• Title/Summary/Keyword: Magnetic particles

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Ferromagnetic Resonance Studies of Ultrathin Co Layers in Co/Ag Multilayers

  • Dubowik, J.
    • Journal of Magnetics
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    • v.4 no.3
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    • pp.92-97
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    • 1999
  • A relationship between microstructure and ferromagnetic resonance of Co/Ag multilayers has been studied in as-deposited and annealed multilayers iwth ultrathin (dCo < 1 nm) Co layers. Depending on the nominal thickness of Co Co/Ag multilayers represent a system of fine magnetic particles (dCo < 0.4 nm) or discontionuous layered structure (dCo/0.5 nm). FMR data has been interpreted in the framework of a odel of interacting fine particles exhibiting superparamagnetic behavior. Changes in the FMR spectra upon annealing have been attributed to the growth of the Co particles and to a transition from the fcc to hcp atomic structure of the highly (111) textured Co particles.

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A Study of the Properties of Magnetic Particles in Medicinal Ointments (의학용 연고제에 포함된 자성물질 입자들의 성질에 대한 연구)

  • Do, Tae-Sung;Nam, Hyo-Duk;Park, Se-Gon;Hwang, Hyeun-Gook;Hwang, Yong-Soon;Kim, Eng-Chan;Park, Eun-Jung;V. I. Nikolaev;A. V. Bykov
    • Progress in Medical Physics
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    • v.8 no.1
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    • pp.69-79
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    • 1997
  • Stability of the properties of magnetite particles in novel medicinal magnetic ointments of multipurpose application has been studied by M ssbauer spectroscopy. It has been found that the comparative analysis of the results obtained by model fitting of $^{57}$ Fe nuclei spectra with those known for the system Fe$_3$O$_4$-${\gamma}$-Fe$_2$O$_3$ allows to identify the phase composition of the particles. It is noted that this composition, as well as that of the initial pure component in the form of a highly dispersed fraction (~100$\AA$), differs noticeably from the stoichiometric one. From the magnetic hyperfine field despite small particle sizes, the particles exhibit no superparamagnetism (in the temperature range from 95 to 300K). Radiative sterilization of the ointments has no effect on the magnetic component composition.

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Development of Microfluidic Chip for Enrichment and DNA Extraction of Bacteria Using Concanavalin A Coated Magnetic Particles (Concanavalin A가 코팅 된 자성 입자를 이용한 미생물 농축 및 유전자 추출 칩 개발)

  • Kwon, Kirok;Gwak, Hogyeong;Hyun, Kyung-A;Jung, Hyo-Il
    • Journal of Sensor Science and Technology
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    • v.27 no.4
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    • pp.237-241
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    • 2018
  • The real-time enrichment and detection of pathogens are serious issues and rapidly evolving field of research because of the ability of these pathogens to cause infectious diseases. In general, bacterial detection is accomplished by conventional colony counting or by polymerase chain reaction (PCR) after DNA extraction. As colony counting requires considerable time to cultivate, PCR is an attractive method for rapid detection. A small number of pathogens can cause diseases. Hence, a pretreatment process, such as enrichment is essential for detecting bacteria in an actual environment. Thus, in this study, we developed a microfluidic chip capable of performing rapid enrichment of bacteria and the extraction of their genes. A lectin, i.e., Concanavalin A (ConA), which shows binding affinity to the surface of most bacteria, was coated on the surface of magnetic particles to nonspecifically capture bacteria. It was subsequently concentrated through magnetic forces in a microfluidic channel. To lyse the captured bacteria, magnetic particles were irradiated by a wavelength of 532nm. The photo-thermal effect on the particles was sufficient for extracting DNA, which was consequently utilized for the identification of bacteria. Our device will help monitor the existence of bacteria in various environmental situations such as water, air, and soil.

Preparation of polymer composites containing hollow magnetic particles and measurement of their electromagnetic properties (중공 자성입자를 포함한 복합재료 제조 및 전자파 특성 측정)

  • Yi, Jin-Woo;Lee, Sang-Bok;Kim, Jin-Bong;Lee, Sang-Kwan;Park, Ki-Yeon
    • Composites Research
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    • v.21 no.2
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    • pp.31-35
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    • 2008
  • In order to design light weight and high efficient electromagnetic wave absorbing materials, hollow magnetic particles have been introduced in this study. The electroless plating method has been utilized to coat Ni and Fe on the substrates of synthesized polystyrene particles of submicron size. Removing polystyrene particles by heat treatment resulted in hollow structures. Observation by SEM, TEM and EDS confirmed the surface morphology and coating thickness of Ni and Fe. Polymeric composites containing hollow particles were tested in order to compare the electromagnetic properties between Ni coated and Fe costed particles. The composite of 30 wt% Fe hollow particles showed the higher complex permeability than Ni hollow particles or the conventional barium ferrite particles.

