• Journal of Welding and Joining
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• 제15권1호
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• pp.116-124
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• 1997

A scope of this study is to establish the optimum plasma spray conditions for fine ($5\mu\textrm{m}$) $Al_2O_3$ powder. However, the flowability of the $Al_2O_3$ powder is not so good because of irregular particle shape and fine particle size. Therefore, powder feeding system was modified by 1) change of powder feeding line material from polymer to copper 2) shorten the powder feeding tube length 3) heating the powder feeding system to $80^{\circ}C$4) vibrating the powder feeding line continuously, in order to feed the fine powder homogeneously. The homogeneous powder feeding conditions were obtained with the modified powder feeding system by controlling the powder carrier gas flow and the powder flow rate indicator. The best plasma spraying conditions for the fine $Al_2O_3$ powder were found out as 40kw gun power, 80 g/min. powder feed rate and 50 mm working distance after characterizing the microstructure, hardness and wear loss of the $Al_2O_3$ coating layer.

• 동아시아식생활학회지
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• 제21권4호
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• pp.553-562
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• 2011

The purpose of this study was to promote the consumption of rice by substituting goami powder for flour when making muffins. Goami powder was prepared in different particle sizes by grinding the powder for 5 min. 10 min. 15 min. and 20 min. Precisely 72.62% of the goami powder, particles were smaller than 75 ${\mu}m$, after grinding the powder for 20 min. with a consistency similar to that of flour (78.86%). To determine the optimal amount of water for goami powder muffin batter, the viscosity of both the flour and the goami powder batter was measured. The appropriate water quantity for goami powder muffins was set at 105 mL. The volume index of flour muffins was 132 mL, while that of the goami powder muffin (GM1, GM2, GM3 and GM4) was 123 mL, 119 mL, 119 mL and 118 mL, respectively. The hardness of the flour muffins, measured by a texture analyer, was 2.03${\times}10^3$ g/$cm^2$, The hardnesses of the goami powder muffins were 2.83${\times}10^3$ g/$cm^2$ for GM1, 2.44${\times}10^3$ g/$cm^2$for GM2, 2.33${\times}10^3$ g/$cm^2$ for GM3, and 2.36${\times}10^3$ g/$cm^2$ for GM4. The L-values and moisture content of the goami powder muffins were higher than those of the flour muffins. In a sensory evaluation the overall preference was the highest for flour muffins. However among the goami powder muffins, GM3, which was made with goami powder ground for 15 min. was the most preferred.

• 동아시아식생활학회지
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• 제21권6호
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• pp.888-896
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• 2011

The purpose of this study was to promote the consumption of cereals rich in dietary fiber by substituting brown rice, barley, oat and goami powder for flour in making muffins. All cereals powder was prepared by grinding for 15 min. The appropriate water quantity for cereal powders muffins was set at 105 mL. The volume index of the flour muffins was 132 mL, while that of cereal powders muffins was 117 mL for broun rice muffins, 118 mL for barley muffins, 132 mL for oat muffins and 119 mL for respectively for goami powder muffins. The hardness of the flour muffins, measured by a texture analyzer, was $2.03{\times}10^3\;g/cm^2$, and the other powder muffins were $3.27{\times}10^3\;g/cm^2$ for broun rice muffins, $3.33{\times}10^3\;g/cm^2$ for barley muffins, $2.38{\times}10^3\;g/cm^2$ for oat muffins, and $2.33{\times}10^3\;g/cm^2$ for goami powder muffins respectively. The L-values and moisture contents of goami powder muffins were higher than those of the other muffins. In the sensory evaluation the overall preference was the highest in oat powder muffins.

• 한국세라믹학회지
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• 제38권12호
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• pp.1085-1092
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• 2001

고효율 AC powder EL 소자를 초저가형과 저전력 소모형으로 분류하여 막의 두께와 제조된 유기결합제에 따라 스크린 프린팅법으로 제조하였다. 제조된 소자의 광전기적 특성을 평가하기 위하여 인가 주파수는 400Hz~1kHz, 인가 전압은 50~300 $V_{rms}$까지 변화시켜 휘도 및 전류밀도를 측정하였다. 주파수 및 전압공급원은 정현파 발생 장치로서 frequency generator를 이용하였다. 또한 휘도는 luminometer 의해 측정되었으며 전류밀도 측정을 위하여 multimeter를 사용하였다. 초저가형 AC powder EL 소자의 경우에는 가소제를 첨가하지 않고 발광층의 두께는 45~50$\mu\textrm{m}$이며 유전층의 두께는 약 10$\mu\textrm{m}$에서 43cd/$m^2$ 정도의 휘도와 20$\mu$A/$cm^2$정도의 전류밀도를 얻을 수 있었으며 저전력 소모형 AC powder EL 소자의 경우에는 15wt의 가소제 첨가하에 발광층의 두께는 45~50$\mu$m이며 유전층의 두께는 15~20$\mu$m에서 74cd/ $m^2$정도의 휘도와 30~40$\mu$A/ $m^2$정도의 전류밀도를 얻을 수 있었다. 또한 수명시간에 있어서 본 연구에서 제조한 AC powder EL 소자가 타사 제품보다 절대적으로 우수한 특성을 보였다.다.

