• 제목/요약/키워드: Materials Testing

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플라즈마 전해 산화 코팅에 있어서 알루미늄 합금 모재 성분의 물리적, 결정학적 영향 I. PEO 층의 물성 (Effect of Al Alloy Composition on Physical and Crystallographical Properties of Plasma Electrolytic Oxidized Coatings I. Physical Properties of PEO Layer)

  • 김배연;이득용;김용남;전민석;송준광;김성엽;김광엽
    • 한국세라믹학회지
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    • 제47권3호
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    • pp.256-261
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    • 2010
  • Physical properties of Plasma electrolytic oxidized 8 different types of Al alloys, A-1100, A-2024, A-5052, A-6061, A-6063, A-7075, ACD-7B and ACD-12 were investigated. The electrolyte for PEO was $Na_2SiO_3$ solutions with NaOH and some alkali earthen metal salts. Porous layer near the surface of PEO coating was not found, and surface roughness Ra50 was below 2.5 ${\mu}m$. Surface roughness was affected by growth rate of plasma electrolytic oxidized layer, not by Si content in Al alloy.

생태독성 숙련도 시료의 적절성 평가 (Validation of Suitability on Proficiency Testing Samples for Acute Toxicity Test with Daphnia magna)

  • 신기식;박우상;이정서;유순주;박태진;김종민
    • 한국물환경학회지
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    • 제31권1호
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    • pp.49-54
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    • 2015
  • Acute toxicity test with Daphnia magna has a variety of factors such as incubation condition of test species, food quality and proficiency of laboratory workers. Therefore, proper proficiency testing samples were required for evaluating the competence of laboratory workers. This study aims to propose some appropriate proficiency testing samples for laboratory workers of acute toxicity test with Daphnia magna. Proposed four kinds of standard samples (Sample A, B, C, and D) for proficiency testing were selected from reference materials which were recommended from Canada and USA WET(Whole Effluent Toxicity) authorities. Proposed standard samples were tested by trial application of proficiency testing, homogeneity and stability checks using repeatability test. Sample A, C and D were estimated ad the suitable candidates for proficiency test standard samples except for Sample B. In addition, Sample A was proved to be the most suitable sample.

플라즈마 전해 산화 코팅에 있어서 알루미늄 합금 모재 성분의 물리적, 결정학적 영향 II. PEO 층의 결정상 분석 (Effect of Al Alloy Composition on Physical and Crystallographical Properties of Plasma Electrolytic Oxidized Coatings II. Crystallographic Analysis of PEO Layer)

  • 김배연;이득용;신민철;신현규;김병곤;김성엽;김광엽
    • 한국세라믹학회지
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    • 제47권4호
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    • pp.283-289
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    • 2010
  • Physical properties of Plasma electrolytic oxidized 8 different kinds of Al alloys, A-1100, A-2024, A-5052, A-6061, A-6063, A-7075, ACD-7B and ACD-12 were investigated. The electrolyte for PEO was $Na_2SiO_3$ and NaOH and some alkali earthen metal salts system solution. $\eta$-alumina, as well as $\gamma$-alumina, was main crystal phase, which were ever reported. Also, $Al_{4.95}Si_{1.05}O_{9.52}$ was found only in this research. So we can conclude that the process conditions of PEO apparatus and composition and concentration of its electrolyte affects crystal structure and physical properties of PEO layers much more than the compositions of Al alloy.

Analysis of the influence of panel characteristics on odor measurement based on the air dilution olfactory method in Korea

  • Kim, Sun-Tae;Lee, Seokjun;Yim, Bongbeen
    • Environmental Engineering Research
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    • 제24권1호
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    • pp.91-98
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    • 2019
  • This study was to objectify differences in the results of odor testing according to the characteristics of panel members that participate in air dilution olfactory method (ADOM) testing. When differences in the results of olfactory testing were reviewed in relation to characteristics of the panelists, the result of entire panels for the site boundary Proficiency Testing Materials (PTMs) showed no difference according to panelist sex, age, smoking status, and past participation in ADOM tests. As for the outlet PTMs, distinct differences appeared in relation to the smoking status and age of panelists. The frequency distribution for all the panelists (Dev($D/T_{total}$)) showed a form similar to a normal distribution, so it is thought to be more appropriate for the review of effect of panelist characteristics on the result of air dilution olfactory tests. In addition, the ADOM testing method implemented as the standard method for odor compounds in Korea (Dev($D/T_3$)) will have to be implemented along with a concurrent assessment, for the purpose of identifying the effect of panelist characteristics on administrative dispositions against malodors.

