• Journal of the Korean Society of Safety
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• v.31 no.6
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• pp.6-11
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• 2016

CFRP composite laminates are widely used as structural materials for airplanes, automobile and aerospace vehicles because of their high strength and stiffness. This study aims to examine an effect of curvature on the penetration fracture characteristic of an orthotropic composite laminated shell. For the purpose, we manufactured orthotropic CFRP shell specimen with different curvatures, and conducted a penetration test using an air-gun. Those specimens were prepared to varied curvature radius(${\infty}$, 200mm, 150mm and 100mm)and were stacked to $[O^{\circ}{_3}/90^{\circ}{_3}]_s$. When the specimen is subjected to transverse impact by a steel sphere(${\Phi}10$), the velocity of steel sphere was measured both before and after impact by determining the time for it to pass two ball-screen sensors located a known distance apart. As the curvature increases, the absorption energy and the critical penetration energy increased linearly because the resistance to the bending moment. Patterns of cracks caused by the penetration of CFRP laminated shells included fiber breakage, lamina fracture, matrix crack interlaminar crack and intralaminar crack.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2003.10a
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• pp.3-6
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• 2003

In this work, poly(ethylene oxide) nanofibers were fabricated by electrospinning to prepare nanofibers-reinforced composites. And the PEO powders-impregnated composites were also prepared to compare with physicochemical properties of nanofibers-reinforced composites. Morphology and fiber diameter of PEO nanofibers were determined by SEM observation. Mechanical interfacial properties of the composites were investigated in fracture toughness tests and interlaminar shear strength (ILSS) test. As a result, the fiber diameter decreased in increasing applied voltage. However the optimum condition for the fiber formation was 15 ㎸, resulting from increasing of jet instability at high voltage and the prepared PEO nanofibers were useful in fiber reinforced composites. The PEO-based nanofibers-reinforced composites showed an improvement of fracture toughness factors ($K_{IC} and G_{ IC}$) and ILSS, compared to the composites impregnated with PEO powders. These results were noted that the nanofibers had higher specific surface area and larger aspect ratio than those of the powder, which played an important role in improving the mechanical interfacial properties of the composites.

• Carbon letters
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• v.9 no.1
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• pp.28-34
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• 2008

Multidirectional reinforcement is aimed primarily at overcoming interlaminar weakness, hence a major interest lies in the mechanical properties of multidirectional carbon/carbon composites. Mechanical properties depend on the type of carbon fiber, the size of the fiber bundle, the spacing of the bundles, the angles of the bundles relative to the axes of the block, and matrix formation. In the present studies, PAN based carbon fiber preforms manufactured different size of unit cell have been prepared. Densification of these used high pressure infiltration and carbonization technique with coal tar pitch as matrix precursor was carried out. Scanning electron microscopy has been used to study the fracture behavior of composites. The size of unit cell of the preforms has considerably affected on the flexural properties as well as microstructure of the carbon/carbon composites.

• Journal of the Korean Society of Fisheries and Ocean Technology
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• v.31 no.3
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• pp.272-278
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• 1995

In this paper to investigate mode I and mode II critical energy release rates, G sub(IC) and G sub(IIC), three prepregs which are domestic products are used. Those are used for the unidirectional composites, but only one is used for the cross-ply laminate composites which is molded [0/90] sub(6s), [0/45] sub(6s) and [0/45/90] sub(6s). The value of G sub(IC) is almost same when modified three calculating methods are applied. The highest value of G sub(IC) at crack initiation is obtained at the [0/90] sub(6s) interlaminar and the lowest one is at the [0/45/90] sub(6s) interlaminar.

• Composites Research
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• v.12 no.5
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• pp.40-53
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• 1999

The interlaminar facture behavior of multidirectional carbon-fiber/epoxy composite laminates under low and high rates of test, up to rate of about 11.4m/s has been investigated using the double cantilever beam specimens. The mode I loasing with rates above 1.0m/s had considerable dynamic effects on the load-time curves and thus revealed higher values of the average crack velocity than thet expected from a simple proportional relationship with the test rate. The modified beam analysis utilizing only the opening displacement and crack length exhibited an effective means for evaluating the dynamic fracture energy $G_{IC}$. Flexural modulus increased gradually with an increase of the test rate, which was utilized in the evaluation of $G_{IC}$. Values of $G_{IC}$ at the crack initiation and arrest were scarcely changed with increasing test rate up to 1.0m/s. However the maximum $G_{IC}$ was much enlarged at 11.4m/s due to the large amount of fiber bridging the crack tip. The larger the initial crack length, the smaller the maximum $G_{IC}$ at high rate.

