• Carbon letters
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• 제3권3호
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• pp.152-154
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• 2002

• Composites Research
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• 제27권5호
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• pp.196-200
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• 2014

A novel, simple and totally recyclable method has been developed for the synthesis of nontoxic, biocompatible and biodegradable bio-composite films from soy protein and silk protein. Bio films are defined as flexible films prepared from biological materials such as protein. These materials have potential application in medical and food as a packaging material. Their use depends on various parameters such as mechanical (strength and modulus), thermal, among others. In this study, prepare and characterization of bio films made from Soy Protein Isolate (SPI) (matrix) and Silk Fiber (SF) (reinforcement) through solution casting method by the addition of plasticizer and crosslinking agent. The obtained SPI and SPI/SF composites were subsequently subjected to evaluate their mechanical and thermal properties by using Universal Testing Machine and Thermal Gravimetric Analyzer respectively. The tensile testing showed significant improvements in strength with increasing amount of SF content and the % elongation at break of the composites of the SPI/SF was lower than that of the matrix. Though the interfacial bonding was moderate, the improvement in tensile strength and modulus was attributed to the higher tensile properties of the silk fiber.

• 대한기계학회논문집A
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• 제27권7호
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• pp.1159-1169
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• 2003

This paper investigates the effects of T-stress and plastic hardening mismatch on the interfacial crack-tip stress field via finite element analyses. Plane strain elastic-plastic crack-tip fields are modeled with both MBL formulation and a full SEC specimen under pure bending. Modified Prandtl slip line fields illustrate the effects of T-stress on crack-tip constraint in homogeneous material. Compressive T-stress substantially reduces the interfacial crack-tip constraint, but increases the J-contribution by lower hardening material, J$\_$L/. For bimaterials with two elastic-plastic materials, increasing plastic hardening mismatch increases both crack-tip stress constraint in the lower hardening material and J$\_$L/. The fracture toughness for bimaterial joints would consequently be much lower than that of lower hardening homogeneous material. The implication of unbalanced J-integral in bimaterials is also discussed.

• Elastomers and Composites
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• 제52권4호
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• pp.257-265
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• 2017

In this work, CR (Chloroprene Rubber) was emulsified by phase-inversion emulsification with nonionic surfactants (NP-1025, LE-1017, and OP-1019) and an anionic surfactant (SDBS; sodium dodecylbenzenesulfonate), and its stabilization was investigated through a study of its adsorption characteristics, zeta potential, and flow behavior. As the amount of the mixed surfactant increased, the droplet size decreased, resulting in the increase of viscosity. In particular, a CR emulsion with a lower absorbance in the UV spectrum exhibited the highest zeta potential. The results of this experiment showed that the CR emulsion prepared using (LE-1017) and SDBS was the most stable. In this study, calcium hydroxide and aluminum hydroxide were added to enhance the mechanical properties of the CR emulsion, and the relationship between tensile strength, tear strength and surface free energy were investigated. The tensile and tear strengths of the CR emulsion incresed as the amount of calcium hydroxide and aluminum hydroxide increased. The highest tensile and tear strengths and surface free energy were observed for additions of 1.0% calcium hydroxide and 0.80% aluminum hydroxide, respectively. It was concluded that the interfacial bonding strength was improved by the even dispersion of calcium hydroxide and aluminum hydroxide in the CR emulsion.

• 대한기계학회논문집
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• 제15권1호
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• pp.299-307
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• 1991

본 연구에서는 근사수평 반류 성층유동에서의 계면마찰계수에 관한 일반화된 실험식을 개발하고자 한다. 이 실험식은 본 저자가 발표한 포화수-수증기와 물-공기 의 실험자료를 기초로 개발되며 공학적인 응용을 위하여 기액상레이놀즈 수와 유체의 물성치를 포함하는 거시적인 유동변수로 표현된다. 또 동일한 계면 마찰계숭에 대한 Nikuradse의 표면조도와 계면의 특성치로 표현되는 무차원 계면 유효조도와의 상관관 계를 구명하고 포화수-수증기와 물-공기의 2상유동에 공통적으로 적용할 수 있는 무차 원 계면유효조도와의 상관관계를 구명하고 포화수-수증기와 물-공기의 2상유동에 공통 적으로 적용할 수 있는 무차원 계면유효조도를 제안할 예정이다. 마지막으로 본 연 구에서 개발한 실험식과 기존 실험식을 비교 검토하고자 한다.

• Tribology and Lubricants
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• 제25권6호
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• pp.404-408
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• 2009

본 연구에서는 마이크로/나노입자를 이용한 연마가공 공정에서의 입자-표면간 접촉상황에서 접촉계면의 기계적 성질과 재료제거율간의 관계를 실험적으로 고찰하였다. 연마가공 공정에서의 입자-평면간 접촉을 모사하기 위하여 팁 대신 실리카 입자를 부착한 콜로이드 프로브를 이용한 원자현미경 실험을 통하여 마찰력과 강성을 실험적으로 측정하였다. 실험결과와 이론적 접촉해석으로부터, 마찰계수는 횡방향 접촉강성에 따라 대체적으로 증가하고 재료제거율은 실리카 입자와 Cu, PolySi, Ni과 같은 다양한 재료표면간 접촉에서의 마찰계수들과 지수함수적인 비례관계를 가지고 있음을 규명하였다.

