on sound absorption of a dental hand piece using micro-porous EPP substrate processed by UV laser)

  • 유동빈;신명호;변효진;최도정;성규원;마용원;신보성
    • 융합정보논문지
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    • 제9권5호
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    • pp.158-164
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    • 2019
  • 최근에는 환자의 귀에 거슬리는 소음을 발생시키는 치과 용 핸드 피스의 소음을 줄이기 위한 많은 연구가 주목 받고 있습니다. 일반적으로 배기 밸브, 기계 또는 자동차의 공기 펌프 내부에 흡음재를 추가하는 방법이 기계적 소음을 줄이는 최적의 방법으로 널리 보고됩니다. 본 논문에서는 EPP 기판의 미세 다공성 구조를 이용한 새로운 UV 레이저 가공 및 흡음 효율 향상을 위한 치과 용 핸드 피스의 제조 방법을 연구 하였다. 슬라이스 된 EPP 기판의 표면에 UV 레이저 가공으로 다수의 미세 크기 기공이 만들어졌다. 본 실험에서 다양한 휴대용 기계에 적용할 수 있는 우수한 잠재력을 가진 마이크로 다공성 EPP 기판은 치과 용 핸드 피스 내부의 마이크로 머플러의 흡음 구조에 적용되었고 핸드피스의 소음을 측정한 결과 적용전의 핸드피스에 비해 약 4dB의 흡음효과를 나타내었다.

마이크로 스파이크로 채취한 조직의 진단을 위한 미세 조직회수도구 (Micro-tissue collecting tool for diagnosis of micro-spike biopsy)

  • 정효영;구교인;이상민;반재원;박호수;방승민;송시영;조동일
    • 센서학회지
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    • 제18권2호
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    • pp.122-127
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    • 2009
  • We have developed and reported several micro-spikes for minimally invasive biopsy. In this paper, a micro-tissue collecting tool for tissue diagnosis extracted by micro-spike is presented. Using proposed polydimethy-siloxane (PDMS) micro-tissue collecting tool, which has a negative micro-spike structure in a porous chamber, the extracted tissue in a micro-spike is effectively detached. The gastro-intestinal tissue of a pig is extracted in an in vivo environment, and then it is detached from a micro-spike using the PDMS micro-tissue collecting tool. A fine clinical picture of the detached tissue is acquired.

개인안전 제품을 위한 3 차원 다공성 폴리머 프린팅의 최적화 공정조건에 대한 연구 (Study of Optimal Process Conditions of 3D Porous Polymer Printing for Personal Safety Products)

  • 유찬주;김혜수;박준한;윤단희;신종국;신보성
    • 한국정밀공학회지
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    • 제33권5호
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    • pp.333-339
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    • 2016
  • In this paper, a fundamental experiment regarding the formation of porous 3D structures for personal safety products using 3D PPP (Porous Polymer Printing) was introduced for the first time. The filament was manufactured by mixing PP (Polypropylene) and CBA (Chemical Blowing Agent) with polymer extruder, and the diameter of the filament was approximately 1.75mm. The proposed 3D PPP method, combined with the conventional FDM (Fused Deposition Modeling) procedure, was influenced by process parameters, such as the nozzle temperature, printing speed and CBA density. In order to verify the best processing conditions, the depositing parameters were experimentally investigated for the porous polymer structure. These results provide parameters under which to form a multiple of 3D porous polymer structures, as well as various other 3D structures, and help to improve the mechanical shock absorption for personal safety products.

규소/질화규소 비가 자전연소합성공정을 이용한 다공질 질화규소 세라믹스의 미세구조와 특성에 미치는 영향 (Effect of Si/$Si_3N_4$ Ration on the Micro structure and Properties of Porous Silicon Nitride Prepared by SHS Method)

  • 김동백;박동수;한병동;정연길
    • 연구논문집
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    • 통권34호
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    • pp.131-138
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    • 2004
  • Porous silicon nitride ceramics were prepared by Self-propagating High Temperature Synthesis from silicon powder, silicon nitride powder and the pore-forming precursor. The microstructure, porosity and the flexural strength of the porous silicon nitride ceramics were varied according to the Si/$Si_3N_4$ ratio, size and amount of the pore-forming precursors. Some samples exhibited as high flexural strength as $162\pm24$ MPa. The high strength is considered to result from the fine pore size and the strong bonding among the silicon nitrid particles.

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Modeling of sulfate ionic diffusion in porous cement based composites: effect of capillary size change

  • Gospodinov, Peter N.
    • Computers and Concrete
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    • 제4권2호
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    • pp.157-166
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    • 2007
  • The paper considers a theoretical model to study sulfate ion diffusion in saturated porous media - cement based mineral composites, accounting for simultaneous effects, such as filling micro-capillaries (pores) with ions and chemical products and liquid push out of them. Pore volume change and its effect on the distribution of ion concentration within the specimen are investigated. Relations for the distribution of the capillary relative radius and volume within the composite under consideration are found. The numerical algorithm used is further completed to consider capillary size change and the effects accompanying sulfate ion diffusion. Ion distribution within the cross section and volume of specimens fabricated from mineral composites is numerically studied, accounting for the change of material capillary size and volume. Characteristic cases of 2D and 3D diffusion are analyzed. The results found can be used to both assess the sulfate corrosion in saturated systems and predict changes occurring in the pore structure of the composite as a result of sulfate ion diffusion.

Low Loss Highly Birefringent Porous Core Fiber for Single Mode Terahertz Wave Guidance

  • Habib, Md. Ahasan;Anower, Md. Shamim
    • Current Optics and Photonics
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    • 제2권3호
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    • pp.215-220
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    • 2018
  • A novel porous-core hexagonal lattice photonic crystal fiber (PCF) is designed and analyzed for efficient terahertz (THz) wave propagation. The finite element method based Comsol v4.2 software is used for numerical analysis of the proposed fiber. A perfectly matched layer boundary condition is used to characterize the guiding properties. Rectangular air-holes are used inside the core to introduce asymmetry for attaining high birefringence. By intentionally rotating the rectangular air holes of porous core structure, an ultrahigh birefringence of 0.045 and low effective material loss of $0.086cm^{-1}$ can be obtained at the operating frequency of 0.85 THz. Moreover, single-mode properties, power fraction in air core and confinement loss of the proposed PCF are also analyzed. This is expected to be useful for wideband imaging and telecom applications.