• Title/Summary/Keyword: Materials testing

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Effect of Al Alloy Composition on Physical and Crystallographical Properties of Plasma Electrolytic Oxidized Coatings I. Physical Properties of PEO Layer (플라즈마 전해 산화 코팅에 있어서 알루미늄 합금 모재 성분의 물리적, 결정학적 영향 I. PEO 층의 물성)

  • Kim, Bae-Yeon;Lee, Deuk-Yong;Kim, Yong-Nam;Jeon, Min-Seok;Song, Jun-Kwang;Kim, Sung-Youp;Kim, Kwang-Youp
    • Journal of the Korean Ceramic Society
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    • v.47 no.3
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    • pp.256-261
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    • 2010
  • Physical properties of Plasma electrolytic oxidized 8 different types of Al alloys, A-1100, A-2024, A-5052, A-6061, A-6063, A-7075, ACD-7B and ACD-12 were investigated. The electrolyte for PEO was $Na_2SiO_3$ solutions with NaOH and some alkali earthen metal salts. Porous layer near the surface of PEO coating was not found, and surface roughness Ra50 was below 2.5 ${\mu}m$. Surface roughness was affected by growth rate of plasma electrolytic oxidized layer, not by Si content in Al alloy.

Validation of Suitability on Proficiency Testing Samples for Acute Toxicity Test with Daphnia magna (생태독성 숙련도 시료의 적절성 평가)

  • Shin, Kisik;Park, Woosang;Lee, Jungseo;Yu, Soonju;Park, Taejin;Kim, Jongmin
    • Journal of Korean Society on Water Environment
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    • v.31 no.1
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    • pp.49-54
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    • 2015
  • Acute toxicity test with Daphnia magna has a variety of factors such as incubation condition of test species, food quality and proficiency of laboratory workers. Therefore, proper proficiency testing samples were required for evaluating the competence of laboratory workers. This study aims to propose some appropriate proficiency testing samples for laboratory workers of acute toxicity test with Daphnia magna. Proposed four kinds of standard samples (Sample A, B, C, and D) for proficiency testing were selected from reference materials which were recommended from Canada and USA WET(Whole Effluent Toxicity) authorities. Proposed standard samples were tested by trial application of proficiency testing, homogeneity and stability checks using repeatability test. Sample A, C and D were estimated ad the suitable candidates for proficiency test standard samples except for Sample B. In addition, Sample A was proved to be the most suitable sample.

Effect of Al Alloy Composition on Physical and Crystallographical Properties of Plasma Electrolytic Oxidized Coatings II. Crystallographic Analysis of PEO Layer (플라즈마 전해 산화 코팅에 있어서 알루미늄 합금 모재 성분의 물리적, 결정학적 영향 II. PEO 층의 결정상 분석)

  • Kim, Bae-Yeon;Lee, Deuk-Yong;Shin, Min-Chul;Shin, Hyun-Gyoo;Kim, Byeong-Kon;Kim, Sung-Youp;Kim, Kwang-Youp
    • Journal of the Korean Ceramic Society
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    • v.47 no.4
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    • pp.283-289
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    • 2010
  • Physical properties of Plasma electrolytic oxidized 8 different kinds of Al alloys, A-1100, A-2024, A-5052, A-6061, A-6063, A-7075, ACD-7B and ACD-12 were investigated. The electrolyte for PEO was $Na_2SiO_3$ and NaOH and some alkali earthen metal salts system solution. $\eta$-alumina, as well as $\gamma$-alumina, was main crystal phase, which were ever reported. Also, $Al_{4.95}Si_{1.05}O_{9.52}$ was found only in this research. So we can conclude that the process conditions of PEO apparatus and composition and concentration of its electrolyte affects crystal structure and physical properties of PEO layers much more than the compositions of Al alloy.

Analysis of the influence of panel characteristics on odor measurement based on the air dilution olfactory method in Korea

  • Kim, Sun-Tae;Lee, Seokjun;Yim, Bongbeen
    • Environmental Engineering Research
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    • v.24 no.1
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    • pp.91-98
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    • 2019
  • This study was to objectify differences in the results of odor testing according to the characteristics of panel members that participate in air dilution olfactory method (ADOM) testing. When differences in the results of olfactory testing were reviewed in relation to characteristics of the panelists, the result of entire panels for the site boundary Proficiency Testing Materials (PTMs) showed no difference according to panelist sex, age, smoking status, and past participation in ADOM tests. As for the outlet PTMs, distinct differences appeared in relation to the smoking status and age of panelists. The frequency distribution for all the panelists (Dev($D/T_{total}$)) showed a form similar to a normal distribution, so it is thought to be more appropriate for the review of effect of panelist characteristics on the result of air dilution olfactory tests. In addition, the ADOM testing method implemented as the standard method for odor compounds in Korea (Dev($D/T_3$)) will have to be implemented along with a concurrent assessment, for the purpose of identifying the effect of panelist characteristics on administrative dispositions against malodors.