• 한국초전도ㆍ저온공학회논문지
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• 제25권3호
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• pp.28-33
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• 2023

Magnetic relaxation properties of pure MgB₂ powder samples and diluted water-treated MgB₂ powder samples were investigated. The magnetic field H-dependence, m(H), and the time t-dependence, m(t), of the magnetic moment m were measured and analyzed using the PPMS-VSM magnetometer equipment, respectively. The m(t) reduction rates of pure MgB₂ powder samples and diluted water-treated MgB₂ powder samples decreased to about 0.7 ~ 1.8% and 0.6 ~ 1.0% for about 7200 s, respectively, at temperature T = 15 K. The magnetic relaxation properties of the two types of MgB₂ powders were analyzed by calculating the magnetic relaxation rate S = -dln(M_irr)/dln(t) values according to Anderson-Kim theory. The magnetic relaxation ratio S values of the two types of MgB₂ powder samples were almost similar. As a result of the quantum creep effect, the constant magnetic relaxation rate S characteristic was confirmed at a temperature range of T = 10 K or less.

• 한국분말재료학회지
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• 제9권5호
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• pp.315-321
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• 2002

Pure tantalum powder has been produced by combining Na as a reducing agent, $K_2TaF_{7}$ as feed material, KCl and KF as a diluent in a stainless steel(SUS) bomb, using the method of metallothermic reduction. The present study investigated the effect of the amount of the diluent and reaction temperature on the characteristics of tantalum powder in the production process. The temperature applied in this study $850^{\circ}C$ and the amount of the additional reductant from +5% of the theoretical amount used for the reduction of the entire $K_2TaF_{7}$. The results showed that as the amount of the diluent increased, the reaction temperature became lower because the diluent prevented a temperature rise. Also, according to the mixture ratio of the feed materials and the diluent changed from 1 : 0.25 to 1 : 2, the particle size decreased from $5\mutextrm{m}$ to $1\mutextrm{m}$ and a particle size distribution which is below 325 mesh in fined powder increases from 71% to 83%. The average size of Tantalum powder, $2-4\mutextrm{m}$, was close to that of the commercial powders($2-5\mutextrm{m}$). Also under this condition, impurities contained in the powder were within the range allowed for the commercial Ta powders.

• 한국분말재료학회지
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• 제1권2호
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• pp.135-144
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• 1994

Silicon carbide powder was prepared from mixtures of Sangdong silica sand and carbon black by SHS (Self propagating High temperature Synthesis) method which utilizes magnesiothermic reduction of silica. In the powder preparation process, the reacted powder was leached by chloric acid to remove the magnesium oxide and was subsequently roasted to remove free carbon. The impurities were mostly eliminated by hot acid treatment. The resultant SiC powder showed the mean particle size of 0.22 ${\mu}{\textrm}{m}$ and the specific surface area of $66.55 m^2/g$. The SiC powder was mixed with 1 wt% of boron and of carbon to increase densification rate. The mixed powder was pressed and sintered pressurelessly at $2100^{\circ}C$ for 30 min in argon gas. The sintered body showed the hardness of $2550 kg{\cdot}f/mm^2$ and the fracture toughness, KIC of $3.47 MN/m^{3/2}$.

• 한국전기전자재료학회논문지
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• 제19권8호
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• pp.737-743
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• 2006

[ $Li[Co_{0.50}Li_{0.17}Mn_{0.33}]O_2$ ] powder was prepared using a simple combustion method. specially, ratio of 2:1, 3:2, 1:1, 2:3, 1:2 was adopted as acetate source/nitrate source. The diffraction pattern of $Li[Co_{0.50}Li_{0.17}Mn_{0.33}]O_2$ powder showed that this compound could be classified as hexagonal $a-NaFeO_2$ structure (space group : $R\bar{3}m$). The size of powder was less than $1{\mu}m$. Small particle size of cathode powder would give a good ionic and electronic conductivity to cathode electrode, which made of cathode powder. As the increase of nitrate source-ratio, discharge capacity of $Li[Co_{0.50}Li_{0.17}Mn_{0.33}]O_2$ at high charge-discharge rate was increased. When the ratio of acetate source/nitrate source was 1:2, discharge capacity at 10 C rate (2000 mA/g) was 180 mAh/g. It was $10{\sim}15%$ larger than that of powder, which have 2:1 as acetate source/nitrate ratio.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 1994년도 추계학술대회강연 및 발표대회 강연및 발표논문 초록집
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• pp.17-17
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• 1994

• 한국분말재료학회지
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• 제5권4호
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• pp.241-249
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• 1998

Sintering kinetics of ball-milled $MoSi_2$ was studied with the addition of Ni. $MoSi_2$ powder with the average particle size of 1 $\mu\textrm{m}$ was obtained from ball-milling of 10 $\mu\textrm{m}$ powder. Small amount of Ni was added to the ball-milled $MoSi_2$ powder by salt solution and reduction method. The powder was compacted into cylindrical shape at 200 MPa and isothermally sintered in a $H_2$ atmosphere at the temperature range of 1100~$1400^{\circ}C$ for 3~600 minutes. The changes of linear shrinkage and sintered density were monitored as a function of sintering time. The microstructure was observed by using optical microscopy and scanning electron microscopy. Phases were identified by X-ray diffratometer and electro-probe micro analysis. Sintering kinetics of Ni-added powder was compared to as-milled powder and the apparent activation energy was calculated from Arrhenius plot.