• Title/Summary/Keyword: Micro hardness profile

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A Study on the Surface Characteristics n the Alumina Grinding (알루미나 연삭표면 특성에 관한 연구)

  • 하상백
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 1999.10a
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    • pp.519-524
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    • 1999
  • To manufacture alumina products, sintering and grinding process are needed. In Al2O3 grinding, macro/micro surface fracture and cracks are easily occurred on the ground surface because of its high brittleness. In view point of fatigue fracture, surface profile produced by grinding is considered as notches. Therefore, it was reasonable that magnitudes and shapes of surface profiles effects on fatigue strength and life. Particularly, surface finish of Al2O3 which have high hardness and brittleness have an effect on fatigue strength. In this paper, some experiments are carried out to examine influence of grinding conditions to magnitude and shape of surface profile as well as the relationships of Ra, Rmax, Rmax/Ra, and Ku. Through the experimental results, It is found that Ra and Rmax was affected by grinding conditions, but Rmax/Ra and Ku was not. There are linear relations between Ra and Rmax, and between Rmax/Ra and Ku.

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Analysis of the Change in Microstructures of Nano Copper Powders During the Hydrogen Reduction using X-ray Diffraction Patterns and Transmission Electron Microscope, and the Mechanical Property of Compacted Powders (X-선 회절 패턴 측정과 투과 전자 현미경을 이용한 구리 나노분말의 수소 환원 처리 시 발생하는 미세조직 변화 및 치밀화 시편의 물성 분석)

  • Ahn, Dong-Hyun;Lee, Dong Jun;Kim, Wooyeol;Park, Lee Ju;Kim, Hyoung Seop
    • Journal of Powder Materials
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    • v.21 no.3
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    • pp.207-214
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    • 2014
  • In this study, nano-scale copper powders were reduction treated in a hydrogen atmosphere at the relatively high temperature of $350^{\circ}C$ in order to eliminate surface oxide layers, which are the main obstacles for fabricating a nano/ultrafine grained bulk parts from the nano-scale powders. The changes in composition and microstructure before and after the hydrogen reduction treatment were evaluated by analyzing X-ray diffraction (XRD) line profile patterns using the convolutional multiple whole profile (CMWP) procedure. In order to confirm the result from the XRD line profile analysis, transmitted electron microscope observations were performed on the specimen of the hydrogen reduction treated powders fabricated using a focused ion beam process. A quasi-statically compacted specimen from the nano-scale powders was produced and Vickers micro-hardness was measured to verify the potential of the powders as the basis for a bulk nano/ultrafine grained material. Although the bonding between particles and the growth in size of the particles occurred, crystallites retained their nano-scale size evaluated using the XRD results. The hardness results demonstrate the usefulness of the powders for a nano/ultrafine grained material, once a good consolidation of powders is achieved.

Heat treatment characteristics of medium carbon steel by CW Nd:YAG Laser (CW Nd:YAG 레이저를 이용한 중탄소강의 열처리특성)

  • Shin H.J.;Yoo Y.T.;Ahn D.G.;Im K.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2005.06a
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    • pp.438-443
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    • 2005
  • Laser surface hardening is an effective technique used to improve the tribological properties and also to increase the service life of automobile components such as camshafts, crankshatfs, lorry brake drums and gears. High power CO2 lasers and Nd:YAG lasers are employed for localized hardening of materials and hence are of potential application in the automobile industries. The heat is conducted rapidly into the bulk of the specimen causing self-quenching to occur and the formation of martensitic structure. In this investigation, the microstructure features occurring in Nd:YAG laser hardening SM45C steel are discussed with the use of optical microscopic and scanning electron microscopic analysis. Moreover, This paper describes the optimism of the processing parameters for maximum hardened depth of SM45C steel specimens of 3mm thickness by using CW Nd:YAG laser. Travel speed was varied from 0.6m/min to 1.0m/min. The maximum hardness and case depth fo SM45C steel are 780Hv and 0.4mm by laser hardening.

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Surface Quality and Corrosion of Additively Manufactured STS316L Treated by Ultrasonic Nanocrystal Surface Modification (적층제조된 스테인레스 316L에 대한 초음파나노표면개질에 따른 표면특성 및 부식성에 관한 연구)

  • Kim, Jun-Ho;Oh, Yeong-Taek;Park, Han-Byeol;Lee, Dong-Ho;Kim, Hwa-Jeong;Kim, Ui-Jun;Shim, Do-Sik
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.19 no.8
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    • pp.94-103
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    • 2020
  • This study investigated the effects of ultrasonic nanocrystal surface modification (UNSM) on the deteriorated surface of AISI SUS316L additively manufactured (AM) using the powder bed fusion (PBF) technique. Specifically, the effects of UNSM conditions on surface topology, hardness, and anti-corrosion were examined. Before UNSM treatment, the stainless steel 316L powder was processed via the PBF machine to prepare a substrate. We observed surface changes due to UNSM treatments in PBF SUS316L substrates and examined the correlation between topology changes, roughness, hardness, and anti-corrosion. After UNSM treatment, the coarse as-built surface was refined, and a regular micro-profile was implemented. Compared to the non-treated PBF sample, the waviness and roughness of the surfaces after UNSM treatment decreased by up to 56.0% and 94.5%, respectively, and decreased further as the interval decreased. The hardness improved by up to 63.0% at a maximum depth of 500 ㎛ from top surface by the UNSM treatment. The results of the corrosion test showed that the corrosion resistance of the UNSM specimens was moderately improved compared to that of the untreated surface. This study confirmed that UNSM is an effective post-processing technique for additively manufactured parts.