Ultrasonic Nondestructive Evaluation(NDE) of Cornposite Materials - A Review -

  • Lee, Ouk-Sub
    • Journal of the Korean Society for Nondestructive Testing
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    • v.9 no.2
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    • pp.25-36
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    • 1989
  • This essay is a general review of the application of ultrasonic NDE techniques to the performance assessment and characterization of composite materials. A brief review of ultrasonic input-output characterization of a composite plate by shear waves is presented. A theoretical development of ultrasonic wave propagation in isotropic and anisotropic media excited, respectively, by a circular transducer and an oscillatory point source is summarized. Some experimental results are described in which ultrasonic velocity and attenuation measurements give insight into material degradation of fatigued composite laminates. Ultrasonic determination of the elastic constants of a composite plate and an experimental attempt at ultrasonic testing of an isotropic plate containing a crack are also included. A recent effort for the characterization of viscoelastic materials using the ultrasonic NDE technique is outlined. Finally, the reliability of ultrasonic NDE is briefly touched upon.

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Model and Field Testing of a Heavy-Duty Gas Turbine Combustor

  • Ahn, Kook-Young;Kim, Han-Seok;Antonovsky, Vjacheslav-Ivanovich
    • Journal of Mechanical Science and Technology
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    • v.15 no.9
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    • pp.1319-1327
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    • 2001
  • The results of stand and field testing of a combustion chamber for a heavy-duty 150 MW gas turbine are discussed. The model represented one of 14 identical segments of a tubular multican combustor constructed 1:1 scale. The model experiments were executed at a lower pressure than that in a real gas turbine. Combustion efficiency, pressure loss factor, pattern factor, liner wall temperature, flame radiation, fluctuating pressure and NOx emission were measured at partial and full loads for both model and on-site testing. The comparison of these items in the stand and field test results led to has the development of a method of calculation and the improvement of gas turbine combustors.

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Pre-service Acoustic Emission Testing for Metal Pressure Vessel (금속압력용기의 사용 전 음향방출시험)

  • Lee, Jong-O;Yoon, Woon-Ha;Lee, Tae-Hee;Lee, Jong-Kyu
    • Journal of the Korean Society for Nondestructive Testing
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    • v.23 no.3
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    • pp.280-284
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    • 2003
  • The field application of acoustic emission(AE) testing for brand-new metal pressure vessel were performed. We will introduce the test procedure for acoustic emission test such as instrument check distance between sensors, sensor location, whole system calibration, pressurization sequence, noise reduction and evaluation. The data of acoustic emission test contain many noise signal, these noise can be reduced by time filtering which based on the description of observation during AE test.

Analysis and Simulation of Ultrasonic Wave Propagation and Scattering in Unidirectional Fiber Composites (단일방향 섬유 복합재료 내의 초음파 전파 및 산란 현상의 해석과 시뮬레이션)

  • Lee, Choon-Jae;Yim, Hyun-June
    • Journal of the Korean Society for Nondestructive Testing
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    • v.21 no.3
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    • pp.269-276
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    • 2001
  • Ultrasonic testing of composite materials is much more difficult than that of isotropic materials, because of the beam skew phenomenon caused by their elastic anisotropy. An established analytical method exists for elastic wave propagation in anisotropic media as a result of previous research efforts. Yet, due to the complexity of the analytical method, solution of real problems must resort to the numerical method. In this work, analytical solutions have first been obtained for the wavefield due to a point source in a unidirectional fiber-reinforced composite, which may be modeled as transversely isotropic. Then, the corresponding numerical solutions have been obtained using the mass-spring lattice model(MSLM). The two solutions have agreed well with each other. Other problems such as reflection from free boundaries and scattering from cracks have also been solved numerically, and the results have been investigated from the viewpoint of wave mechanics. The numerical model whose validity has been confirmed by this work will be of great use in simulating ultrasonic testing of composite materials.

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Measurement of Cortisol in Human Serum by Isotope Dilution Liquid Chromatography/Mass Spectrometry and a Comparison through a Proficiency Testing

  • Lee, Hwa-Shim;Shin, Hye-Sun;Park, Sang-Ryoul;Park, Chang-Joon
    • Bulletin of the Korean Chemical Society
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    • v.31 no.5
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    • pp.1149-1154
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    • 2010
  • Liquid chromatography/mass spectrometry using isotope dilution method has been established as a primary method for the measurement of cortisol in human serum. Verification of this method was accomplished by the participation in Consultative Committee for Amount of Substance-Metrology in Chemistry (CCQM) pilot study. Two levels of cortisol certified reference materials were prepared and certified by the established method. They were used as sample materials for the proficiency testing. The expanded uncertainty in the measurement of cortisol in human serum was approximately 1.2% at 95% confidence level. The results of the proficiency testing showed a good precision among the participants, but some bias to the certified values. This means that commercial field laboratories should keep traceability chain to SI unit through available reference measurement procedures and/or available reference materials.