• 제목/요약/키워드: Intergranular failure

검색결과 27건 처리시간 0.028초

전자비임 용접한 250 및 300 Grade 18% Ni Maraging 강의 수소취화 거동에 관한 연구 (A study of hydrogen embrittlement behavior in E.B welded 250,300 grade 18% Ni maraging steel)

  • 윤한상;정병호
    • Journal of Welding and Joining
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    • 제5권2호
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    • pp.53-59
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    • 1987
  • The effect of applied stress, current density and heat-treatment after welding on the time to fracture, fracture behavior was investigated by the method of constant load tensile testing under catholic charging with hydrogen in E.B. welded 250,300 Grade 18% Ni Maraging steel sheet. The main results obtained are as follows: 1. All specimen showed the characteristic delayed failure and the time to fracture showed decreasing tendency with the increase in current density and applied stress. 2. Hydrogen embitterment susceptibility of notched specimen after solution-treatment and aging after welding was more increased than that of aged smooth specimen and as welded specimen. 3. Fracture surface showed a typical intergranular fracture on the border, a dimple pattern in the center of specimen and some quasi-cleavage fracture between the intergranular and the dimple.

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고강도 볼트 카드늄 취성파괴 사례연구 (The Case Study on Cadmium Embrittlement Failure of High Strength Bolt)

  • 윤용인
    • 한국군사과학기술학회지
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    • 제13권5호
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    • pp.769-774
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    • 2010
  • It happened fractures on special bolt which supported main landing gear actuator up-lock rod of aircraft. Cracks were initiated mainly from the center hole and the external thread of the special bolt. To find out failure root causes, metallographic, fractographic analyses as well as test work were carried out. From the fractographic study by SEM work, fracture occurred by a brittle intergranular type failure. The fracture could be occurred primarily by solid-metal-induced embrittlement due to cadmium embrittler penetrated into the flaw existed after machining work for center hole and thread on the bolt during baking treatment processing to eliminate hydrogen. For its successful application, cadmium EP bolts require proper and adequate baking treatment after electroplating, and make no more drilled center hole on the bolt to prevent same failure.

Fe-Aluminide합금의 미세조직과 기계적 특성에 관한 연구 (A Study on the Microstructure and Mechanical properties of Fe Aluminide alloys)

  • 조종춘;이도인;이성재;최병학;김학민
    • 연구논문집
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    • 통권22호
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    • pp.115-125
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    • 1992
  • Mechanical properties and microstructure were investigated on vacuum induction melted $Fe_3A1$base alloys of $DO_3$ structure. Specal emphasis were put on the effect of alloy chemistry, grain size and process(rolling, directional solidification) on mechanical properties of Fe-22.5-39at.%Al at elevated temperature between room temperature and $800^{\circ}C$. grain size of as-cast alloys is refined by rolling from 1mm to $80\mum$. Tensile strength of Fe-24.lat.%AI was about 404MPa at the critical ordering temperature, and the fracture strain of the alloy was 1-2% at room temperature. An inverse temperature dependence of the strength is noticed as-cast $Fe_3A1$. The presence of Cr and Zr do not affect the room temperature ductility and high temperature strength. Fracture strain of directionally solidified(DS) $Fe_3A1$ is about 1%at room temperature, but is about 60%at. $T_C$(550^{\circ}C)$. Tensile strength of DS alloy is lower than that of as-cast alloy at $530^{\circ}C$ and $430^{\circ}C$. Failure mode at room temperature varies from transgranular fracture to intergranular fracture with the addition of Al. the failure mode also varies from mixed(transgranular+ intergranular) mode between room temperature and $500^{\circ}C$ to intergranular mode above $550^{\circ}C$

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A Study on Analysis of J85 Engine V.G. Actuator Arm Shaft Crack

