• Title/Summary/Keyword: Instrumental Analysis Method

검색결과 199건 처리시간 0.019초

천연오염 평가에 대한 화상분석의 응용 (Application of Image Analysis to the Evaluation of Natural Soils)

  • 이일심;차옥선
    • 한국의류학회지
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    • 제21권1호
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    • pp.194-205
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    • 1997
  • The typical instrumental assessment of ununiform natural soils has been carried out by yellowing of the specimens instead of the surface reflectance or the calculated formula. However, the regular instrumental area of sample holder is necessary for the measure of yellowing. Therefore, this study attempted to apply image analysis which had full color image by scanning of one time without limitation of instrumental area. The test samples were analyzed pseudo and full color image. This paper evaluated soil with hue of yellowing and gradation of gray level with color image analysis. Then, it was studied propriety of image analysis with correlation of yellowing, hue and gray level. Ultimately, the proposed image analysis in this paper was advanced method against the typical instrumental assessment.

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ACTIVATION ANALYSIS OF ENVIRONMENTAL SAMPLES USING THE MT-25 MICROTRON OF THE FLNR

  • Maslov, O.D.;Belov, A.G.;Starodub, G.Ya.;Dmitriev, S.N.
    • 분석과학
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    • 제8권4호
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    • pp.815-820
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    • 1995
  • Instrumental neutron and gamma activation analysis of coal and combustion products, determination of platinum content in natural samples by radiochemical gamma activation analysis and high-sensitive track method of thorium determination has been studied with the use of the MT-25 microtron.The optimal conditions for complete elemental analysis of coal and combustion products, isolation and determination of platinum and thorium are recommended.

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Determination of trace elements in food reference materials by instrumental neutron activation analysis

  • Cho, K.H.;Zeisler, R.;Park, K.W.
    • 분석과학
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    • 제18권6호
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    • pp.520-528
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    • 2005
  • Two biological Certified Reference Materials (CRMs), KRISS 108-04-001 (oyster tissue) and 108-05-001 (water dropwort stem), were prepared by Korea Research Institute of Standards and Science (KRISS)during FY '01. The certified values of these materials had been determined by Isotope Dilution Mass Spectrometry (IDMS) for six elements (Cd, Cr, Cu, Fe, Pb and Zn). Additional analytical works are now progressing to certify the concentrations of a number of the environmental and nutrimental elements in these CRMs. The certified values in a CRM are usually determined by using a single primary method with confirmation by other method(s) or using two independent critically-evaluated methods. Instrumental Neutron Activation Analysis (INAA) plays an important role in the determination of certified values as it can eliminate the possibility of common error sources resulting from sample dissolution. In this study INAA procedure was used in determination of 23 elements in these two biological CRMs to acquire the concentration information and the results were compared with KRISS certified values.

도구변수법을 이용한 지역 노동시장의 내외국인근로자 고용관계 분석 (An Analysis on the Employment Relationship of Domestic and Foreign Workers in the Regional Labor Market Using Instrumental Variable Method)

  • 조은지;이찬영
    • 노동경제논집
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    • 제44권2호
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    • pp.33-69
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    • 2021
  • 본 연구는 2010~2018년 기간 동안의 16개 시도 지역 패널데이터를 구축하여 내외국인근로자의 고용관계를 추정한다. 산업별(제조업과 건설업), 규모별(5~29인, 5~99인, 5~299인 그리고 5인 이상) 분석을 시도하고 외국인근로자의 내생성을 통제하기 위하여 지역 내 외국인근로자의 출신 국가 점유율(Foreigner's Concentration Index: FCI)을 도구변수로 사용한다. 최종적으로는 외국인근로자의 내생성을 고려하지 않는 패널 GLS와 이를 고려한 도구변수법의 결과를 비교한다. 분석 결과, 패널 GLS 분석에서는 내외국인근로자 사이에 보완관계가 확인되었다. 그러나 도구변수법에서는 내외국인근로자의 고용관계가 통계적으로 유의하지 않았지만, 정(+)에서 부(-)로 바뀌었으며, 제조업과 건설업을 결합한 분석에서는 통계적으로 유의한 대체관계가 나타났다. 본 연구는 내외국인근로자의 고용관계를 추정하는 데 있어서 내생성 통제 여부의 중요성을 확인하고 이를 통제하기 위해 도구변수를 국내 최초로 고안했다는 점에서 높은 평가를 받을 수 있다.

