• 대한전기학회:학술대회논문집
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• 대한전기학회 2005년도 제36회 하계학술대회 논문집 전기설비
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• pp.76-78
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• 2005

Moisture contents measurement is frequently used as one of parameters for degradation diagnosis of transformer insulation. In general Karl-Fisher method is mainly used for moisture contents till now. But this method is inconvenient because of dismounting transformer for sampling oil or paper, and also partial sampling. At latest Recovery Voltage Method(RVM) is noticed for complement of this method. RVM can directly estimate moisture contents of transformer insulations in field without dismounting transformer. In this paper the accelerated aging process of oil-paper samples have been investigated at a temperature up to 140$^{\circ}C$ for 500 hours. The oil-paper insulation samples have been measured at intervals of 100 hours. Next to, we have estimated moisture contents using both Karl-Fisher Titration Method and RVM. And we have compared with Karl-Fisher Titration Method and RVM for estimating moisture contents. At last we have verified reliability of RVM which is new measurement method.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2005년도 제36회 하계학술대회 논문집 C
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• pp.1912-1914
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• 2005

The electrical, chemical and mechanical characteristics in transformer insulations are changed due to thermal stress. It is known that characteristics of transformer insulations is deteriorated such as decrease of dielectric strength, deterioration of dielectric constant and tensile strength of paper as transformer oil and paper are aged by thermal stress. Furthermore, chemical characteristics of them are deteriorated as like increment of moisture contents and dissolved by-products in oil, etc. In this paper we have been investigated chemical characteristics of transformer by accelerated thermal aging. For this working we have made experimental test cell and aged at a temperature up to $140^{\circ}C$ for 500 hours. The oil-paper insulation samples have been measured at intervals of 100 hours. For analysis we used Karl-Fisher titration method and high performance liquid chromatography (HPLC).

• 한국응용과학기술학회지
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• 제25권4호
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• pp.503-510
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• 2008

This research is related to the process of refining the raw material, industrial 2-propanone to the 2-propanone of the electronic grade. With this view, the high purity of 2-propanone was obtained through the complex preprocessing(physical adsorption method), distillation process and membrane-filtration of distillate. Impurities were identified by GC and UV, and then we assayed the water content in 2-propanone passing adsorption step made of activated carbon and Zeolite 4A. Furthermore, the distillation was performed with the packed column distillation apparatus to eliminate impurities such as acetaldehyde. Particulates were removed by reduced-pressure filtration through $0.5{\mu}m$ membrane filter and the number of the particulates was measured by particulate counter to confirm the removal of impure particles.