• 한국레이저가공학회지
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• 제6권3호
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• pp.19-28
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• 2003

The manufacturing process for the microfluidic device can include sequential steps such as master fabrication, electroforming, and injection molding. The laser ablation, using masks, has been applied to the fabrication of channels in microfluidic devices. In this research, an excimer laser was used to engrave microscopic channels on the surface of PET (polyethylene terephthalate), which shows a high absorption ratio for an excimer laser beam with a wavelength of 248 m. When 50-${\mu}{\textrm}{m}$-wide rectangular microscopic channels are ablated with a 500 ${\times}$ 500 ${\mu}{\textrm}{m}$ square mask at a magnification ratio of 1/10, ditch-shaped defects were found in both corners. The measurement of laser beam intensity showed that a coherent image in the PET target caused such defects. Analysis based on the Fourier diffraction theory enabled the prediction of the coherent shape at the image surface as well as the diffraction beam shape between the mask and the image surface. It also showed that the diameter of the aperture had a dominant effect. The application of aperture with a diameter of less than 3 mm helped to eliminate such defects in the ablated rectangular microscopic channels on PET without such ditch-shaped defects.

• 대한토목학회논문집
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• 제41권3호
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• pp.237-246
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• 2021

기후변화로 극한강우에 의해 발생하는 얕은 비탈면 붕괴와 침식으로 토석류 유발이 잦아지고 있다. 앵커나 네일링 공법으로 보강하기 보다는 원지반을 이용하여 식생이 되는 비탈면 보강이 경제적이면서 친환경적인 공법으로 연구되고 있다. 본 연구에서는 충분한 식생이 가능하도록 부엽토와 한약재 찌꺼기를 활용하여 토양개량제를 개발하였다. 그리고 표면침식을 방지하기 위해 첨가제로 마이크로 시멘트와 반수석고 등을 사용하여 전단강도를 증가시켰다. 이러한 주재료와 첨가제 결정은 실내시험을 통하여 강우로 인한 지반 표층의 침식 진행을 확인하여 전단강도의 증가를 확인할 수 있었다. 원지반을 활용하는 토양개량제의 보강은 식생이 가능하고 침식에 대해 저항력이 크게 증가한다. 이러한 보강은 사면 불안정성의 주요 원인인 인장균열 발생을 방지하고 침식에 의한 토석류 유발을 막을 수 있기 때문에 다른 공법들보다 장마철 폭우에 대한 대처방안으로 효율적인 방법이라고 판단된다.

• Restorative Dentistry and Endodontics
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• 제22권1호
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• pp.1-33
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• 1997

The objective of this study was to analyze the in vitro and in vivo corrosion products of low and high copper amalgams. The four different types of amalgam alloy used in this study were Fine cut, Caulk spherical, Dispersalloy, and Tytin. After each amalgam alloy and Hg were triturated according to the directions of the manufacturer by means of the mechanical amalgamator(Amalgam mixer. Shinhung Co. Korea), the triturated mass was inserted into a cylindrical metal mold which was 12mm in diameter and 10mm in height. The mass was condensed by 150Kg/cm compressive force. The specimen was removed from the mold and aged at room temperature for about seven days. The standard surface preparation was routinely carried out by emery paper polishing under running water. In vitro amalgam specimens were potentiostatically polarized ten times in a normal saline solution at $37^{\circ}C$(potentiostat : HA-301. Hukuto Denko Corp. Japan). Each specimen was subjected to anodic polarization scan within the potential range -1700mV to+400mV(SCE). After corrosion tests, anodic polarization curves and corrosion potentials were obtained. The amount of component elements dissolved from amalgams into solution was measured three times by ICP AES(Inductive Coupled Plasma Atomic Emission Spectrometry: Plasma 40. Perkim Elmer Co. U.S.A.). The four different types of amalgam were filled in occlusal and buccal class I cavities of four human 3rd molars. After about five years the restorations were carefully removed after tooth extraction to preserve the structural details including the deteriorated margins. The occlusal surface, amalgam-tooth interface and the fractured surface of in vivo amalgam corrosion products were analyzed. In vivo and in vitro amalgam specimens were examined and analyzed metallographically by SEM(Scanning Electron Microscope: JSM 840. Jeol Co. Japan) and EDAX(Energy Dispersive Micro X-ray Analyser: JSM 840. Jeol Co. Japan). 1. The following results are obtained from in vitro corrosion tests. 1) Corrosion potentials of all amalgams became more noble after ten times passing through the in vitro corrosion test compared to first time. 2) After times through the test, released Cu concentration in saline solution was almost equal but highest in Fine cut. Ag and Hg ion concentration was highest in Caulk spherical and Sn was highest in Dispersalloy. 3) Analyses of surface corrosion products in vitro reveal the following results. a)The corroded surface of Caulk spherical has Na-Sn-Cl containing clusters of $5{\mu}m$ needle-like crystals and oval shapes of Sn-Cl phase, polyhedral Sn oxide phase. b)In Fine cut, there appeared to be a large Sn containing phase, surrounded by many Cu-Sn phases of $1{\mu}m$ granular shapes. c)Dispersalloy was covered by a thick reticular layer which contained Zn-Cl phase. d)In Tytin, a very thin, corroded layer had formed with irregularly growing Sn-Cl phases that looked like a stack of plates. 2. The following results are obtained by an analysis of in vivo amalgam corrosion products. 1) Occlusal surfaces of all amalgams were covered by thick amorphous layers containing Ca-P elements which were abraded by occlusal force. 2) In tooth-amalgam interface, Ca-P containing products were examined in all amalgams but were most clearly seen in low copper amalgams. 3) Sn oxide appeared as a polyhedral shape in internal space in Caulk spherical and Fine cut. 4) Apical pyramidal shaped Sn oxide and curved plate-like Sn-Cl phases resulted in Dispersalloy. 5) In Tytin, Sn oxide and Sn hydroxide were not seen but polyhedral Ag-Hg phase crystal appeared in internal space which assumed a ${\beta}_l$ phase.