• Journal of the Korean Society for Precision Engineering
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• v.22 no.2
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• pp.164-171
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• 2005

This study aims to examine an effect of stacking sequence and curvature on the penetration characteristic of a composite laminated shell. For the purpose, we manufactured specimens with different stacking sequences and curvatures, and conducted a penetration test using an air-gun. To examine an influence according to stacking sequence, as flat plate and curvature specimen had more plies, their critical penetration energy was higher, Critical penetration energies of specimen A and C with less interfaces somewhat higher than those of B and D with more interfaces. The reason that with less interfaces, critical penetration energy was higher is pre-impact bending stiffness of composite laminated shell with less interfaces was lower than that of laminated shell with more interfaces, but bending stiffness after impact was higher. And it is because interface, the weakest part of the composite laminated shell, was influenced by transverse impact. As curvature increases, critical penetration energy increases linearly. It is because as curvature increases, resistance to in-plane deformation as well as bending deformation increases, which need higher critical penetration energy. Patterns of cracks caused by penetration of composite laminated shells include interlaminar crack, intralaminar crack, and laminar fracture. A 0$^{\circ}$ply laminar had a matrix crack, a 90$^{\circ}$ply laminar had intralaminar crack and laminar fracture, and interface between 0$^{\circ}$and 90$^{\circ}$laminar had a interlaminar crack. We examined crack length and delamination area through a penetration test. For the specimen A and C with 2 interface, the longest circumferential direction crack length and largest delamination area were observed on the first interface from the impact point. For the specimen B and D with 4 interface, the longest crack length and largest delamination area were observed on the third interface from the impact point.

• Polymer(Korea)
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• v.24 no.3
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• pp.326-332
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• 2000

The effects of sizing agent on the final mechanical properties of the glass fiber/unsaturated polyester composites were investigated by contact angle measurements at room temperature. In this work, glass fibers were coated by poly(vinyl alcohol), polyester, and epoxy type sizing agent and each property was compared. Contact angles of the sized glass fiber were measured by the wicking method based on Washburn equation using deionized water and diiodomethane as testing liquids. As an experimental result, the surface free energy calculated from contact angle showed the highest value in case of the glass fiber coated by epoxy sizing agent. From measurements of interlaminar shear strength (ILSS) and fracture toughness ( $K_{IC}$ ) of the composites, it was found that the sizing treatment on fibers could improve the fiber/matrix interfacial adhesion, resulting in growing the final mechanical properties. This was due to the enhanced surface free energy of glass fibers in a composite system.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2001.05a
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• pp.89-92
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• 2001

Drop weight impact tests were performed to investigate the impact behavior of carbon fiber/epoxy composite laminates reinforced by short fibers and other interleaving materials. Characterization techniques, such as cross-sectional fractography and scanning acoustic microscopy, were employed quantitatively to assess the internal damage of some composite laminates. Scanning electron microscopy was used to observe impact damage and fracture modes on specimen fracture surfaces. The results show that composite laminates experience various types of fracture; delamination, intra-ply cracking, matrix cracking and fiber breakage depending on the interlayer materials. Among the composite laminates tested in this study, the composites reinforced by Zylon fibers showed very good impact damage resistance with medium level of damage, while the composites interleaved by poly(ethylene-co-acrylic acid) (PEEA) film is expected to deteriorate the bulk strength due to the reduction of fiber volume fraction, even though the damaged area is significantly reduced.

• Polymer(Korea)
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• v.38 no.6
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• pp.726-734
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• 2014

Three different types of additives, thiokol, epoxidized natural rubber (ENR) and epoxidized linseed oil (ELO), were dispersed in an epoxy matrix before being used in glass fiber (GF) composites, and their effects on the mechanical and dielectric properties of epoxy resin and glass fiber reinforced epoxy composites (GF/EP) were examined. The addition of each of 7 phr ENR, 9 phr ELO and 5 phr thiokol into the epoxy resin increased the fracture toughness significantly by 56.9, 43.1, and 80.0%, respectively, compared to the unmodified resin. The mode I interlaminar fracture toughness of the GF/EP at propagation was also improved by 26.9, 18.3 and 32.7% when each of 7 phr ENR, 9 phr ELO, and 5 phr thiokol, respectively, was dispersed in the epoxy matrix. Scanning electron microscopy showed that the additives reduced crack growth in the GF/EP, whereas their dielectric measurements showed that all these additives had no additional effect on the real permittivity and loss factor of the GF/EP.

• Composites Research
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• v.32 no.6
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• pp.327-334
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• 2019

The delamination is a special mode of failure occurring in composite laminates. Several numerical studies with finite element analysis have been carried out on the delamination behavior of unidirectional composite laminates. On the other hand, the fracture for the multi-directional composite laminates may occur not only along the resin-fiber interface between plies known as interply or interlaminar fracture but also within a ply known as interyarn or intralaminar fracture accompanied by matrix cracking and fiber bridging. In addition, interlaminar and intralaminar cracks appear at irregular proportions and intralaminar cracks proceeded at arbitrary angle. The probabilistic analysis method for the prediction of crack growth behavior within a layer is more advantageous than the deterministic analysis method. In this paper, we analyze the crack path when the mode I load is applied to the cross-ply carbon/epoxy composite laminates and collect and analyze the probability data to be used as the basis of the probabilistic analysis in the future. Two criteria for the theoretical analysis of the crack growth direction were proposed by analyzing the stress field at the crack tip of orthotropic materials. Using the proposed method, the crack growth directions of the cross-ply carbon/epoxy laminates were analyzed qualitatively and quantitatively and compared with experimental results.