• 한국자기학회지
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• 제16권4호
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• pp.211-215
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• 2006

구조 강이나 터빈로터 강의 기계적 물성은 자기적 특성과 관계되므로, 비파괴적으로 자기적 특성을 측정하여 기계적 물성을 평가하는 연구가 많이 수행되었다. 따라서 자동차용 강판으로 사용되는 냉연강판에서도 비파괴적으로 자기적 특성을 측정함으로써 냉연강판의 기계적 물성을 유추할 수 있을 것이고, 냉연강판 생산 라인에서 자기적 특성을 측정하여 온라인상에서 냉연강판의 기계적 특성을 모니터할 수 있을 것이다. 기계적 특성이 다른 세 종류의 냉연강판 CBQ 3060, CBQ 3041 및 CBQ 3036의 시편을 준비하고 교류 섭동 자기장을 인가하여 자기적 특성인 가역투자율을 비파괴적으로 측정함으로서 기계적 물성인 경도와의 상관관계를 규명하였다. 세 종류의 냉연강판 시편에서 기계적 물성인 비커스 경도, 항복강도 및 인장강도를 측정하였다. 주파수가20 Hz일 때, surface type 프로브로 측정한 섭동자기장의 제 1차 고조파인 가역투자율의 피크 간 간격에서 구한 보자력은 비커스경도, 항복강도 및 인장강도가 증가할 때 선형적으로 증가하였다. 주파수 20 Hz에서 lift-off에 대한 가역투자율 측정을 하였는데,lift-off가 증가함에 따라 고조파의 amplitude가 급격히 감소하였다.

• 한국자기학회지
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• 제8권3호
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• pp.138-143
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• 1998

본 연구에서는 RF magnetron reactive sputtering system에 의해 증착된 FeBN막의 자기박막의 자기특성과 비저항의 변화를 연구하엿다. 막의 자기특성과 비저항의 변화는 막내에 첨가되는 B, Si, N의 조성에 따라 큰 변화를 나타내었으며, 소량의 N의 첨가에 따라 우수한 자기 특성과 비저항이 증가하였다. 그러나 과도한 N의 첨가는 Fe4N과 같은 질화물의 형성으로 비저항은 증가하였으나 자기 특성은 열화되었다. 제조된 FeBN과 FeSiN 자성막은 1 Oe이하의 보자력과 18~19kG의 포화자속말도, 그리고 1000이상의 투자율을 갖는 우수한 연자기 특성을 보였다. 이때의 막의 조성은 AES(Auger Electron Spectroscpy)로 분석하여 Fe75(BN)25, Fe78(BN)25이었으며 비저항값은 100~120$\mu$$\Omega$-cm이었다.

• Journal of Magnetics
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• 제16권3호
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• pp.300-303
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• 2011

The effect of the hot-compaction temperature on the microstructure and magnetic properties of anisotropic nanocrystalline magnets was investigated. The hot-compaction temperature was found to impact both the magnetic properties and the microstructure of die-upset magnets. The remanence of the isotropic precursor increases slightly with the improved hot-compaction temperature, and the grains start to grow on the flake boundary at higher hot-compaction temperatures. After hot deformation, it was found that the change in the magnetic properties was the inverse of that observed with the hot-compaction temperature. Microstructural investigation showed that die-upset magnets inherit the microstructural characteristics of their precursor. For the die-upset magnets, hot pressed at low temperature, scarcely any abnormal grain growth on the flake boundary can be seen. For those hot pressed at higher temperatures, however, layers with large equiaxed grains could be observed, which accounted for the poor alignment during the hot deformation, and thus the poor magnetic properties.

• 열처리공학회지
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• 제37권1호
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• pp.9-15
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• 2024

Nd-Fe-B permanent magnets have been utilized on various industrial fields such as electric vehicles, generator, robots with actuator, etc, due to their outstanding magnetic properties even 10 times better than conventional magnets. Recently, there are many researches that report magnetic properties improved by controlling microstructure through adjusting alloying elements or conducting various processing. Especially, post-sintering annealing (PSA) can significantly improve the coercivity by modifying the distribution and morphology of Nd-rich phase which formed at grain boundaries. In this study, Nd-Fe-B sintered magnets were subjected to primary heat treatment followed by secondary heat treatment at 460℃, 500℃, and 540℃ to investigate the changes in microstructure and magnetic properties with the secondary heat treatment temperature. EBSD analysis was conducted to compare anisotropic characteristics. Through the SEM and TEM observation for analyzing the morphology and distribution of Nd-rich phase, we investigated the relationship between microstructure and magnetic properties of sintered Nd-Fe-B magnets.

