• 대한치과보철학회지
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• 제39권6호
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• pp.682-697
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• 2001

This investigation evaluated the fracture toughness($K_{IC}$) of eight currently available core materials, and relate the fracture toughness value to fractography analysis and surface characteristics using a atomic force microscope (AFM). Single-edge notched (SEN) test specimens (n=10) and compact tension (CT) test specimens (n=10) were prepared conforming to the ASTM Standard E-399 for a high copper amalgam, three composite core materials (Core-Max II, Core Paste, Bisfil Core), two reinforced composite core materials (Ti-Core, Ti-Core Natural), a resin-modified glass ionomer core material (Vitremer), and a conventional glass ionomer core material (Ketac-Molar). The specimens were tested with an Instron Universal Testing Machine. The maximum loads were measured to calculate the fracture toughness ($K_{IC}$). Thereafter, fracture surfaces of SEN specimens of each material were investigated for fractography analysis using scanning electron microscope. And, disc-shaped specimens with 1mm thickness were fabricated for each material and were investigated under AFM for surface morphology analysis. The results were as follows: 1. Bisfil Core showed the highest mean fracture toughness regardless of test methods. 2. For the tooth-colored materials, Ti-Core Natural exhibited the highest fracture toughness. 3. Ketac Molar showed a significantly low fracture toughness when compared with the amalgam and the composite resin core materials(p<0.05). 4. The fracture toughness values obtained with the single-edge notched test, except Ketac Molar, were higher than those obtained in the compact tension test. 5. SEM revealed that the fracture surface of high fracture toughness material was rougher than that of low fracture toughness material. 6. AFM revealed that the surface particles of the composite resins were smaller in size, with a lower surface roughness than the glass ionomer core materials.

• 한국해양공학회지
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• 제15권3호
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• pp.63-68
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• 2001

SG-365 steel is an important material and used for manufacturing a pressure vessel which the gas piping. In this investigation, the elastic plastic fracture toughness of this material is evaluated by the an unloading compliance method according to the ATM E813-97 method on the smooth and side groove 1CT specimens. The effect of smooth and side groove is studied on the elastic plastic fracture toughness. The side grooved specimen is very useful in estimation of the $J_IC. Because it is much easier than the smooth specimen to the onset of the ductile tearing by the R curve method. Besides, it improves the accuracy of toughness values, decreases the scattering of them and tunneling and shear lip by the side groove.

• 한국정밀공학회지
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• 제22권3호
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• pp.130-136
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• 2005

The nondestructive evaluation system consisted of a ball indentation tester and a ultrasonic tester was developed to evaluate material properties. The relations between the parameters from test results using the system and the results of tensile and fracture toughness tests were investigated. The fracture toughness and tensile properties could be determined using the system. Some metallic materials were experimented to predict the fracture toughness and tensile properties and verify the relations between them. The predicted fracture toughness and tensile properties show a good agreement with the results obtained by conventional tests. It is found that the material properties and the material degradation can be evaluated using the nondestructive evaluation system.

• 대한기계학회논문집A
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• 제22권1호
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• pp.64-72
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• 1998

This paper was undertaken to develop the fracture toughness testing method using small and single specimen compared to the conventional method in evaluating elastic-plastic fracture toughness of the superconducting magnet structural material at cryogenic temperature. The elastic-plastic fracture toughness test was conducted by using the unloading compliance method recommended by ASTM E813-89 to accomplish the above purpose. And, the 20% side-grooved 0.5TCT and 1TCT specimens were used to evaluate the fracture toughness by using as possible as miniaturized CT specimen. The unloading compliance method was a very useful method in evaluating elastic-plastic fracture toughness at cryogenic temperature. It could be taken valid fracture toughness values by using 20% side-grooved 0.5TCT specimen recommended by ASTM E813-89.

• The Korean Journal of Ceramics
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• 제4권4호
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• pp.311-322
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• 1998

American Society for Testing and Materials (ASTM) standard test method PS 070-97 has been created for measuring fracture toughness of advanced ceramics. PS 070-97 includes three test methods which use beams in bending: chevron notch (CNB), single-edged precracked beam (SEPB), and surface crack in flexure (SCF). Supporting data has been collected through several Versailles Advanced Materials and Standards round robins. This paper discusses the evolution of the standard including the rationale for the choice of the three methods and the specifications in the standard. Progress on Standard Reference material 2100 which will have certified values of fracture toughness is presented.