  • Hwang, Young-Ha;Son, Kyung-Sug;Kim, Tae-Gu
    • International Journal of Safety
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    • 제8권1호
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    • pp.6-9
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    • 2009
  • The crack in a J85 engine V.G. actuator arm shaft for a bell crank on the engine compressor was investigated. The crack was observed in twenty two shafts during the inspection of 238 shafts. The failure analysis of shaft cracks was performed by chemical composition analysis using ICP(Inductively Coupled Plasma) and by fracture surface and microstructure analysis using FE-SEM and optical microscope. The crack initiated from the top and bottom and propagated to the center along the grain boundaries. From the chemical composition analysis, the fractography of the fracture surface and the microstructure, it was found that the failure mechanism of the shafts is the inclusion-related intergranular decohesion crack. The inclusion was found out from MnS particle by EDS(Energy Dispersive Spectroscopy). The crack initiated MnS inclusion in the grain boundary and propagated with the increase of applied shear stress during long operation. In order to prevent the fracture, NDI(Nondestructive inspection) is needed periodically as recommended.

UNS N08810 합금의 입계부식손상과 원인 분석 (Elucidation of Intergranular Corrosion of UNS N08810 alloys)

  • 김영식;황보덕
    • Corrosion Science and Technology
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    • 제11권5호
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    • pp.196-204
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    • 2012
  • Corrosion failure of petrochemical facilities is one of the difficulties in maintenance, since operating conditions of crude oil production, storage, and refinement are very aggressive. UNS N08810, which has been used for crude oil transportation pipes and storage tanks in petrochemical industries, shows good resistance to general corrosion and localized corrosion in several environments. Among its environments, UNS N08810 showed better corrosion resistance in fuel gas containing sulfuric acid and phosphoric acid and sulfur. However, ductility and toughness at high temperature over about $500^{\circ}C$ were greatly reduced due to microstructural change. In general, welding process is the representative method to join the parts in industrial components. Because the alloy by welding can be sensitized and corroded, the manufacturing process should be controlled. In this work, UNS N08810 was used and heat treatment conditions including solution and stabilization treatments were controlled. Oxalic acid etch test by ASTM A262 Practice A was done to evaluate the qualitative sensitization in room temperature. Huey test by ASTM A262 Practice C was done to evaluate the intergranular corrosion rate in boiling 65% $HNO_3$ solution. Also, the microstructure by thermal history was analyzed. Experimental alloy showed high intergranular corrosion rate and its corrosion mechanism was elucidated.

굽힘 압전 복합재료 작동기의 전기적 피로 거동 (Electric Fatigue Behavior of a Bending Piezoelectric Composite Actuator)

  • 우성충;구남서
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2008년도 추계학술대회A
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    • pp.362-367
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    • 2008
  • In the present work, we address electric fatigue behavior in bending piezoelectric actuators using an acoustic emission technique. Electric cyclic fatigue tests have been performed up to ten million cycles on the fabricated specimens. To confirm the fatigue damage onset and its pathway, the source location and distributions of the AE behavior in terms of count rate are analyzed over the fatigue range. It is concluded that electric cyclic loading leads to fatigue damages such as transgranular damages and intergranular cracking in the surface of the PZT ceramic layer, and intergranular cracking even develops into the PZT inner layer, thereby degrading the displacement performance. The electric-induced fatigue behavior seems to show not a continuous process but a step-by-step process because of the brittleness of PZT ceramic. Nevertheless, this fatigue damage and cracking do not cause the final failure of the bending piezoelectric actuator loaded up to 107 cycles. Investigations of the AE behavior and the linear AE source location reveal that the onset time of the fatigue damage varies considerably depending on the existence of a glass-epoxy protecting layer.

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전기적 피로하중을 받는 압전 작동기의 손상 메커니즘 (Damage Mechanisms of a Piezoelectric Actuator under Electric Fatigue Loading)