• Journal of Magnetics
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• 제7권2호
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• pp.45-50
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• 2002

A magnetic field annealing is firstly used for nanostructured Sm-Co/Co films, prepared by magnetron sputtering method. The effects of magnetic field annealing on single-layered Sm-Co films are different from those on multi-layered Sm-Co/Co films. A detailed analysis of microstructures and magnetic properties is made by means of HRTEM, Auger electron spectroscopy, XRD and Physical Property Measurement System (PPMS). From magnetic properties and microstructure analysis, it was confirmed that these differences originate from the effects of magnetic field annealing on crystallization behavior of the films. The relationship between magnetic properties and microstructures explains a different demagnetization process of single-layered and multilayered films. For the single-layered Sm-Co films, magnetic-field-annealing makes the main phases change from $CaCu_5/ to Zn_2Th_{17}$ structure, resulting in a decrease of coercivity. The results show that the magnetic-field-annealing is useful to improve the properties of nanostructured Sm-Co(30 nm)/Co(10 nm) films, which ascribe to improving the pinning effectiveness in coercivity mechanism and decreasing the magnetostatic interaction of films. A very high coercivity about 0.7 T was obtained from nanoscaled multi-layered Sm-Co(30 nm)-/Co(10 nm) films.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2001년도 하계학술대회 논문집
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• pp.478-480
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• 2001

Fe-base amorphous films exhibit large saturation magnetostriction and soft magnetic Properties, which make them suitable for strain sensor applications. Most important material properties for the performance of these elements are the superior soft magnetic properties, such as high permeability and small coercive force, as well as magnetoelastic properties. It is well known that the strain generated in film deposition and/or post-heat treatment processes is one of important material properties, which effects on the soft magnetic properties of the film via magnetoelastic coupling. In this study, the effect of an isotropic strain in plane of magnetic films have been performed experimently. Amorphous films with the composition of (F $e_{90}$ $Co_{10}$)$_{78}$S $i_{l2}$ $B_{10}$ were employed in this study. The film with 5${\mu}{\textrm}{m}$ thick was deposed onto the polyimide substrate with 50${\mu}{\textrm}{m}$ thick by virtue of RF sputtering. The film was subject to post annealing with a static magnetic field with 500Oe magnetic field intensity at 35$0^{\circ}C$ for 1 hour. The polyimide substrate with the film was bonded with an adhesive on PZT piezoelectric substrate with 600${\mu}{\textrm}{m}$ thick in applying voltage of 500V. The change in MH loops of films due to the isotropic strain was measured by using VSM. The coercive force was evaluated from MH loops. It has shown in the results that M-H loops of films are subject to change considerably with a dc voltage, resulting of the magnetization rotation from normal to plane direction as the applied voltage is changed from 500V to 250V.50V.V.

• 한국초전도저온공학회:학술대회논문집
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• 한국초전도저온공학회 1999년도 제1회 학술대회논문집(KIASC 1st conference 99)
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• pp.77-80
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• 1999

In this paper. We experimentally investigated the magnetic properties of YBCO bulk superconductor using AC magnetization method. The sample is 2.8cm wide in a diameter and 1.4cm long. We applied Ac magnetic field parallel to the direction of length of YBCO bulk. It is observed that YBCO bulk has the diamagnetic properties. AC loss calculation of YBCO bulk superconductor was performed by evaluating the total area of magnetization traces. As depends on the frequency and amplitude of the applied magnetic field.

• 한국정밀공학회지
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• 제6권4호
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• pp.103-107
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• 1989

The effects of annealing temperature on the magnetic properties (maximum permeability, coercive force and remanence) and mechanical properties (hardness, tensile strength and elongation at rupture) were analyzed using the nondestructive impulsive magnetic analyzer in a medium carbon cold rolled steel sheet. This nondestructive method was very useful for the analysis of magnetic and mechanical properties of materials. As it was known in the literature, the three distinct processes that indicate the recovery, recrystallization, and grain growth of a metal were measured with the non-destructive analyzer.

• 한국전기전자재료학회논문지
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• 제15권3호
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• pp.281-286
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• 2002

In odder to investigate the magnetic properties of CoCr-based bilayered thin films on kind of underlayer, we introduced amorphous Si layer to Co-Cr(-Ta) magnetic layer as underlayer. First, we prepared CoCr and CoCrTa single layer using the Facing Targets Sputtering system to investigate theirs properties. It was revealed that with increasing the film thickness of CoCr, CoCrTa single layer, crystalline orientation and perpendicular coercivity was improved. The CoCrTa thin film showed bettor crystalline and magnetic characteristics than CoCr thin film. As a result of investigating magnetic properties of CoCr and CoCrTa magnetic layer on introducing the Si underlayer, perpendicular coercivity and saturation magnetization of CoCr/Si and CoCrTa/Si bilayered thin film were decreased due to the increased grain size and diffusion of Si atoms to magnetic layer. And they showed constant with increasing the film thickness of Si thin film. However, in case of CoCrTa/Si bilayered thin film, in-plane coercivity was controlled low at about 250Oe. The c-axis orientations of CoCr/si and CoCrTa/Si bilayered thin film showed a good crystalline characteristics as about $2^{\circ}$.

• E2M - 전기 전자와 첨단 소재
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• 제11권10호
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• pp.72-77
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• 1998

The effects of Al micro-bumps on the magnetic properties of CoCr(Pt)Ta/Cr films deposited on glass substrates were investigated. The coercivity increased and the coercivity squareness decreased by incorporating Cr/Al underlayers. The cause of the coercivity increase is attributed to the reduction of Co(0002) texture, the increase of magnetic isolation of CoCr(Pt)/Ta grains, and the refinement of CoCr(Pt)/Ta grains deposited on Cr/Al underlayers. The effects of an Al overlayer on the magnetic properties of CoCr(Pt)Ta/Cr films were also studied. The decrease of coercivity squareness is ascribed to the magnetic isolation of CoCr(Pt)Ta grains.