• 유변학
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• 제11권1호
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• pp.34-43
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• 1999

수지 이동 성형공정에서 섬유직조가 수지에 의해 함침될 때 발생하는 기공 또는 나쁜 젖음성은 최종 성형품의 물성 저하에 심각한 영향을 미치게 된다. 본 연구에서는 수지이동 성형공정에서의 이러한 문제점을 극복하기 위한 기초 데이터를 제공하기 위하여, 실란 커플링제를 사용한 섬유의 표면 개질이 수지의 유동특성과 수지와 섬유 사이의 젖음성 및 기공함량에 미치는 영향을 조사하였다. 빔 형태의 금형을 대상으로 에폭시 수지와 평직형태의 유리섬유를 사용하여 미시적인 유동가시화 실험 및 경화실험을 수행하였다. 섬유의 표면을 개질함으로써 수지와 섬유 사이의 동적 접촉각이 감소하고 위킹속도는 증가한 것으로 나타났으며, 이러한 결과로부터 본 연구에서 사용한 화학적 표면개질이 섬유직조의 젖음성 및 미시적 흐름 거동을 향상시킬 수 있는 중요한 요인임을 확인할 수 있었다. 또한 수지의 높은 온도와 낮은 침투 속도는 동적 접촉각을 감소시키기 위한 중요한 가공 변수임을 알 수 있었다. 그러나 섬유직조의 투과성은 표면을 개질하였을 경우 오히려 감소하였는데, 이는 젖음성의 향상으로 인하여 수지와 섬유 사이의 접촉시간의 증가에 기인하는 것으로 생각된다. 마지막으로 경화공정을 통해 제조된 시편의 기공 함량을 측정 비교한 결과, 표면개질은 수지이동 성형공정에서의 기공형성에도 중요한 변수로 작용하여, 수지와 섬유 사이의 젖음성을 향상시키고, 최종 성형품의 기공함량을 감소시킴을 확인할 수 있었다.

• 보존과학회지
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• 제29권4호
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• pp.333-343
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• 2013

문화재를 보존, 보관, 전시하는 박물관의 전시실은 실내 공기에 부유하고 있는 먼지와 곰팡이로 인해 생물적 피해를 받는다. 미생물의 발생은 문화재 표면의 착색, 재질 분해, 변질 등의 손상을 야기한다. 본 연구에서는 무위사 성보박물관의 전시실, 전시진열장, 그리고 벽화 표면의 미생물 분포 상태와 온습도 분포 특성을 조사하였다. 전시실과 진열장에서 포집된 미생물을 동정한 결과, Aspergillus sp., Penicillium sp., Cladosporium sp. 등 다양한 미생물이 동정되었다. 특히 1, 3 전시실은 2 전시실에 비해 미생물의 개체 수가 많은 것을 알 수 있었다. 3개 전시실 모두 온 습도 분포도를 살펴본 결과, 대부분이 $28{\pm}4^{\circ}C$의 높은 온도 분포와 70~80% 사이의 고습도 환경에서 높은 분포율을 나타냈다. 각 전시실의 진열장을 비교한 결과, 1 전시실의 진열장이 2, 3 전시실의 진열장에 비해 높은 습도환경 분포율을 보였는데, 이는 미생물 농도 분포와 상관성이 있는 것으로 판단되었다. 이와 같은 무위사 성보박물관 전시실 및 진열장 내부의 고온, 고습 환경의 분포는 근본적으로 전시실의 밀폐도와 환경관리 등에 의해 발생되는 특성임이 확인되었다.