• 대한기계학회논문집A
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• 제22권2호
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• pp.343-351
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• 1998

This paper was investigated degradation of the fracture toughness caused by sensitizing heat-treatment of the cryogenic structural material JN1 base metal using unloading compliance method reported as useful a method in evaluating the elastic-plastic fracture toughness at cryogenic temperature. The specimens used in this paper were 20% side-grooved 0.5T-CT specimens which were machined in the JN1 base metal. Also, to investigate cryogenic fracture toughness of the fusion line region in the JN1 GTA weldments, it was also used 20% side-grooved 0.5T-CT specimens that was machined fusion line to located in the middle of the specimen. The cryogenic fracture toughness values of the JN1 base metal were significantly decreased with increasing the time and temperature of the heat treatment. The fracture toughness value obtained from the fusion line specimen was invalid, but it was lower value than that of the JN1 base metal. Especially, this value was approximately equal with that obtained from the JN1 650.deg. C-5h heat-treated material.

• 비파괴검사학회지
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• 제18권1호
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• pp.10-16
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• 1998

사용중인 터빈 로터에서 균열이 발견된다면 그 안전성을 평가하기 위해서는 제조 당시의 재료물성 데이터가 아닌 열화된 재료의 물성 및 인성을 사용해야 한다. 본 연구에서는 시험재료로 터빈 로터재로 널리 사용되고 있는 1Cr-1Mo-0.25V강을 사용하였다. 로터강의 경우 발전소에서 실제 사용된 열화재를 종류별로 입수하는 것은 매우 어렵기 때문에 실제로 열화된 재료의 미세조직과 유사한 미세조직을 갖는 시료를 얻기 위해서 실제 사용온도보다 높은 $630^{\circ}C$에서 등온 열화처리하여 열화도가 다른 7종류의 시료를 만들었다. 열화도와 재료의 인성을 비파괴적으로 평가하기 위하여 직류 전위차법을 이용하였으며, 상온에서 전기비저항을 측정하였다. 열화도의 증가에 따라 전기비저항과 재료인성은 일정시간까지는 감소하는 것으로 나타났으며, 전기비저항과 인성과의 상관관계를 만들었다. 따라서 이를 이용하여 비파괴적으로 재료인성을 평가할 수 있는 기초를 마련하였다.

• 동력기계공학회지
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• 제11권1호
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• pp.127-133
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• 2007

SG-365 steel is an important material and used for manufacturing a pressure vessel which the gas piping. In this investigation, the elastic plastic fracture toughness of this material is evaluated by the unloading compliance method according to the ASTM E813-97 and E1152-97 method on the smooth and side groove 1CT specimens. The effect of smooth and side groove is studied on the elastic plastic fracture toughness. The side grooved specimen is very useful in estimation of the $J_{IC}$. It is much easier than the smooth specimen to the onset of the ductile tearing by the R curve method. Besides, it improves the accuracy of toughness values, decreases a phenomenon of the tunneling and shear lip by the side groove.

• Fibers and Polymers
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• 제7권3호
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• pp.286-294
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• 2006

This study has examined the flexural properties of natural and chemically modified coir fiber reinforced cementitious composites (CFRCC). Coir fibers of two different average lengths were used, and the longer coir fibers were also treated with a 1% NaOH solution for comparison. The fibers were combined with cementitious materials and chemical agents (dispersant, defoamer or wetting agent) to form CFRCC. The flexural properties of the composites, including elastic stress, flexural strength, toughness and toughness index, were measured. The effects of fiber treatments, addition of chemical agents and accelerated ageing of composites on the composites' flexural properties were examined. The results showed that the CFRCC samples were 5-12 % lighter than the conventional mortar, and that the addition of coir fibers improved the flexural strength of the CFRCC materials. Toughness and toughness index, which were associated with the work of fracture, were increased more than ten times. For the alkalized long coir fiber composites, a higher immediate and long-term toughness index was achieved. SEM microstructure images revealed improved physicochemical bonding in the treated CFRCC.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2001년도 춘계학술대회논문집A
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• pp.268-273
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• 2001

Fossil power plants operated in high temperature condition are composed of components such as turbine, boiler, and piping system. Among these components, turbine blades made with 12%Cr steel operate at a temperature above $500^{\circ}C$. Due to the long term service, turbine blades experience material degradation manifested by change in mechanical and microstructural properties. The need to make life assessment and to evaluate material degradation of turbine blade is strongly required but in reality, there is a lack of knowledge in defining failure mechanism and fundamental data for this component. Therefore, in making life assessment of turbine blade, evaluation of material degradation must be a priority. For this purpose, evaluation of toughness degradation is very important. The major cause of toughness degradation in 12Cr turbine blade is reported to be critical corrosion pitting induced by segregation of impurity elements(P etc.), coarsening of carbide, and corrosion, but the of materials for in-service application. In this study, the purpose of research is focused on evaluating toughness degradation with respect to operation time for 12%Cr steel turbine blade under high temperature steam environment and quantitatively detecting the degradation properties which is the cause of toughness degradation by means of non-destructive method, electrochemical polarization.