• 대한기계학회논문집
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• 제17권2호
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• pp.277-284
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• 1993

본 연구에서는 적분변환에 의한 해법을 사용하여 폐형으로 주어지는 엄밀해를 얻었다. 먼저 평면에 수직한 방향의 변위를 도입하여 주어진 문제를 Mellin 변환하 고 수식화 하면 Wiener-Hopf 방정식이 주어진다.이 방정식을 푼 다음 변위에 관한 적분 표현식을 점근(asymptotic)전개하여 평가하면 균열선단 부근의 변위가 결정된다. 이로부터 폐형(closed form)으로 구성되는 균열선단부근의 응력확대계수(stress in- tensity factor)를 얻었다. 이 결과를 가지고 특정한 경우에 해당되는 기존의 연구 결과와 비교하였다. 특별히 가해진 하중이 자기평형(self equilibrium)을 이루는 경 우에 한정하여 계면에 인접한 재료의 결과와 동일함을 무한고체물에 대한 해석에서 보 인 바 있는데, 이와같은 정성적인 결과가 본문제와 같이 계면방향 표면균열을 지니는 반무한 크기의 고체물에서도 유지되는가를 검토하였다. 아울러 본 연구와 동일한 모 양의 균열이라면 고체물표면 혹은 균열면에 임의로 분포하는 비평면하중문제에 대한 응력확대계수는 본 연구의 결과를 가지고 간단한 적분을 수행함으로써 용이하게 계산 됨을 보였다.

• 대한기계학회논문집A
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• 제30권3호
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• pp.260-268
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• 2006

The micromechanical approach was used to investigate the interfacial strain distributions of a unidirectional composite under transverse loading in which fibers were usually found to be randomly packed. Representative volume elements (RVE) for the analysis were composed of both regular fiber arrays such as a square array and a hexagonal array, and a random fiber array. The finite element analysis was performed to analyze the normal, tangential and shear strains at the interface. Due to the periodic characteristics of the strain distributions at the interface, the Fourier series approximation with proper coefficients was utilized to evaluate the strain distributions at the interface for the regular and random fiber arrays with respect to fiber volume fractions. From the analysis, it was found that the random arrangement of fibers had a significant influence on the strain distribution at the interface, and the strain distribution in the regular fiber arrays was one of special cases of that in the random fiber array.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2011년도 제40회 동계학술대회 초록집
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• pp.476-476
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• 2011

Introduction of CNTs into a metal matrix has been considered to improve the mechanical properties of the metal matrix. However, the binding energy between metals and pristine CNTs wall is known to be so small that the interfacial slip between CNTs and the matrix occurs at a relatively low external stress. The interfacial strength between CNT and metal matrix is thus one of the key factors for successful development of the CNT/metal composites. Defective or functionalized CNT has been considered to enhance the interfacial strength of nanocomposites. In the present work, we design the various realistic hybrid structures of the single wall CNT/Cu complexes and characterize the interaction between single wall CNTs and Cu nano-particle and Cu13 cluster using first principle calculations. The characteristics of functionalized CNTs with various surface functional groups, such as -COOH, -OH, and -O interacting with Cu are investigated. We found that the binding energy can be enhanced by the surface functional group including oxygen since the oxygen atom can mediate and reinforce the interaction between carbon and Cu. These results strongly support the recent experimental work which suggested the oxygen on the interface playing an important role in the excellent mechanical properties of the CNT/Cu composite.

• 약학회지
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• 제41권1호
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• pp.30-37
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• 1997

In order to formulate a controlled release system for oral drug delivery, the microcapsules were prepared in w/o emulsion containing cefaclor as a water-soluble model drug by th e method of interfacial polycondensation. Gelatin wis selected as a suitable polymer for interfacial polycondensation. Gelatin solution containing drug was emulsified in an organic phase under mechanical stirring. After emulsification, terephthaloyl chloride was added as cross linking agent, followed by mechanical stirring, washing and drying. Physical characteristics of microcapsules were investigated by optical microscopy, scanning electron microscopy and particle size analysis. Mean particle sizes of gelatin microcapsules were, in the range, of about 20~50 ${\mu}$m. The microcapsules were in good apperance with spherical shapes before washing, but were destroyed partially after washing and drying, even though some microcapsules were still maintained in their shapes. Contents of cefaclor in the microcapsules were calculated by UV spectrophotometry after 3 days extraction with pH 4 carbonate buffer solution. The effects of cross linking time. pH. concentration of cross-linking agent, and temperature on drug release kinetics have been discussed extensively.