• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.10a
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• pp.70-73
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• 2007

The forming characteristics of cup-rod combined extrusion process were investigated with process parameter change. Simultaneous forward rod extrusion and backward cup extrusion was conducted with magnesium alloy, AZ31B. Process parameters such as forward extrusion ratio, backward extrusion ratio, and working temperature were controlled in a specific region and the effects of the parameter change were examined. Surface crack was developed in a certain state of the process parameters combination. The crack-free forming limit of the alloy in the combined process was disclosed by the parameter study. The microstructures of the initial and extruded workpieces were observed.

• Journal of the Korean institute of surface engineering
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• v.42 no.3
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• pp.109-115
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• 2009

Magnesium is one of the lightest metals, and magnesium alloys have excellent physical and mechanical properties such as high stiffness/weight ratios, good castability, good vibration and shock absorption. However their poor corrosion resistance, wear resistance, hardness and so on, have limited their application. To improve these defects, many techniques are developed. Micro arc oxidation(MAO) is a one of the surface treatments under anodic oxidation in which ceramic coating is directly formed on the surface of magnesium alloy. In this study, the characteristics of anodic film were examined after coating the AZ31B magnesium alloy through the MAO process. MAO was carried out in potassium hydroxide, potassium fluoride, and various concentration of sodium silicate in electrolyte. The morphology and chemical composition of the coating layer were characterized by SEM, XRD, EPMA and EDS. The hardness of anodic films was measured by micro-vickers hardness tester. As a result, the morphology and composition of anodic film were changed by concentration of sodium silicate. Thickness and Si composition of anodic film was increased with increasing concentration of sodium silicate in electrolyte. The hardness of anodic film was highly increased when the concentration of sodium silicate was above 40 g/l in electrolyte.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2009.10a
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• pp.118-118
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• 2009

• Transactions of Materials Processing
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• v.31 no.3
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• pp.117-123
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• 2022

In this study, a commercial AZ61 magnesium alloy is extruded at 300 ℃ and 400 ℃ and the microstructures, mechanical properties, and high-cycle fatigue properties of the extruded materials are investigated. Both extruded materials have a fully recrystallized microstructure with no Mg₁₇Al₁₂ precipitates. The average grain size and maximum basal texture intensity of the extruded material increase with increasing extrusion temperature. The material extruded at 400 ℃ (AZ61-400) has higher tensile yield strength and lower compressive yield strength than the material extruded at 300 ℃ (AZ61-300) because of the stronger basal texture of the former. Because of coarser grain size, the tensile elongation of AZ61-400 is lower than that of AZ61-300. Despite the differences in microstructures and tensile/compressive properties, the two extruded materials have the same fatigue strength of 110 MPa. This is because the finer grain size of AZ61-300 causes an increase in fatigue strength, but its weaker texture causes a decrease in fatigue strength. In both extruded materials, fatigue cracks initiate at the surface of fatigue specimens at all stress amplitudes tested.

• Journal of Korea Foundry Society
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• v.23 no.5
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• pp.251-256
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• 2003

Effects of Ca addition on grain refinement, microstructure and mechanical properties of AZ31 Mg alloy were investigated. Due to Ca addition to Mg alloy (AZ31), the microstructure was refined, the quantity of $Mg_{17}Al_{12}$phase was reduced, and new $Al_2Ca$ phase was formed. The tensile property of AZ31 was increased with the minor addition of Ca, but was decreased rapidly over 0.2 wt.% of Ca content. The $Al_2Ca$ phase was considered to be detrimental to the mechanical property of AZ31 Mg alloy.