  • 우성충;구남서
    • 대한기계학회논문집A
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    • 제32권10호
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    • pp.856-865
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    • 2008
  • Damage mechanisms in bending piezoelectric actuators under electric fatigue loading are addressed in this work with the aid of an acoustic emission (AE) technique. Electric cyclic fatigue tests have been performed up to $10^7$ cycles on the fabricated bending piezoelectric actuators. An applied electric loading range is from -6 kV/cm to +6 kV/cm, which is below the coercive field strength of the PZT ceramic. To confirm the fatigue damage onset and its pathway, the source location and distributions of the AE behavior in terms of count rate and amplitude are analyzed over the fatigue range. It is concluded that electric cyclic loading leads to fatigue damages such as transgranular damages and intergranular cracking in the surface of the PZT ceramic layer, and intergranular cracking even develops into the PZ inner layer, thereby degrading the displacement performance. However, this fatigue damage and cracking do not cause the final failure of the bending piezoelectric actuator loaded up to $10^7$ cycles. Investigations of the AE behavior and the linear AE source location reveal that the onset time of the fatigue damage varies considerably depending on the existence of a glass-epoxy protecting layer.

고강도 볼트 카드늄 취성파괴 사례연구 (The Case Study of High Strength Bolt Cadmium Embrittlement Failure)

  • 윤용인;박찬욱;손경숙
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2008년도 추계학술대회A
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    • pp.244-249
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    • 2008
  • It happened a failure on special bolt which supported main landing gear actuator up-lock rod of 00 aircraft. Fracture was occurred at end of center drilled hole and thread machined on bolt. Metallographic, fractographic, and other characteristics of embrittlement analysis and experiments carried out on the failed bolt to find out the reason. Bolt surface was cadmium electroplated(EP) to give lubrication and provide excellent corrosion resistance. Resultly, Bolt was failed due to cadmium embrittlement occurred during baking treatment as well as center drilled hole. for the failure that are relevant to failure analysis and prevention. For their successful functional application, cadmium EP bolts require proper and adequate baking treatment after electroplating, and is complete with no center drilled hole

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Nd:YAG 레이저로 용접한 인코넬 600관과 인코넬 690의 C링 응력 부식시험 (C-Ring Stress Corrosion Test for Inconel 600 Tube and Inconel 690 welded by Nd:YAG Laser)

  • 김재도;문주홍;정진만;김철중
    • 대한용접접합학회:학술대회논문집
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    • 대한용접접합학회 1998년도 특별강연 및 추계학술발표 개요집
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    • pp.288-291
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    • 1998
  • Inconel 600 alloy is used as the material of nuclear steam generator tubing because of its mechanical properties, formability, and corrosion properties. According to reports, the life time of nuclear power plants decreases because of the pitting, intergranular attack, primary water stress corrosion cracking(PWSCC), and intergranular stress corrosion cracking(IGSCC), and denting in the steam generator. The SCC test is very important because of SCC appears in various environment such as solutions, materials, and stress. The C-Rig specimen was made of the steam generator welded sleeve repairing by the pulsed Nd:YAG laser. In the corrosion invironment, corrosion solutions are Primary Water, Caustic, and Sulfate solution and corrosion time is 1624-4877hr. The permitted stress is 30-60ksi.In this C-Ring SCC test is the relationship between corrosion depth, crack and corrosion environment is evaluated. SCC was happens in Sulfate and Corrosion solution but doesn't happen in Primary Water. The corrosion time and stress is very affected by the severely environment of Sulfate or Caustic solution. The microstructure observation indicates that SCC causes interganular failure in the grain boundary of vertical direction.

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Electronic Packaging에 쓰이는 공정 조성의 Pb-Sn Solders에서 Grain Boundary Sliding과 관련된 계면파괴현상 (INTERGRANULAR FAILURE ASSOCIATED WITH BOUNDARY SLIDING IN Pb-SN EUTECTIC SOLDERS USED FOR MICROELECTRONICS APPLICATIONS)

  • 이성민
    • 한국재료학회지
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    • 제4권3호
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    • pp.334-338
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    • 1994
  • Pb-Sn eutectic bulk specimens을 thermal cycling동안 electronic package의 땜납이 격게되는 변형 조건 즉 $10^{-3}-10^{-5}$/s정도의 낮은 frequency와 0.2-1%정도의 적당한 strain range에서 피로파괴 실험을 했을때, grain boundary sliding과 관련하여 임계면을 따라 일어나는 균열이 5단계에 의해 묘사될 수 있다는 것을 보였음.

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