• Title/Summary/Keyword: Low-Shrinkage

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Warpage of Co-fired High K/Low K LTCC Substrate (고유전율/저유전율 LTCC 동시소성 기판의 휨 현상)

  • Cho, Hyun-Min;Kim, Hyeong-Joon;Lee, Chung-Seok;Bang, Kyu-Seok;Kang, Nam-Kee
    • Journal of the Microelectronics and Packaging Society
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    • v.11 no.3 s.32
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    • pp.77-82
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    • 2004
  • In this paper, warpages of heterogeneous LTCC substrates comprised of high K/low K hi-layered structure were investigated. The effect of glass content in high K LTCC layer on the warpage of substrate during co-firing process was examined. Shrinkage and dielectric properties of high K and low K green sheets were measured. In-situ camber observation by hot stage microscopy showed different camber development of heterogeneous LTCC substrates according to glass content in high K green sheet. High K green sheet containing $50\%$ glass was matched to low K green sheet in the shrinkage. Therefore, LTCC substrate of Low K/High K+$50\%$ glass structure showed flat surface after sintering.

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Preparation and Characteristic of Sheet Molding Compound using Unsaturated Polyester Resin with Low Profile Agent of Polystyrene (저수축제 폴리스틸렌과 불포화 폴리에스터 수지를 사용한 Sheet Molding Compound 제조 및 특성)

  • Bae, Gi Boong;Lee, Sang Goo;Yoon, Hong Jin;Lee, Jong Dae
    • Korean Chemical Engineering Research
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    • v.50 no.3
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    • pp.588-593
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    • 2012
  • Compatibility of unsaturated polyester (UP) and low profile agent (LPA) of polystyrene (PS) have been investigated under various mixing conditions such as the ratio of UP and LPA, mixing time, mixing temperature, and input amount of 2nd UP. It was possible to obtain mixture with small particle size and low phase separation in condition of 35 g of LPA, 25 g of 1st UP input, 5 min of mixing time, 1700 rpm of mixing speed, and 45 g of 2nd UP input. It was found that compatibility of UP and LPA was very sensitive to mixing conditions. In addition, molded sample using sheet molding compound prepared by stable mixing condition appeared good properties such as low water adsorption, low shrinkage, and high gloss.

Properties and Prediction Model for Ultra High Performance Fiber Reinforced Concrete (UHPFRC): (I) Evaluation of Setting and Shrinkage Characteristics and Tensile Behavior (초고성능 섬유보강 콘크리트(UHPFRC)의 재료 특성 및 예측모델: (I) 응결 및 수축 특성과 인장거동 평가)

  • Yoo, Doo-Yeol;Park, Jung-Jun;Kim, Sung-Wook;Yoon, Young-Soo
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.32 no.5A
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    • pp.307-315
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    • 2012
  • Recently, ultra high performance fiber reinforced concrete (UHPFRC) having over 180 MPa compressive strength and 10 MPa tensile strength has been developed in Korea. However, UHPFRC represents different material properties with normal concrete (NC) and conventional high performance concrete (HPC) such as a high early age autogenous shrinkage and a rapid dry on the surface, because it has a low water-binder ratio and high fineness admixtures without coarse aggregate. In this study, therefore, to propose suitable experimental methods and regulations, and to evaluate mechanical properties at a very early age for UHPFRC, setting, shrinkage and tensile tests were performed. From the setting test results, paraffin oil was an appropriate material to prevent drying effect on the surface, because if paraffin oil is applied on the surface, it can efficiently prevent the drying effect and does not disturb or catalyze the hydration of cement. From the ring-test results, it was defined that the shrinkage stress is generated at the time when the graph tendency of temperature and strain of inner steel ring is changed. By comparing with setting test result, the shrinkage stress was firstly occurred as the penetration resistance of 1.5 MPa was obtained, and it was about 0.6 and 2.1 hour faster than those of initial and final sets. So, the starting time of autogenous shrinkage measurement (time-zero) of UHPFRC was determined when the penetration resistance of 1.5 MPa was obtained. Finally, the tensile strength and elastic modulus of UHPFRC were measured from near initial setting time by using a very early age tensile test apparatus, and the prediction models for tensile strength and elastic modulus were proposed.

