• Title/Summary/Keyword: Lead cross sections

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THE MICROSTRUCTURE OF Pb-DOPED SOLIDIFIED WASTE FORMS USING PORTLAND CEMENT AND CALCITE

  • Yoo, Hee-Chan;Lee, Dong-Jin
    • Environmental Engineering Research
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    • v.11 no.1
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    • pp.54-61
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    • 2006
  • An electron probe microanalysis (EPMA) investigation can provide quantitative and qualitative insight into the nature of the surface and bulk chemistry on solidified waste forms(SWF). The proportion of Pb in grain areas is below 0.3 wt. %, and the proportion near the border of the grain slightly increases to 0.98 wt. % but in the inter-particle areas farther from the grain, the concentration of Pb markedly increases. It is apparent that very little Pb diffuses into the tricalcium silicate($C_3S$) particles and most of the Pb exists as precipitates of sulfate, hydroxide, and carbonate in the cavity areas between $C_3S$ grains. Calcite additions on Pb-doped SWF are also observed to induce deeper incorporation of lead into the cement grains with EPMA line-analysis of cross-sections of cement grains. The line-analysis reveals the presence of $0.2{\sim}5$ weight % Pb over $5\;{\mu}m$ from cement grain boundaries. In the inter-particle areas, the ratio of Ca, Si, Al and S to Pb is relatively similar even at some distance from the grain border and the Pb (wt. %) ratio is reasonably constant throughout the whole inter-particles area. It is apparent that the enhanced development of C-S-H on addition of calcite can increasingly absorbs lead species within the silica matrix.

Inelastic lateral-distortional buckling of continuously restrained rolled I-beams

  • Lee, Dong-Sik;Bradford, Mark A.
    • Steel and Composite Structures
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    • v.2 no.4
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    • pp.297-314
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    • 2002
  • An energy method of analysis is presented which can be used to study the inelastic lateral-distortional buckling of hot-rolled I-sections continuously restrained at the level of the tension flange. The numerical modelling leads to the incremental and iterative solution of a fourth-order eigenproblem, with very rapid solutions being obtainable, so as to enable a study of the factors that influence the strength of continuously restained I-beams to be made. Although hot-rolled I-sections generally have stocky webs and are not susceptible to reductions in their overall buckling loads as a result of cross-sectional distortion, the effect of elastic restraints, particularly against twist rotation, can lead to buckling modes in which the effect of distortion is quite severe. While the phenomenon has been studied previously for elastic lateral-distortional buckling, it is extended in this paper to include the constitutive relationship characteristics of mild steel, and incorporates both the so-called 'polynomial' and 'simplified' models of residual stresses. The method is validated against inelastic lateral-torsional buckling solutions reported in previous studies, and is applied to illustrate some inelastic buckling problems. It is noted that over a certain range of member slenderness the provisions of the Australian AS4100 steel standard are unconservative.

Measurement of the Energy-Dependent Neutron Capture Cross Section of $^{99}Tc$ by Using the Neutron TOF Method (-중성자 TOF법에 의한 $^{99}Tc$의 에너지의존 중성자 포획단면적측정-)

  • Yoon Jung-Ran;Lee Sang-Bock;Lee Jun-Haeng;Lee Sam-Yol
    • The Journal of the Korea Contents Association
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    • v.5 no.5
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    • pp.133-139
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    • 2005
  • The neutron capture cross section of $^{99}Tc$ has been measured relative to the $^{10}B(n,\gamma)$ standard cross section by the neutron time-of-flight(TOF) method in the energy range of 0.007 eV to 47 keV using a 46-MeV electron linear accelerator(linac) at the Research Reactor. Institute, Kyoto University(KURRI). In order to experimentally prove the result obtained, the supplementary cross section measurement has been made from 0.3 eV to 1 keV using the Kyoto University Lead stowing-down spectrometer (KULS) coupling to the linac. The relative measurement by the TOF method has been normalized to the reference value(20.01 b) at 0.0253 eV and the KULS measurement to that by the TOF method. The existing experimental data and the evaluated capture cross sections in ENDF/B-VI, JENDL-3.2, and JEF-2.2 have been compared with the current measurements by the linac TOF and the KULS experiments.