Characterization of DLC Coated Surface of Fe-3.0%Ni-0.7%Cr-1.4%Mn-X Steel (DLC 코팅한 Fe-3.0%Ni-0.7%Cr-1.4%Mn-X강의 표면특성평가)

  • Jang, Jaecheol;Kim, Song-Hee
    • Journal of the Korean institute of surface engineering
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    • v.47 no.1
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    • pp.13-19
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    • 2014
  • The various surface treated conditions of Fe-3.0%Ni-0.7%Cr-1.4%Mn-X steel such as as-received, ion nitriding, DLC coated, DLC coated after nitriding for 3 hrs and 6 hrs were investigated to evaluate the beneficial effect for plastic mold steel. Micro Vickers hardness tester was used to estimate nitriding depth from the hardness profile and to measure hardness on the surface. Elastic modulus and residual stress were measured by a nanoindentator. Scratch test and SP (small ball punch test) were utilized to assess the adhesive strength of DLC coating. The depth of nitriding layer was measured as $50{\mu}m$ for the condition of 3 hrs nitriding and $90{\mu}m$ for that of 6 hrs nitriding. Hardness, elastic modulus, residual stress of DLC coating were 20.37 GPa, 162.78 GPa and -1456 MPa respectively. Residual stress on the surface of DLC coating after nitriding could increase to -3914 MPa by introducing nitriding before DLC coating. During the 'Ball-On-Disc' test ${\gamma}^{\prime}$ particles pulled out from the surface of nitrized layer tend to enhance abrasive wear mode since the fraction of ${\gamma}^{\prime}$ (Fe4N) in ion-nitrized layer is known to increases with nitriding time. Thus the specific wear rate of the nitriding layer increased. Comparing with nitriding the specific wear rate in work piece disc as well as ball decreased prominently in DLC coating due to the remarkable reduction in friction coefficient.

Fabrication of High Strength Transparent Bulletproof Materials by Ion Exchanged Borosilicate Glass (보로실리케이트 유리의 이온교환에 의한 고강도 투명방탄소재의 제조)

  • Kim, Young-Hwan;Shim, Gyu-In;Lim, Jae-Min;Choi, Se-Young
    • Journal of the Korea Institute of Military Science and Technology
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    • v.13 no.6
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    • pp.1121-1126
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    • 2010
  • Borosilicate glass (81% $SiO_2$-2% $Al_2O_3$-13% $B_2O_3$-4% $Na_2O_3$) was prepared, and the glass was ion exchanged in $KNO_3$ powder containing different temperature and time. The $K^+-Na^+$ ion exchange takes place at the glass surface and creates compressed stress, which raise the mechanical strength of the glass. The depth profile of $Na^+$ and $K^+$ was observed by electron probe micro analyzer. With the increasing heat-treatment time from 0min to 20min, the depth profile was increased from 17.1um to 29.4um, but mechanical properties were decreased. It was also found out that excessive heat treatment brings stress relaxation. The Vickers hardness, Fracture Toughness and bending strength of ion exchanged samples at $570^{\circ}C$ for 10min were $821.8H_v$, $1.3404MPa{\cdot}m^{1/2}$, and 953MPa, which is about 120%, 180%, and 450% higher than parent borosilicate glass, respectively. Transmittance was analyzed by UV-VIS-NIR spectrophotometer. Transmittance of ion exchanged borosilicate glass was decreased slightly at visible-range. It can be expected that transparent bulletproof materials in more light-weight and thinner by ion exchanged borosilicate glass.

Mechanical Characteristics and Microstructure on Friction Stir Welded Joints with 6061-T6 Aluminium Alloy (알루미늄합금 6061-T6의 마찰교반용접 조건에 따른 기계적특성 및 용접부 조직평가)

  • Jang, Seok-Ki;Park, Jong-Seek
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.33 no.7
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    • pp.693-699
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    • 2009
  • This paper shows mechanical properties and behaviors of macro- and micro-structures on friction stir welded specimen with 6061-T6 aluminum alloy plate. It apparently results in defect-free weld zone jointed at welding conditions like the traverse speed of 267mm/min, tool rotation speed of 2500rpm, pin inserted depth of 4.5mm and tilting angle of $2^{\circ}$ with tool dimensions such as tool pin diameter of 5mm, shoulder diameter of 15mm and pin length of 4.5mm. The tensile stress ${\sigma}_T=228MPa$ and the yield point ${\sigma}Y=141MPa$ are obtained at the condition of traverse speed of 267mm/min and tool rotation speed of 2500rpm. With the constant rotation speed, the higher traverse speed become, the higher tensile stress and yielding point become. Vickers hardness for welding zone profile were also presented.