Autogenous Shrinkage of Very-Early Strength Latex-Modified Concrete with Latex Contents (라텍스함량 변화에 따른 VES-LMC의 자기수축)

  • Park, Won-Il;Choi, Pan-Gil;Yun, Kyong-Ku;Lee, Bong-Hak
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.11 no.3
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    • pp.1059-1065
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    • 2010
  • Very-early strength latex-modified concrete (VES-LMC) was developed for the purpose of fast-track overlay of a concrete bridge deck under heavy traffic, concentrated on the workability, durability, and strength gain so that it can be opened to the traffic only three hours after its placement. The mixture of VES-LMC might accompany very high heat of hydration at early-age because of its inherent rapid hardening property and could have susceptibility to autogenous shrinkage because of its relatively low water-cement ratio. This study evaluated the effect of the latex-cement ratio(L/C) both of the constant and variable slumps on the autogenous shrinkage of VES-LMC by carrying out simple temperature rise test and early-age shrinkage experiment. Test results are as follows: The latex contributes on the enhancement of the concrete durability but has little effect on its hydration and the accompanied heat of hydration in VES-LMC. Autogenous shrinkage increased with the increase in latex-cement ratio at variable slumps and its pattern followed regularly a logarithmic increase. However, the influence of water-cement ratio and latex-cement ratios for the test specimens at constant slump on early-age autogenous shrinkage property was found to be minor due to the simultaneous effect of the two experimental variables.

Correlation between UV-dose and Shrinkage amounts of Post-curing Process for Precise Fabrication of Dental Model using DLP 3D Printer (DLP 공정을 이용한 정밀 치아모델 제작에서 UV 조사량과 후경화 수축률의 상관관계 분석)

  • Shin, Dong-Hun;Park, Young-Min;Park, Sang-Hu
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.17 no.2
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    • pp.47-53
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    • 2018
  • Nowadays, additive manufacturing (AM) technology is a promising process to fabricate complex shaped devices applied in medical and dental services. Among the AM processes, a DLP (digital light processing) type 3D printing process has some advantages, such as high precision, relatively low cost, etc. In this work, we propose a simple method to fabricate precise dental models using a DLP 3D printer. After 3D printing, a part is commonly post-cured using secondary UV-curing equipment for complete polymerization. However, some shrinkage occurs during the post-curing process, so we adaptively control the UV-exposure time on each layer for over- or under-curing to change the local shape-size of a part in the DLP process. From the results, the shrinkage amounts in the post-curing process vary due to the UV-dose in 3D printing. We believe that the proposed method can be utilized to fabricate dental models precisely, even with a change of the 3D CAD model.

Study on the Physical Property of PTT/Tencel/Cotton MVS Blended Yarn for High Emotional Garment (I) - Physical property of blended yarn according to yarn structure - (고감성 PTT/Tencel/Cotton MVS 혼방사 패션소재의 물성에 관한 연구 (I) - 사 구조에 따른 혼방사 물성 -)

  • Kim, Hyun Ah
    • Fashion & Textile Research Journal
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    • v.18 no.1
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    • pp.113-119
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    • 2016
  • The evolution of spinning technology was focused on improving productivity with good quality of yarns. More detail spinning technology according to mixing of various kinds of fibre materials on the air vortex spinning system is required for obtaining good quality yarns. This paper investigated the physical properties of air vortex yarns compared with ring and compact yarns using PTT/tencel/cotton fibres. It was observed that unevenness of air vortex yarns was higher than those of ring and compact yarns, which resulted in low tenacity and breaking strain of air vortex yarns. Initial modulus of air vortex yarns was higher than those of ring and compact yarns. Yarn imperfections of air vortex yarns such as thin, thick and nep were much more than those of ring and compact yarns. These poor yarn qualities of air vortex yarn were attributed to the fasciated yarn structure with parallel fibres in the core part of the air vortex yarn. However, yarn hairiness of air vortex yarns was less and shorter than those of ring and compact yarns. Thermal shrinkage of air vortex yarns were higher than that of ring yarns, which was caused by sensible thermal shrinkage of PTT fibres on the bulky yarn surface and core part of air vortex yarns.

Improvement of precision of three-dimensional ceramic microstructures employing silica nanoparticle-mixed precursor (나노 실리카분말의 충진효과를 이용한 극미세 3차원 세라믹 구조물 정밀화)

  • Lim T.W.;Park S.H.;Yang D.Y.;Pham Tuan Anh;Kim D.P.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2006.05a
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    • pp.157-158
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    • 2006
  • A novel nanofabrication process has been developed using two-photon crosslinking (TPC) for the fabrication of three-dimensional (3D) SiCN ceramic microstructures applicable to high functional 3D devices, which can be used in harsh working environments requiring a high temperature, a resistance to chemical corrosion, as well as tribological properties. After sequential processes: TPC and pyrolysis, 3D ceramic microstructures are obtained. However, large shrinkage due to low-ceramic yield during the pyrolysis is a serious problem to be solved in the precise fabrication of 3D ceramic microstructures. In this work, silica nanoparticles were employed as a filler to reduce the amount of shrinkage. In particular, the ceramic microstructures containing 40 wt% silica nanoparticles exhibited relatively isotropic shrinkage owing to its sliding free from the substrate during pyrolysis.

