• Natural Product Sciences
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• v.25 no.3
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• pp.222-227
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• 2019

Quantitative nuclear magnetic resonance (qNMR) is a well-established method adopted by international pharmacopoeia for quantitative and purity analyses. Emodin is a type of anthraquinone, well known as the main active component of Fabaceae, Polygonaceae and Rhamnaceae. Purity analysis of emodin is usually performed by using the high-performance liquid chromatography (HPLC)-UV method. However, it cannot detect impurities such as salts, volatile matter, and trace elements. Using the qNMR method, it is possible to determine the compound content as well as the nature of the impurities. Several experimental parameters were optimized for the quantification, such as relaxation delay, spectral width, number of scans, temperature, pulse width, and acquisition time. The method was validated, and the results of the qNMR method were compared with those obtained by the HPLC and mass balance analysis methods. The qNMR method is specific, rapid, simple, and therefore, a valuable and reliable method for the purity analysis of emodin.

• KEPCO Journal on Electric Power and Energy
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• v.6 no.4
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• pp.427-432
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• 2020

In this study, a multi-zone furnace analysis method that couples a 1D energy and mass balance calculation with a 3D radiative heat transfer calculation is tested in order to verify its reliability. The calculated results for a domestic 500 MW capacity coal-fired boiler furnace were compared with the design data of the boiler manufacturer and CFD analysis, and a good agreement was achieved. Although this calculation method is less sophisticated than the CFD furnace analysis, it has an advantage in terms of calculation time while being able to provide the furnace behavior according to the fuel characteristics and operational variable changes. Therefore, it is expected to be useful for boiler operation diagnosis and daily fuel/operation planning.

• Journal of Welding and Joining
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• v.19 no.4
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• pp.399-405
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• 2001

A dynamic force balance model is proposed in this work as an extension of the previous static force balance model to predict metal transfer in arc welding. Dynamics of a pendant drop is modeled as the second order system, which consists of the mass, spring and damper. The spring constant of a spherical drop at equilibrium is derived in the closed-form equation, and the inertia force caused by drop vibration is included in the drop detaching condition. While the inertia force is small in the low current range, it becomes larger than the gravitational force with current increase. The inertia force reaches half of the electromagnetic force at transition current, and has considerable effects on drop detachment. The proposed dynamic force balance model predicts the detaching drop size more accurately than the static force balance model.

• The Journal of Korean Physical Therapy
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• v.27 no.2
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• pp.124-127
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• 2015

Purpose: The emphasis on gait rehabilitation after stroke depends on training support through the lower limbs, balance of body mass over the changing base of support. However, muscle weakness, lack of control of lower limb, and poor balance can interfere with training after stroke. For this case study report, a wearable robot orthosis was applied to stroke patients in order to verify its actual applicability on balance and gait ability in the clinical field. Methods: Two stroke patients participated in the training using the wearable robot orthosis. Wearable robot orthosis provides patient-initiated active assistance contraction during training. Training includes weight shift training, standing up and sitting down, ground walking, and stair up and down Training was applied a total of 20 times, five times a week for 4 weeks, for 30 minutes a day. Gait ability was determined by Stance phase symmetry profile, Swing phase symmetry profile, and velocity using the GAITRite system. Balance ability was measured using the Biodex balance system. Results: Subjects 1, 2 showed improved gait and balance ability with mean individual improvement of 72.4% for velocity, 19.4% for stance phase symmetry profile, 9.6% for swing phase symmetry profile, and 13.6% for balance ability. Conclusion: Training utilizing a wearable robot orthosis can be useful for improvement of the gait and balance ability of stroke patients.

• Proceedings of the Korean Nuclear Society Conference
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• 1996.05b
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• pp.108-113
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• 1996

Several analytical models for the departure from nucleate boiling (DNB) phenomenon have been developed during the last decade. Among these, Chang & Lee's model based on a bubble crowding mechanism is remarkable in the fundamental features characterized as the formulation of mass, energy, and momentum balance equation at thermal-hydraulic conditions leading to the DNB. However, Bricard and Souyri remarked that the assumption of stagnant bubbly layer at the DNB condition is questionable and the signs on the axial projections of the momentum fluxes at the core/bubbly layer interface in the momentum balance equations are erroneous. From this remark, Chang & Lee's model has been re-examined and modified by correcting the erroneous treatments in the momentum balance equations and removing the spurious assumptions. The revised model predicts well the extensive DNB data of water in uniformly heated tubes at low qualities and shows more accurate prediction compared with the original model.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2006.11a
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• pp.135-138
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• 2006