Dry Magnetic Particle Inspection of Ingot Cast Billets (강편 빌레트의 건식 자분 탐상)

  • Kim, Goo-Hwa;Lim, Zhong-Soo;Lee, Eui-Wan
    • Journal of the Korean Society for Nondestructive Testing
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    • v.16 no.3
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    • pp.162-173
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    • 1996
  • Dry magnetic particle inspection(MPI) was performed to detect the surface defects of steel ingot cast billets. Magnetic properties of several materials were characterized by the measurement of the B-H hysteresis curve. The inspection results were evaluated in terms of the magnetizing current, temperature, and the amount of magnetic particles applied to billets. Magnetic flux leakage near the defect site of interest was measured and compared with the results of calculation by the finite element method in the case of direct magnetizing current. Direct and alternating magnetizing currents for materials were deduced by the comparison of the inspections. Results of the magnetic particle inspection by direct magnetizing current were compared with those of finite element method calculations, which were verified by measuring magnetic leakage flux above the surface and the surface defects of the material. For square rods, due to the geometrical effect, the magnetic flux density at the edges along the length of the rods was about 30% of that at the center of rod face for a sufficiently large direct magnetizing current, while it was about 70% for an alternating magnetizing current. Thus, an alternating magnetizing current generates rather uniform magnetic flux density over the rods, except for the region on the face across about 10 mm from the edge. The attraction of the magnetic particle by the magnetic leakage field was nearly independent of the surface temperature of the billets up to $150^{\circ}C$. However, the temperature should have been limited below $60^{\circ}C$ for an effective fixing of gathered magnetic particles to the billet surface using methylene chloride. We also found that the amount of applied magnetic particles tremendously affected the detection capability.

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Synthesis and Magnetic Properties of Dendron Capped Fe2O3 Nanoparticles

  • George, Sheby M.;Hong, In-Seok;Kim, Jin-Kwon
    • Bulletin of the Korean Chemical Society
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    • v.29 no.8
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    • pp.1545-1553
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    • 2008
  • Using a one-pot reaction technique, monodisperse $\gamma-Fe_2O_3$ nanoparticles were prepared by thermal decomposition of Fe$(CO)_5$ in the presence of a long alkyl chain terminated dendron surfactant. The size of the particles is controlled by adjusting the concentration of the dendron ligands in the reaction solution. Spherical, 2 nm sized nanoparticles were obtained with a 3:1 ratio of dendrons to Fe$(CO)_5$, while 4.6 nm sized particles were formed with a 1:3 ratio. Superparamagetic properties of 2 nm, 4 nm, and 4.6 nm sized particles were measured using a SQUID magnetometer.

Synthesis and Compaction of Al-based Nanopowders by Pulsed Discharge Method

  • Rhee, Chang-Kyu;Lee, Geun-Hee;Kim, Whung-Whoe
    • Journal of Powder Materials
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    • v.9 no.6
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    • pp.433-440
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    • 2002
  • Synthesis and compaction of Al-base nano powders by pulsed discharge method were investigated. The aluminum based powders with 50 to 200 nm of diameter were produced by pulsed wire evaporation method. The powders were covered with very thin oxide layer. The perspective process for the compaction and sintering of nanostructured metal-based materials stable in a wide temperature range can be seen in the densification of nano-sized metal powders with uniformly distributed hard ceramic particles. The promising approach lies in utilization of natural uniform mixtures of metal and ceramic phases, e.g. partially oxidized metal powders as fabricated in our synthesis method. Their particles consist of metal grains coated with oxide films. To construct a metal-matrix material from such powder, it is necessary to destroy the hard oxide coatings of particles during the compaction process. This goal was realized in our experiments with intensive magnetic pulsed compaction of aluminum nanopowders passivated in air.

Experimental investigation of organic fouling mitigation in membrane filtration and removal by magnetic iron oxide particles

  • Jung, Jaehyun;Sibag, Mark;Shind, Bora;Cho, Jinwoo
    • Membrane and Water Treatment
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    • v.11 no.3
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    • pp.223-229
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    • 2020
  • Here magnetic iron oxide particles (MIOPs) were synthesized under atmospheric air and which size was controlled by regulating the flow rate of alkali addition and used for efficient removal of bovine serum albumin (BSA) from water. The MIOPs were characterized using field-emission scanning electron microscopy (FE-SEM), Fourier transformation-Infrared spectroscopy (FT-IR) and vibrating sample magnetometer (VSM). The results revealed a successful preparation of the MIOPs. The removal efficiency for BSA using MIOPs was found to be about 100% at lower concentrations (≥ 10 mg/L). The maximum adsorption of 64.7 mg/g for BSA was achieved as per the Langmuir adsorption model. In addition, microfiltration membrane for removal of BSA as model protein organic foulant is also studied. The effect of various MIOPs adsorbent sizes of 210, 680 and 1130 nm on the absorption capacity of BSA was investigated. Water permeability of the BSA integrated with the smallest size MIOPs membrane was increased by approximately 22% compared by the neat BSA membrane during dead-end filtration. Furthermore, the presence of small size MIOPs were also effective in increasing the permeate flux.

Oil Separation from Oil-Contaminated Seawater by MHD Method I (선박사고로 인한 해양유출기름의 MHD방식 분리기술 연구 I)

  • Lee, Seung-Hwan
    • Proceedings of the Korean Institute of Navigation and Port Research Conference
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    • v.29 no.1
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    • pp.299-303
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    • 2005
  • A new method of oil separation from oil-contaminated seawater based on electromagnetic forces, so-called MHD method was designed and formulated. MHD method has advantages of easy treatment of separated oil as well as little effect upon the environment, comparing with a conventional separation method using magnetic powders. Assuming high polymer particles instead of oil, the separation ratio (the mass of simulation particles / the total mass of simulation particles) for the sample fluid was calculated as fuction of electric current, magnetic field and seawater velocity.

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