• Proceedings of the KWS Conference
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• 2002.10a
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• pp.522-527
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• 2002

The microstructure and mechanical properties of friction stir welded OFC plates with 2mm in thickness were examined with the changing welding parameters such as welding speed, rotation speed in this study. The sounding welding conditions was acquired at the optimum welding conditions of the 41mm/min to 61mm/min of welding speed at 1250 rpm of rotation speed. The microstructure of weld zone was divided into four parts such as the base metal region (EM), thermal mechanical affected zone (TMAZ), heat affected zone (HAZ), stir zone (SZ). The grain size in the SZ and the width of weld nugget were increased with increasing welding speed. The hardness profiles of the base metal were distributed about 80HV. The HAZ is a slightly softened region of about 60~75 HV relative to the base metal. The hardness profiles of the SZ were higher than that of base metal. The tensile strength was increased with increasing welding speed. In case increasing rotation speed, tensile strength was decreased. The maximum tensile strength was about 220:MPa which was 110% of joint efficience of that of base metal at 41mm/min of welding speed, 1250rpm of rotation speed.

• Journal of the Korean Ceramic Society
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• v.56 no.4
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• pp.394-398
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• 2019

In this paper, the joining characteristics of GDC-LSM ceramics with Crofer 22 APU metal alloys was investigated at different brazing temperatures and holding times by reactive air brazing. Brazing was performed using Ag-10 wt% CuO filler, at three different temperatures (1000, 1050, and 1100℃ for 30 minutes) as well as for three different holding times (10, 30, and 60 minutes at 1050℃). The interfacial microstructures were examined by scanning electron microscopy and the joining strengths were assessed by measuring shear strengths at room temperature. The results show that with increasing brazing temperature and holding time, joint microstructure changed obviously and shear strength was decreased. Shear strength varied from a maximum of 100±6 MPa to a minimum of 18±5 MPa, depending on the brazing conditions. These changes were attributed to an increase in the thickness of the oxide layer at the filler/metal alloy interface.

• Journal of the Korean Society for Heat Treatment
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• v.6 no.1
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• pp.9-16
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• 1993

To investigate the properties of diffusion bonding of 7050 Al alloy, the diffusion bonding joints have been produced in self-made diffusion bonding hot-press which admits a defined application of the bonding pressure during the heating phase and also rapid cooling after the bonding process with various bonding condition. The strength of the bond increases with increasing the bonding time and temperature. Shear test at toom temperature showed that high strength up to 70% that of parent metal (320 MPa), 220 MPa for the specimen bonded 14 hr at $560^{\circ}C$, with 3 MPa. In this case, however, there is large deformation more than 20% reduction in thickness. The results were correlated with joint characteristics found by optical microstructure and by fractography by SEM. When the strengths of the bonds are more than 50% that of parent metal, a great deal of dimples stretched along the direction of shear stress are observed over the fractured surface of the bond. On the microstructure of the bond line, initial mophology of the bond line disapeared for the grain boundary migration with increasing the bonding time.

• Journal of Welding and Joining
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• v.35 no.3
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• pp.44-51
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• 2017

In the present study, AA 5083-O plates are joined by friction stir welding technique. A universal milling machine was used to perform the welding process of the work-pieces which were fixed on the proper position by a vice. The joints were friction stir welded by two tools with different pin profiles; cylindrical threaded pin and tapered smooth one at different rotational speed values; 400 rpm and 630 rpm, and different welding speed values; 100 mm/min and 160 mm/min. During FSW of each joint, the temperature was measured by infra-red thermal image camera. The welded joints were inspected by visually as well as by the macro- and microstructure evolutions. Furthermore, the joints were tested for measuring the hardness and the tensile strength to study the effect of changing the FSW parameters on the mechanical properties. The results show that increasing the rotational speed results in increasing the peak temperature, while increasing the welding speed results in decreasing the peak temperature for the same tool pin profile. Defect free welds were obtained at lower rotational speed by the threaded tool profile. Moreover, the threaded tool pin profile gives superior mechanical properties at lower rotational speed.

• Nuclear Engineering and Technology
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• v.56 no.6
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• pp.2367-2374
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• 2024

In this paper, based on the need for high-strength connections between all-tungsten-oriented plasma materials and thermal sinking materials of copper and its alloys in nuclear fusion devices, a study on the effect of tungsten surface laser micro structuring on the interfacial bonding properties of W/Cu joints was carried out. In the experiment, the connectors were prepared by vacuum fusion infiltration technology, and the effects of microgroove structure on the mechanical and thermal conductivity of W/Cu connectors were investigated under different parameters (including microgroove pitch, microgroove depth, and microgroove taper). The maximum shear strength is 126.0 MPa when the pitch is 0.15 mm and the depth is 34 ㎛. In addition, the negative taper structure, i.e., the width of the entrance of the microstructure is smaller than the width of the interior of the microstructure, is also investigated. The shear tests show that there is an approximately linear relationship between the shear strength of W/Cu and taper. Compared with the positive taper, the shear strength of the samples with the same morphological density and depth of the tungsten surface is significantly higher.