We developed an engine system design program by balancing the pressure-mass-power relation which can be acquired from each component's specification. In gas generator type open-cycle rocket engine system it is possible to distinguish the variables into two categories, which are input variables and requirement variables. We define 11 design variables corresponding to the 11 balance equations as functions of pressure, mass and power of target engine system. We solved these equations by Newton method. As an example we designed gas generator cycle engine system and finally we could conclude that this developed program is well suited to the engine system design.

• Korean Journal of Air-Conditioning and Refrigeration Engineering
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• v.10 no.5
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• pp.535-549
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• 1998

A numerical study for performance analysis of a counterflow type forced draft tower and natural draft cooling tower has been performed based on the method using the finite volume method with non-orthogonal body fitted and non-staggered grid system. For solving the coupling problem between water and air, air enthalpy balance, moisture fraction balance, water enthalpy balance, and water mass balance equations are solved with Navier-Stoke’s equations simultaneously. For the effect of turbulence, the standard k-$\varepsilon$ turbulent model is implied in this analysis. The predicted result of the present analysis is compared with the experimental data and the commercial software result to validate the present study, The predicted results show good agreement with the experimental data and the commercial software result. To investigate the influence of the cooling tower design parameters such as approach, range and wet bulb temperature, parametric studies are also peformed.

• Transactions of the Korean Society of Automotive Engineers
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• v.5 no.5
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• pp.51-66
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• 1997

A heat transfer model of the intake valve in a spark ignition engine is presented, which is calibrated with a number of the valve temperature profiles measured during engine warm-up for the gaseous fuel(propane). The valve is divided into four identical elements for which the assumption of lumped thermal mass is applied. The calibration is made so that the difference between the measued and simulated valve temperatures becomes minimal. Then the model is applied to the cases of the liquid fuel(indolene) to estimate the amount of the liquid fuel vaporized from the intake valve by assuming that fuel evaporation accounts for the deficit of the heat balance budget. The results of the model show quantitative contribution of each heat transfer source to the heat balance. The behavior of the calculated mass fraction of the fuel vaporized from the intake valve explains how the liquid fuel evaporate during engine warm-up. The mass fraction at warmed-up condition is closely related with the fraction directly targeted on the valve back by the fuel spray geometry.

• Biotechnology and Bioprocess Engineering:BBE
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• v.6 no.1
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• pp.42-50
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• 2001

The activity of immobilized cell-support particle aggregates is influenced by physical and biochemical elements, mass transfer, and physiology. Accordingly, the mathematical model discussed in this study is capable of predicting the steady state and transient concentration profiles of the cell mass and substrate, plus the effects of the substrate and product inhibition in an immobilized cell-support aggregate. The overall mathematical model is comprised of material balance equations for the cell mass, major carbon source, dissolved oxygen, and non-biomass products in a bulk suspension along with a single particle model. A smaller bead size and higher substrate concentration at the surface of the particle, resulted in a higher supply of the substrate into the aggregate and consequently a higher biocatalyst activity.

• Journal of Korean Society of Water and Wastewater
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• v.33 no.5
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• pp.367-377
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• 2019

In this study, the fate and removal of 15 pharmaceuticals (including stimulants, non-steroidal anti-inflammatory drugs, antibiotics, etc.) in unit processes of a sewage treatment plant (STP) were investigated. Mass loads of pharmaceuticals were 2,598 g/d in the influent, 2,745 g/d in the primary effluent, 143 g/d in the secondary effluent, and 134 g/d in the effluent. The mass loads were reduced by 95% in the biological treatment process, but total phosphorous treatment did not show a significant effect on the removal of most pharmaceuticals. Also, mass balance analysis was performed to evaluate removal characteristics of pharmaceuticals in the biological treatment process. Acetaminophen, caffeine, acetylsalicylic acid, cefradine, and naproxen were efficiently removed in the biological treatment process mainly due to biodegradation. Removal efficiencies of gemfibrozil, ofloxacin, and ciprofloxacin were not high, but their removal was related to sorption onto sludge. This study provides useful information on understanding removal characteristics of pharmaceuticals in unit processes in the STP.