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Fast Neutron Dosimetry with Two Threshold Detectors in Criticality Accidents of Nuclear Reactors

  • Ro, Seung-Gy
    • Nuclear Engineering and Technology
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    • v.2 no.2
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    • pp.85-95
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    • 1970
  • An attempt has been made to do interpretation of the fast neutron dose with two threshold detectors incorporated with the Harwell criticality locket. This method is based on the assumption that the spectral distribution of fission neutrons in criticality accidents may be governed by one spectral parameter. The surface-absorbed dose for a unit fission neutron fluence seems to be insensitive to spectral shifts of the fission neutron spectrum. The average cross-sections for the activation detectors, however, are considerably changed with the neutron spectral shape, which may lead to a large error in calculating the dose from the reaction rate if one uses a fixed value for the average cross sections regardless of the neutron spectral distribution. Besides, the doses calculated from three representative formulae for fission neutron spectra have been compared : these formulae are Watt, Cranberg at al. and Maxwellian forms. The results obtained front the Maxwellian formula show a departure from the Watt and Cranberg's, both being similarly close.

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Buckling analysis of complex structures with refined model built of frame and shell finite elements

  • Hajdo, Emina;Ibrahimbegovic, Adnan;Dolarevic, Samir
    • Coupled systems mechanics
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    • v.9 no.1
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    • pp.29-46
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    • 2020
  • In this paper we deal with stability problems of any complex structure that can be modeled by beam and shell finite elements. We use for illustration the steel plate girders, which are used in bridge construction, and in industrial halls or building construction. Long spans, slender cross sections exposed to heavy loads, are all critical design points engineers must take into account. Knowing the critical load that will cause lateral torsional buckling of the girder, or load that can lead to web buckling, as an important scenario to consider in a design process.Many of such problem, including lateral torsional buckling with influence of lateral supports and their spacing on critical load can be solved by the proposed method. An illustrative study of web buckling also includes effects of position and spacing of transverse and longitudinal web stiffeners, where stiffeners can be modelled optionally using shell or frame elements.

An Electron Microscopy of Spermiogenesis in the Dragonfly, Crocothemis servilia Drury (고추잠자리의 精子完成의 電子顯微鏡的 硏究)

  • Paik, Kyong Ki;Choi, Choon Keun;Lee, Kuk Bum
    • The Korean Journal of Zoology
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    • v.15 no.3
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    • pp.133-147
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    • 1972
  • Ultrastructures of spermiogeneis in other invertebrates were investigated by several workes (Anderson, et al., 1967; Bloch, et al., 1964; Christen, 1961; Gatenby, et al., 1959; Paik, et al., 1968; Silveira, 1964; Yasuzumi, 1957) but spermiogenesis of dragonfly has not been reported previously. Testes and vass deferentia of the Korean dragonfly, Crocothemis servilia, were used for electron microscopic study of spermiogenesis. Materials were prefixed for 1-2 hours at $3^{\circ}C$ in 1.25% glutaraldehyde buffered to pH 7.2 with 0.2M sodium cacodylate buffer. Fixed tissue was washed twice in 0.2M cacodylate buffer and was subsequently postfixed for 2 hours at $3^{\circ}C$ in 1% osmium tetroxide buffered to pH 7.2 with 0.4M sodium cacodylate buffer solution. Specimens were dehydrated in graded ethyl alcohol, and finally embedded in epoxy Epon resin. Thin sections prepared from all the blocks were doubly stained; first in uranyl acetate and then in lead citrate. All thin sectios were examined with a Hitachi HS-7S electron microscope. The results of this study were summarized as follows. 1. Along the condensation of chromatin in nucleus, the shpae of nucleus was changed from spherical shpae to ellipse and cone cell type. 2. During the elongation of nucleus and the migration of cytoplasm, the nucleus removed to the one side of spermatid and began to invaginate from the posterior portion of nucleus. 3. There are ring centrioles in invaginated portion and axial filaments derived from centriole extend to the tail through the tailward half of spermatid. 4. In the cross sections the axial filament consisted of a central sheath, a central fibril, and 9 peripheral doublets.

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An Ultrastructural Study of Tentacular Retractor Muscle of Chinese Mystery Snail, Cipangopaludina chinensis malleata Reeve (논우렁이 촉수(觸手) 수축근(收縮筋)의 미세구조(微細構造))

  • Song, Yong-Jik;Kim, Woo-Kap;Kim, Chang-Whan
    • Applied Microscopy
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    • v.17 no.2
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    • pp.31-40
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    • 1987
  • The tentacular retractor muscle has many arrays of muscle fiber bundles under the epithelial layer. Most of muscle fiber bundles are arranged in parallel to the longitudinal axes of muscle fibers and a small number of them perpendiculary to them. These smooth muscle cells are filled with compactly arranged myosins and actins. These microfilaments, when the tentacle is protracted, keep abreast with straight for-ward-lined shapes while these microfilaments, when it is retracted, with curved shapes. The foldings in the sarcolemma of the muscle cell, when the tentacle is retracted, lead to the formation of normal subsurface tubules along with which a few mitochondria are included. It is thought that the formation of the sarcolemmal differentiation like the subsurface tubules has a close relation with the protraction and retraction of the tentacle. Mitochondria are found throughout the muscle cell, and sarcoplasmic reticulum (SR) developed greatly in the exoplasm close to the sarcolemma and associated with the cell membrane. Dense bodies are distributed irregularly and thin filaments are scattered around the thick filament in cross-sections, but the thin filaments may be arranged in complete or partial orbits around thick filaments. Complete orbits are infrequent.