• 한국산학기술학회논문지
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• 제12권11호
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• pp.4924-4931
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• 2011

본 연구는 유산균을 함유한 녹즙제품의 HACCP(Hazard Analysis Critical Control Point)시스템에 의한 제조공정도 작성과 공정별 원료 농산물과 제조 시설에 대한 일반 세균수와 병원성 미생물을 평가하기 위한 목적으로 수행하였다. 공정별 원료농산물의 원재료보관공정 단계의 4가지 시료에서 일반세균이 검출되었으며, 용수(water)는 8.67~14.67 CFU/$m{\ell}$ 검출되었다. 하지만 자외선살균공정 이후, 모든 시료는 법적기준치인 $10^5\;CFU/m{\ell}$이하로 검출되었다. 식중독균인 E. coil, E. coli O157:H7, B. cereus, L. monocytogenes, Salmonella spp, Staph. aureus 실험결과, 보관공정에서 E.coli는 자외선 살균 전단계 공정까지 검출되었으며, B. cereus는 1차세척까지 일부 검출되었다. 모든 세균 및 진균류는 주원료에서 많이 검출되고 있어 주원료의 초기 균수를 최소화하는 선행관리방법을 수립할 필요가 있으며, 세균수와 황색포도상구균 등의 교차 오염방지를 위한 제조설비 등의 효과적인 세척 소독방법을 수립할 필요가 있다고 사료된다. 상기 결과을 바탕으로 유산균을 함유한 녹즙류의 일반세균 및 식중독균을 감소 또는 제거할 수 있는 중요한 공정으로 UV살균공정이 CCP로 관리되어야 한다. 따라서 자외선살균공정의 관리기준 및 이탈시 조치방법, 검증방법, 교육 훈련과 기록관리 등 철저한 HACCP 계획이 필요하다고 사료된다.

• Restorative Dentistry and Endodontics
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• 제22권1호
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• pp.254-266
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• 1997

This study was to know the usefulness of argon laser for composite resin, to prove the polymerized effect of heat treatment of composite resin inlay and to get the curing method for optimal physical properties of composite resin inlay. In this study we used four light curing units and one heat curing unit: Visilux $II^{TM}$, a visible light gun: $SPECTRUM^{TM}$, an argon laser: Unilux AC$^{(R)}$ and Astorn XL$^{(R)}$, visible light curing unit: CRC-$100^{TM}$ for heat treatment. Compared to a control group, we divided the experemental groups into five as follows: Control group: Light curing(Visilux $II^{TM}$) Experimental group 1 : Light curing(Visilux $II^{TM}$) + Light curing(Unilux AC$^{(R)}$) Experimental group 2: Light curing(Visilux $II^{TM}$) + Light curing(Astron XL$^{(R)}$) + Heat treatment(CRC-$100^{TM}$) Experimental group 3 : Laser curing($SPECTRUM^{TM}$) Experimental group 4 : Laser curing($SPECTRUM^{TM}$) + Light curing(Unilux AC$^{(R)}$) Experimental group 5 : Laser curing($SPECTRUM^{TM}$) + Light curing(Astron XL$^{(R)}$) + Heat treatment (CRC-$100^{TM}$) According to the above classification, we made samples through the curing of Clearfil CR Inlay$^{(R)}$, which is a composite resin for inlay, in a separable cylindrical metal mold and polycarbonate plate. And then, we measured and compared the value of compressive strength, diametral tensile strength and the surface micro hardness of each sample. The results were as follows : 1. Among the experimental groups, group 5 showed the highest value of compressive strength, $157.50{\pm}10.24$ kgf and control group showed the lowest value of compressive strength, $103.93{\pm}21.93$ kgf. Control group showed significant difference with the experimental groups(p<0.001). Group 2 which was treated by the heat showed higher compressive strength than that of group 1 which was not, and there was significant difference between group 1 and group 2(p<0.001). Group 5 which was treated by heat showed higher compressive strength than group 4 which was not, and there was significant difference group 4 and group 5(p<0.001). 2. Among the experimental groups, group 5 showed the highest value of diametral tensile strength, $95.84{\pm}1.97$ kgf and control group showed the lowest value of diametral tensile strength, $81.80{\pm}2.17$ kgf. Control group which was cured by visible light showed higher diametral tensile strength than group 3 which was cured Argon Laser. Group 2 which was treated by heat showed higher compressive strength than that of group 1 which was not, and there was significant difference between group 1 and group 2(p<0.001). Group 5 which was treated by heat showed higher compressive strength than group 4 which was not, and there was a significant difference group 4 and group 5(p<0.001). 3. Among the experimental groups, group 5 showed the highest value of microhardness of top surface, $148.42{\pm}9.57$ kgf and control group showed the lowest value of microhardness, $111.43{\pm}7.63$ kgf. In the case of bottom surface, group 5 showed the highest value of $146.19{\pm}7.62$ kgf, and control group showed the lowest, $104.03{\pm}11.05$ kgf. Group 3 which was cured by Argon Laser showed higher diametral tensile strength than control group which was cured only with a visible light gun. Group 2 which was treated by heat showed higher compressive strength than that of group 1 which was not, and there was a significant difference between group 1 and group 2(p<0.001). Group 5 which was treated by heat showed higher compressive strength than group 4 which was not, and there was a significant difference group 4 and group 5(p<0.001). 4. According to the above results, we took a conclusion that argon laser can be used as a useful unit for curing the composite resin and heat treatment can improve the physical properties of the composite resin inlay.