Ultrasonic Nondestructive Evaluation(NDE) of Cornposite Materials - A Review -

  • 이억섭
    • 비파괴검사학회지
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    • 제9권2호
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    • pp.25-36
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    • 1989
  • This essay is a general review of the application of ultrasonic NDE techniques to the performance assessment and characterization of composite materials. A brief review of ultrasonic input-output characterization of a composite plate by shear waves is presented. A theoretical development of ultrasonic wave propagation in isotropic and anisotropic media excited, respectively, by a circular transducer and an oscillatory point source is summarized. Some experimental results are described in which ultrasonic velocity and attenuation measurements give insight into material degradation of fatigued composite laminates. Ultrasonic determination of the elastic constants of a composite plate and an experimental attempt at ultrasonic testing of an isotropic plate containing a crack are also included. A recent effort for the characterization of viscoelastic materials using the ultrasonic NDE technique is outlined. Finally, the reliability of ultrasonic NDE is briefly touched upon.

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Model and Field Testing of a Heavy-Duty Gas Turbine Combustor

  • Ahn, Kook-Young;Kim, Han-Seok;Antonovsky, Vjacheslav-Ivanovich
    • Journal of Mechanical Science and Technology
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    • 제15권9호
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    • pp.1319-1327
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    • 2001
  • The results of stand and field testing of a combustion chamber for a heavy-duty 150 MW gas turbine are discussed. The model represented one of 14 identical segments of a tubular multican combustor constructed 1:1 scale. The model experiments were executed at a lower pressure than that in a real gas turbine. Combustion efficiency, pressure loss factor, pattern factor, liner wall temperature, flame radiation, fluctuating pressure and NOx emission were measured at partial and full loads for both model and on-site testing. The comparison of these items in the stand and field test results led to has the development of a method of calculation and the improvement of gas turbine combustors.

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금속압력용기의 사용 전 음향방출시험 (Pre-service Acoustic Emission Testing for Metal Pressure Vessel)

  • 이종오;윤운하;이태희;이종규
    • 비파괴검사학회지
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    • 제23권3호
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    • pp.280-284
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    • 2003
  • 사용하지 않은 새 금속 압력용기에 대하여, 사용 전 음향방출시험을 수행할 때 장비점검, 탐촉자간 거리, 탐촉자 위치, 전 측정 시스템 점검, 가압방법, 잡음 제거법 및 시험 결과의 평가 등에 대한 절차를 수립하고 현장 응용시험이 수행되었다. 일반적으로 음향방출 시험은 많은 잡음을 포함하는데 시험동안 관찰결과를 기록하여 평가 시 시간 필터링함으로서 잡음을 제거할 수 있었다.

단일방향 섬유 복합재료 내의 초음파 전파 및 산란 현상의 해석과 시뮬레이션 (Analysis and Simulation of Ultrasonic Wave Propagation and Scattering in Unidirectional Fiber Composites)

  • 이춘재;임현준
    • 비파괴검사학회지
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    • 제21권3호
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    • pp.269-276
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    • 2001
  • 복합재료의 초음파검사는 매직의 탄성이방성으로 인해 빔스큐(beam skew)현상 등이 발생하기 때문에 등방성 재료의 검사에 비해 훨씬 어렵다. 그 동안의 많은 연구의 결과로서 이방성 재료 네 탄성파의 전파 현상에 대한 해석해법이 정립되어 있으나, 그 해석해가 매우 복잡하여 실제 문제의 해를 구하기 위해서는 수치적인 방법에 의존하여야 하는 경우가 많다. 본 연구에서는 횡등방 이방성(transversely isotropic)으로 가정할 수 있는 단일방향 섬유 복합재료 내 점원에 의한 초음파 전파의 해석해를 먼저 구하고, 이러한 복합재료를 질량-스프링 모델로 모델링하여 해석해에 상응하는 수치해를 구하였다. 그 결과, 초음파의 전파에 대한 수치해와 해석해가 매우 잘 일치하는 것을 확인하였다. 동일한 수치해석법을 사용하여 초음파가 복합재료의 자유표면에서 반사되는 현상과 균일에 의해 산란되는 현상에 대한 수치해도 구하였으며 그 결과를 파동역학의 관점에서 고찰하였다. 본 연구에서 그 유효성이 확인된 수치 모델은 복합재료의 초음파검사를 시뮬레이션 함에 있어 매우 유용하게 사용될 수 있을 것이다.

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Measurement of Cortisol in Human Serum by Isotope Dilution Liquid Chromatography/Mass Spectrometry and a Comparison through a Proficiency Testing

  • Lee, Hwa-Shim;Shin, Hye-Sun;Park, Sang-Ryoul;Park, Chang-Joon
    • Bulletin of the Korean Chemical Society
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    • 제31권5호
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    • pp.1149-1154
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    • 2010
  • Liquid chromatography/mass spectrometry using isotope dilution method has been established as a primary method for the measurement of cortisol in human serum. Verification of this method was accomplished by the participation in Consultative Committee for Amount of Substance-Metrology in Chemistry (CCQM) pilot study. Two levels of cortisol certified reference materials were prepared and certified by the established method. They were used as sample materials for the proficiency testing. The expanded uncertainty in the measurement of cortisol in human serum was approximately 1.2% at 95% confidence level. The results of the proficiency testing showed a good precision among the participants, but some bias to the certified values. This means that commercial field laboratories should keep traceability chain to SI unit through available reference measurement procedures and/or available reference materials.