• Journal of the Korean Ceramic Society
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• v.39 no.10
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• pp.955-962
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• 2002

The microstructure change of brazed $Si_3N_4$/Stainless steel 316 joint with Cu buffer layer were examined to clarify the effects of brazing process conditions such as brazing time and temperature on the mechanical properties and reliability of brazed joints. For the brazed joint above 900${\circ}C$, the Cu buffer layer was completely dissolved into brazing alloy and the thickness of reaction product formed at $Si_3N_4$/brazing alloy joint interface was abruptly increased, which could increase the amounts of residual stress developed in the joint. The fracture strength of brazed $Si_3N_4$/Stainless steel 316 joint with Cu buffer layer at 950${\circ}C$ was much reduced comparing to those of joints brazed at the lower temperature. But, it was found that the effects of brazing time was not critical on the mechanical properties as well as the reliability of $Si_3N_4$/Stainless steel 316 joint with Cu buffer layer brazed at the temperature below 900${\circ}C$.

• Journal of Welding and Joining
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• v.4 no.2
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• pp.21-29
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• 1986

The influence of welding heat input variation(600-900J/cm) and heat-treatment condition after welding on tensile strength of butt welded joint in $175Kg/mm^2$ strength level Maraging steel(Co-free and Co-containing) sheets was investigated on the basis of hardness distribution, microstructure of weld metal and fracture surface. The obtained main results are as follows; 1. The strength of weldment (UTS, NTS), joint efficiency showed a little decreasing tendency with the increase in welding heat input, and the elongation showed a little increasing tendency with the increase in the width of weld metal. It was considered because of the plastic constraint of the high strength base metal. 2. The strength of weldment was better in the solution treatment and aging than the aging only after welding due to the disappearance of almost denverite in weld metal. 3. The hardness distribution in weldment after welding and heat-treatment was almost similar to both Co containing and Co free Maraging steel with change in welding heat input. 4. The fracture was occurred at weld metal, and the fracture surface showed a relatively shallow dimples in both Co containing and Co free Maraging steel.

• Journal of Welding and Joining
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• v.21 no.7
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• pp.59-64
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• 2003

Microstructure and shear strength of Sn-Zn lead-free solders and Au/Ni/Cu UBM joint under thermal aging conditions was investigated. The samples were aged isothermally at 10$0^{\circ}C$ and 15$0^{\circ}C$ for 300, 600, and 900 hours. The IMCs(Intermetallic Compound) at the interface between solder and UBM were examined by FESEM and TEM. The results showed that the shear strength was decreased with aging time and temperature. The solder ball with high activated RA flux had about 8.2% higher shear strength than that of RMA flux. Poor wetting and many voids were observed in the fractured solder joint with of RMA flux. The decreased shear strengths were caused by IMC growth and Zn grain coarsening. Zn reacted with Au and then was transformed to the $\beta$ -AuZn compound. Although AuZn grew first, $r-Ni_5Zn_{21}$ compounds were formed with aging time. The layers indicated by $Ni_5Zn_{21}(1)$, (2), and (3) were formed with the thickness of ∼0.7 ${\mu}{\textrm}{m}$, ∼4 ${\mu}{\textrm}{m}$, and ∼2 ${\mu}{\textrm}{m}$, respectively.

• Proceedings of the KWS Conference
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• 2002.10a
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• pp.516-521
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• 2002

A study was carried out to grow an understanding of the microstructural development of friction stir welds on an AZ91D magnesium alloy, and to evaluate the mechanical properties of the welds. AZ91D plates with the thickness of 4mm were used, and the microstructural development of the weld zone was investigated using optical and scanning electron microscopes. Square butt welding joint with good quality was obtained at the conditions of under 187mm/min of travel speed with 1100 to 1250 rpm of tool rotation speed. The microstructure within the weld region consisted of fine equiaxed grains with no evidence of the original dendritic structure. The hardness tests showed slightly increased harness in the weld region, and the minimum hardness measured is in that of the parent material. Tensile strength of the weld zone was remarkably improved due to very fine recrystallized structure. XRD pattern of weld zone revealed the removal of $\beta$ intermetallic compounds, $Mg_{17}$Al$_{12}$, which had been distributed in the base metal.l.

• Journal of Ocean Engineering and Technology
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• v.7 no.2
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• pp.121-130
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• 1993

A study off riction welding of high speed steel(SKH 51) bar for blade side to carbon steel(STC 3)bar for shank side was carried out experimentally through tensile test, hardness test, microstructure, and acoustic emission (AE) test. So, this paper deals with optimizing the welding conditions and the real-time quality (strength) evaluation of friction weleded joints by acoustic emission technique. The results obtained are summarized as follows: (1) For friction welded joints of SKH 51to STC 3 steel bars, the total upset (U) increases linearly with an increase of heating time (t sub(1)). (2) The determined optimum welding conditions are heating time (t sub(1)) 7-9 sec, upsetting time (t sub(2)) 5 sec, heating pressure(P sub(1)) 12 kg sub(f)mm supper(2), upsetting pressure (P sub(2)) 15 kg sub(f) mm supper(2) and rotating speed (n) 2, 000 rpm, resulting in a computed relationship between the tensile strength of the joint .sigma. (kg sub(f) mm supper(2)) and the heating time t sub(1) (sec) as the following. sigma.=2.39t sub(1)