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A Study on Reducing Deterioration in Long-span Slab Concrete (장스팬 슬라브 콘크리트의 열화저감에 대한 연구)

  • Kim, Dae-Geon;Cha, Hun;Choi, Sang-Hwan;Moon, Kyeong-Sik
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2014.11a
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    • pp.11-12
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    • 2014
  • In this study, fundamental properties of concrete mixed with fiber has been analysed. Compressive strength, tensile strength and plastic shrinkage has been tested to conduct the optimum addition ratio of fiber. Effect to control press concrete's cracking has been tested. The following results could be made as the conclusion. For the flowability, slump decreased about 41-79% when all types of fiber used in the concrete. When the addition ratio of fiber is 1.2%, the slump of concrete decreased about 45%. For the strength properties. all the specimens with different addition ratio of fiber shown higher compressive strength comparing with Plain. Comparing with Plain, cracking decreased when the fiber added. Especially, when NY fiber used in the concrete, the plastic shrinkage did not occurred. In addition, Latex modified concrete(LMC) has improved superior physical and chemical properties. The properties of latex, combined with the low water-cement ratio, produce a concrete that has improved flexural, tensile, and bond strength, lower modulus of elasticity, increased freeze-thaw resistance, and reduced permeability compared to conventional concrete of similar mix design.

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The Physical Properties of Super Bulky Yarn According to Textured Condition (Super Bulky Yarn의 사가공 조건에 따른 물성변화)

  • Park, Myung-Soo
    • Fashion & Textile Research Journal
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    • v.12 no.4
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    • pp.500-507
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    • 2010
  • In this study, physical properties were studied by using latent stretching yarn in order to develop the texturing yarn technique for super bulky yarn, which is better in bulkiness and handle than natural wool and also adds property of synthetic fiber to natural wool. In order to obtain textured conditions by analysing basic properties for manufacturing DTY yarn with super bulky property, DTY 50d/12 after spinning latent yarn spined POY 80d/12 was obtained under the two conditions of (i) false twist(T/M) level 3 in DTY texturing and (ii) draw ratio level 4 in draw texturing. For DTY texturing yarn, Elongation rate increased as the heat treatment time and temperatures increased. In addition, shrinkage became higher as false twist was higher, so that elongation rate became lower. When annealing became longer in time and higher in temperature, initial modulus increased. In addition, as the count of false twist increased, the initial modulus showed higher values. For draw texturing yarn, under the conditions of heat temperature 180 and heating time 30 minutes, shrinkage rate in draw ratio 1.55 and 1.6 draw ratio was 7%, and that in 1.65 and 1.7 draw ratio was 8.5%. High draw ratio samples' tenacity was much influenced by heating time and temperature, but low draw ratio samples' tenacity was influenced not by treated time, but by treated temperature.

Low Temperature Sintering Mg-Zn Ferrites (Mg-Zn Ferrites의 저온소결화)

  • Kwon Oh-Heung
    • Resources Recycling
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    • v.12 no.6
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    • pp.8-12
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    • 2003
  • According to the recent trend to raise the horizontal scan frequency to increase the image refinement of the High Definition TV and High Resolution Display, material with low core loss is required for the ferrite core for deflection yoke, which is secured even in the high frequency range. liking notice of the influence on the fine structure of Mg-Zn ferrite by the chemical com position and process, low temperature sintering was proceeded. Cu was added to the low loss Mg-Zn system ferrite. After select-ing MgO, ZnO, $Fe_2$$O_3$, CuO, MgO was substituted for CuO while varying the composition ratio. Then the sample was sintered for 3 hours between $980~1350^{\circ}C$ Magnetic permeability, power consumption, shrinkage rate, core loss were measured. The start-ing temperature to test the shrinkage of the sample was nearby $900^{\circ}C$, it increased according to the substitution process of Cu, and the firing temperature was lowered about $-50~-75^{\circ}C$ alongside of the process.