• 대한치과보철학회지
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• 제23권1호
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• pp.39-59
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• 1985

The purpose of this study was to investigate how gap distances of 0.13mm, 0.15mm, 0.20mm, and 0.30mm affects solder joint strength from gold alloys and nickel-chromium base alloys and to examine the composition of solder gold, the solder joint of gold alloys and nickel-chromium base alloys. The tensile test specimens were prepared in the split stainless steel mold with a half dumbbell shape 2.5mm in diameter and l2mm in length. 6 pairs of specimens of each gap distance group of gold alloys and nickel-chromium base alloys were made and 48 pairs of all specimens were soldered with solder gold of 666 fineness. All soldered specimens were machined to a uniform diameter and then a tensile load was applied at a cross-head speed of 0.10mm/min using Instron Universal Testing Machine, Model 1115. The fractured specimens at solder gold of solder joint fracture with each gap distance of 0.13mm, 0.15mm, 0.20mm, and 0.30mm were examined under the Scanning Electron Microscope, JSM-35c and the composition of solder gold, the solder joint of gold alloys and nickel-chromium base alloys was analyzed by Electron Probe Micro Analyzer. The results of this study were obtained as follows: 1. In case of soldering of gold alloys, the tensile strength between gold alloys showed $37.33{\pm}2.52kg/mm^2$ at 0.13, $39.14{\pm}3.35kg/mm^2$ at 0.15mm, $43.76{\pm}2.97kg/mm^2$ at 0.20mm, and $49.18{\pm}4.60kg/mm^2$ at 0.30mm. There was statistically significant difference at each gap distance, and so the greater increase of gap distance showed the greater tensile strength. 2. In case of soldering of nickel-chromium base alloys, the tensile strength between nickel-chromium base alloys showed $34.84{\pm}4.26kg/mm^2$ at 0.13mm, $37.25{\pm}2.49kg/mm^2$ at 0.15mm, $42.91{\pm}4.32kg/mm^2$ at 0.20mm, and $46.93{\pm}4.21kg/mm^2$ at 0.30mm. There was not statistically significant difference only between 0.13mm and 0.15mm and bet ween 0.20 mm and 0.30mm, but generally the greater increase of gap distance showed the greater tensile strength. 3. The greater increase of gap distance shoed less porosities in solder gold at solder joint fracture. 4. In solder gold Au, Cu, Ag, Zn, and Sn were composed and Au and Cu were mostly distributed uniformly. 5. In solder joints of solder gold and gold alloys Au, Cu, Ag, Zn, and Sn were composed in solder gold and Au, Cu, Ag, Pt, and Pd were composed in gold alloys. Au and Cu of solder gold and gold alloys were mostly distributed uniformly and the diffusion of other elements except Pt and Pd around the solder joint was not almost found. In solder joints of solder gold and nickel-chromium base alloys Au, Cu, Ag, Zn, and Sn were composed in solder gold and Ni, Cr, and Al were composed in nickel-chromium base alloys. Au and Cu of solder gold and Ni and Cr of nickel-chromium base alloys were mostly distributed uniformly and the diffusion of other elements except Cr around the solder joint was not almost found.