• 한국분말재료학회지
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• 제31권1호
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• pp.8-15
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• 2024

The emergence of ferrous-medium entropy alloys (FeMEAs) with excellent tensile properties represents a potential direction for designing alloys based on metastable engineering. In this study, an FeMEA is successfully fabricated using laser powder bed fusion (LPBF), a metal additive manufacturing technology. Tensile tests are conducted on the LPBF-processed FeMEA at room temperature and cryogenic temperatures (77 K). At 77 K, the LPBF-processed FeMEA exhibits high yield strength and excellent ultimate tensile strength through active deformation-induced martensitic transformation. Furthermore, due to the low stability of the face-centered cubic (FCC) phase of the LPBF-processed FeMEA based on nano-scale solute heterogeneity, stress-induced martensitic transformation occurs, accompanied by the appearance of a yield point phenomenon during cryogenic tensile deformation. This study elucidates the origin of the yield point phenomenon and deformation behavior of the FeMEA at 77 K.

• 열처리공학회지
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• 제37권5호
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• pp.237-246
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• 2024

In this study, hydrogen embrittlement was investigated for 316L stainless steel (SS316L) and CoCrFeNi medium-entropy alloy (MEA) fabricated by laser-powder bed fusion. The in-situ hydrogen charging tensile tests revealed that the reduction in ductility due to hydrogen was more significant in the CoCrFeNi MEA, compared to the SS316L. In the case of SS316L, hydrogen-assisted cracks (HACs) were observed mainly on the surface, whereas in CoCrFeNi, cracks were found not only at the edges but also in the central region. HACs analysis confirmed that transgranular (TG) cracks were predominant in SS316L, whereas only intergranular cracks were formed in the CoCrFeNi MEA. The difference in hydrogen embrittlement resistance between SS316L and CoCrFeNi was discussed in terms of the differences in deformation microstructure and hydrogen diffusivity, as investigated through electron channeling contrast imaging and nanoindentation.

• 한국분말재료학회지
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• 제27권1호
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• pp.1-7
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• 2020

In this research, a new medium-entropy alloy with an equiatomic composition of FeCuNi was designed using a phase diagram (CALPHAD) technique. The FeCuNi MEA was produced from pure iron, copper, and nickel powders through mechanical alloying. The alloy powders were consolidated via a high-pressure torsion process to obtain a rigid bulk specimen. Subsequently, annealing treatment at different conditions was conducted on the four turn HPT-processed specimen. The microstructural analysis indicates that an ultrafine-grained microstructure is achieved after post-HPT annealing, and microstructural evolutions at various stages of processing were consistent with the thermodynamic calculations. The results indicate that the post-HPT-annealed microstructure consists of a dual-phase structure with two FCC phases: one rich in Cu and the other rich in Fe and Ni. The kernel average misorientation value decreases with the increase in the annealing time and temperature, indicating the recovery of HPT-induced dislocations.