• Transactions of Materials Processing
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• v.20 no.7
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• pp.498-503
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• 2011

The strain rate sensitivity index, m, plays an important role in plastic deformation at elevated temperatures. It is affected by strain rate, temperature, and the microstructure of the material. The strain rate sensitivity index has been used as a constant in numerical analysis of plastic forming at a specified strain rate and temperature. However, the value of m varies as deformation proceeds at an elevated temperature and a certain strain rate. Thus, in this present study, the value of m has been characterized as a function of strain by multiple tensile jump tests for AZ31 magnesium alloy sheet, and the variation of m has been discussed in conjunction with the microstructural observations before and after deformation. The experimental results show that the variation of m is dependent on the temperature and strain rate. Grain growth with dynamic recrystallization also affects the variation of m.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.12 no.2
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• pp.594-599
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• 2011

In this paper, the effect of the boundary conditions on the reliability and the cumulative distribution characteristics of the fatigue failure life is analyzed in a magnesium alloy AZ31. The boundary conditions are specimen thickness, stress ratio, and maximum fatigue load. The statistical data of the fatigue failure life are obtained by fatigue crack propagation tests under the detail conditions for each boundary condition. The 3-parameter Weibull distribution is used to analyze a statistical characteristics of the fatigue failure life in magnesium alloy AZ31. It is found that the statistical fatigue failure life is long in the case of a thicker specimen, a larger stress ratio, and a smaller maximum fatigue load. Under the opposite cases, the reliability on the fatigue failure life is rapidly dropped.

• Design & Manufacturing
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• v.12 no.3
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• pp.42-47
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• 2018

Recently, in the surge of global environmental issues, there has been a great attention to lightweight materials in purpose of saving energy. Magnesium alloys not only have low specific gravity, and superb specific stiffness, but are also excellent in blocking vibrations and electromagnetic waves. So demand for this material is getting bigger rapidly throughout the industry. In this study, we examined the improvement of formability of magnesium alloy AZ31 material in warm working. Drawing, bending and shearing process were carried out by varying the forming temperature and the forming speed, and the influence of the variables on each process was studied. In the experiments, the high forming temperature and low forming speed results in high formability in the drawing process and the bending process. In the shearing process, as the forming temperature increases, the length of the fracture decreases.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2013.05a
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• pp.62-62
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• 2013

Magnesium alloys exhibit many attractive properties such as low density, high strength/weight ratio, high thermal conductivity, very good electromagnetic features and good recyclability. However, most commercial magnesium alloys require protective coatings because of their poor corrosion resistance. Attempts have been made to improve the corrosion resistance of the Mg alloys by surface treatments, such as chemical conversion coatings, anodizing, plating and metal coatings. Among them, chemical conversion coatings are regarded as one of the most effective and cheapest ways to prevent corrosion of Mg alloys. In this study, the effects of various $Zn^{2+}$ concentrations and pH levels on the formation of zinc phosphate conversion coatings (ZPCCs) on AZ31 magnesium alloy were investigated, and corrosion resistances of the coated samples were evaluated by immersion test and potentiodynamic polarization experiment. The corrosion resistance of the coated AZ31 samples was found to increase with increasing $Zn^{2+}$ concentration and the lowest corrosion rate was obtained for the samples coated at pH of 3.07, independent of $Zn^{2+}$ concentration. The best coatings on AZ31 were obtained at [$Zn^{2+}$] = 0.068 M and pH 3.07. At the conditions of [$Zn^{2+}$] = 0.068 M and pH 3.07, the formation and growth processes of ZPCCs on AZ31 Mg alloy are divided into four stages: formation of a dense layer, precipitation of fine crystals on the dense layer, growths of the inner and outer layers, and reorganization of outer crystalline layer.

• Transactions of Materials Processing
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• v.27 no.3
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• pp.145-153
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• 2018

Magnesium material could be widely used in the automotive industry because of its high strength to weight ratio, but the electric resistance spot welding process of magnesium sheets is difficult because of its low electric resistance and high thermal conduction and thermal expansion. For this reason, an electric resistance surface friction spot welding process using rotating dies is suggested for the spot welding of magnesium metal sheets. This welding method can be characterized by three heating methods: (1) electric resistance heating on contacted surface, (2) surface friction heating by rotating dies, and (3) thermal conduction heating from heated steel electrodes, for the fusion of metal at the interfacial zone between the two magnesium sheets. This welding process also has variables to explore, such as welding currents, diameters of the steel electrode, and rotating dies. It was found that the welding strength could reach industrial requirements by applying a welding current of 11.0kA, with steel electrodes of 12mm diameter, with rotating dies of 4.4 mm diameter, under the condition of a revolution speed of 1200rpm of rotating dies, for the surface friction spot welding process of AZ31 magnesium alloy sheets of 1.4mm thickness.