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Chlorine effect on ion migration for PCBs under temperature-humidity bias test (고온고습 전원인가 시험에서 Cl에 의한 이온 마이그레이션 불량)

  • Huh, Seok-Hwan;Shin, An-Seob
    • Journal of Welding and Joining
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    • v.33 no.3
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    • pp.47-53
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    • 2015
  • By the trends of electronic package to be more integrative, the fine Cu trace pitch of organic PCB is required to be a robust design. In this study, the short circuit failure mechanism of PCB with a Cl element under the Temperature humidity bias test ($85^{\circ}C$/85%RH/3.5V) was examined by micro-structural study. A focused ion beam (FIB) and an electron probe micro analysis (EPMA) were used to polish the cross sections to reveal details of the microstructure of the failure mode. It is found that $CuCl_x$ were formed and grown on Cu trace during the $170^{\circ}C$/3hrs and that $CuCl_x$ was decomposed into Cu dendrite and $Cl_2$ gas during the $85^{\circ}C$/85%RH/3.5V. It is suggested that Cu dendrites formed on Cu trace lead to a short circuit failure between a pair of Cu traces.

Flow Dynamics Near End-To-End Anastomoses - Part I. In Vitro Compliance Measurement -

  • Kim, Y.H
    • Journal of Biomedical Engineering Research
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    • v.13 no.2
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    • pp.165-174
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    • 1992
  • Compliance mismatch across an end-to-end anastomosis was measured In the In vitro experimental setup. A 35mm camera was used and Image process was done in Gould/ DeAnza Image processor. The results showed that compliances of Penrose tubing and synthetic PTFE grafts were In good agreement with the previously reported In vivo data. PTFE grafts exhibited a nonlinear behavior with compliance decreasing with Increasing transmural pressure, whereas the compliance of the Penrose tubing remained relatively constant within the range of the pressures in which data were obtained. The lumen cross sections at the anastomosis were affected by the suture and the mismatch In compliance between the Penrose tubing and vascular grafts. The varla~lons In the lumen dtameter at the anastomosis was more pronounced with increasing transmural pressures. From the present study, it was clearly demonstrated that the compliance of prosthetic grafts Is much lower than that of the arteries. In addition to the hemodynamlc consequences, compliance mismatch across the anastomosis has been known to lead to Increased anastomotlc and suture stresses with resultant suture line dehlscence and false aneurysm formation. Thus, there are good hemodynamic reasons to suppose that Introduction of a less compliant arterial graft Into the arterial circulation wlll be damaging and that grafts should be made to match the elastic behavior of their host arteries as closely possible.

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An optimization framework for curvilinearly stiffened composite pressure vessels and pipes

  • Singh, Karanpreet;Zhao, Wei;Kapania, Rakesh K.
    • Advances in Computational Design
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    • v.6 no.1
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    • pp.15-30
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    • 2021
  • With improvement in innovative manufacturing technologies, it became possible to fabricate any complex shaped structural design for practical applications. This allows for the fabrication of curvilinearly stiffened pressure vessels and pipes. Compared to straight stiffeners, curvilinear stiffeners have shown to have better structural performance and weight savings under certain loading conditions. In this paper, an optimization framework for designing curvilinearly stiffened composite pressure vessels and pipes is presented. NURBS are utilized to define curvilinear stiffeners over the surface of the pipe. An integrated tool using Python, Rhinoceros 3D, MSC.PATRAN and MSC.NASTRAN is implemented for performing the optimization. Rhinoceros 3D is used for creating the geometry, which later is exported to MSC.PATRAN for finite element model generation. Finally, MSC.NASTRAN is used for structural analysis. A Bi-Level Programming (BLP) optimization technique, consisting of Particle Swarm Optimization (PSO) and Gradient-Based Optimization (GBO), is used to find optimal locations of stiffeners, geometric dimensions for stiffener cross-sections and layer thickness for the composite skin. A cylindrical pipe stiffened by orthogonal and curvilinear stiffeners under torsional and bending load cases is studied. It is seen that curvilinear stiffeners can lead to a potential 10.8% weight saving in the structure as compared to the case of using straight stiffeners.