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$k_0$-표준화방법에 의한 기기중성자방사화 분석법의 고찰 (The Review of Instrumental Neutron Activation Analysis by $k_0$-standardization method)

  • 문종화;정용삼;김선하
    • 분석과학
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    • 제14권4호
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    • pp.1075-1081
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    • 2001
  • 기기중성자방사화 분석법은 핵 분석기술의 대표적인 방법으로 비파괴-동시 다원소분석의 장점과 함께 절대측정값에 의해 정량 할 수 있다는 특징을 갖고 있다. 최근에는 정확도와 편의성을 만족할 수 있는 $k_0$-정량법을 사용한 기기중성자방사화 분석법이 세계적으로 일반화되고 있다. 본 연구에서는 $k_0$-법의 적용을 위하여 이 방법의 전체적인 개념의 소개와 함께 $k_0$-파라미터를 측정하고자 하였다. 이를 위하여 $k_0$-법의 개념이해와 정량에 필요한 인자들의 정의 및 파라미터인 $Q_0$(${\alpha}$)와 f 값을 결정하기 위한 수식과 실험적 측정방법 등을 요약하였고 중성자조사공에 따라 특성 값을 갖는 ${\alpha}$와 f 값을 하나로 연구용원자로의 방사화분석용 조사공(NAA#1)에서 측정하여 $k_0$-법의 도입을 위한 기반을 마련하였다.

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모드해석법과 보조변수법을 이용한 NFR 슬라이더 평가방법 (Evaluation Method of NFR Slider Using Modal Analysis Method and Instrumental Variable Method)

  • 안채헌;임경화
    • 한국소음진동공학회:학술대회논문집
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    • 한국소음진동공학회 2002년도 춘계학술대회논문집
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    • pp.688-693
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    • 2002
  • Identification method is formulated to evaluate the dynamic characteristics of air bearings under NFR(Near Field Recording) sliders. Impulse responses and frequency response functions of NFR sliders are obtained on numerical non-linear models including rigid motion of slider and fluid motion of air bearing under the slider. Modal parameters and system parameters are identified by modal analysis method and instrumental variable method. The parameters of sliders are utilized to evaluate the dynamic characteristics of air bearings. Also, this study shows the difference between the dynamic characteristics of NFR and HDD slides, and squeeze effect of air bearings.

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공기희석관능법과 기기분석법에 기초한 악취감지기술의 연계성 비교: 산단지역 및 음식물 부패시료를 중심으로 (A Comparative Study of Odors between Air Dilution Sensory Test and Instrumental Detection Method Using Industrial and Food Waste Samples)

  • 박신영;김기현
    • 한국대기환경학회지
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    • 제23권4호
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    • pp.420-429
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    • 2007
  • In this study, we attempted to evaluate the relationship between air dilution sensory test and instrumental detection method for individual odorous compound. For the purpose of our comparative study, we conducted the analysis of malodor on total of 46 samples collected from both industrial and food waste sectors using the two independent approaches. The results of instrumental analyses were explained after modification to several parameters such as: the sum of odor concentration (SOC), sum of odor quotient (SOQ) and sum of odor intensity (SOI). When we compared dilution ratio values (DRV) of threshold limit (TL) with the modified instrumental data sets, pearson coefficient of SOC, SOQ, and SOI were 0.556 (p=5.83E-05), 0.911 (p=9.64E-19) and 0.847 (p=8.93E-14), respectively. The results of this study thus suggest that the DRV of TL sensitively reflects odor strength measured intuitive.

유도결합 플라즈마 원자방출 분광법에 의한 아연광 중 Ga 및 In의 분석에 관한 연구 (Studies on Analysis of Gallium and Indium in Zinc Ores by Inductively Coupled Plasma Atomic Emission Spectrometry)

  • 황윤옥;심상권;성학제;양명권
    • 분석과학
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    • 제6권1호
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    • pp.131-139
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    • 1993
  • 아연광 중 미량으로 존재하는 갈륨 및 인듐을 유도결합 플라스마 원자방출분광법(ICP-AES)으로 분석할 때 간섭하는 아연 및 다른 이온들과 특히 Fe(III) 이온으로부터 이들을 분리하는 방법에 대해 연구하였다. 갈륨과 인듐을 tributyl phosphate(TBP)로 용매추출하였는데 이때 영향을 주는 산농도, 다른 이온들의 간섭, 수용액상/유기상의 비율, TBP의 농도 및 탈거율 등에 대하여 조사하였다. 갈륨과 인듐이 함유되어 있는 아연광을 녹인 5N 염산용액에서 100% TBP로 추출하여 아연 및 기타 간섭이온들로부터 분리하였으며, 이때 철(III)이온은 hydroxylamine hydrochloride를 사용하여 Fe(II)로 환원시켜 coetraction되는 것을 방지하였다. 유기상으로부터 갈륨과 인듐의 탈거는 0.02N 염산용액으로 역추출하여 이루어졌으며 이 용액을 ICP-AES로 측정하여 이들을 정량하였다. 전체적으로 추출률이 95% 이상으로 정량적이었다.

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중성자 방사화분석법을 이용한 대기분진시료의 정량 (Determination of Trace Elements in Airborne Particulates by Instrumental Neutron Activation Analysis)

  • Chung, Yong-Sam;Chung, Young-Ju;Jeong, Eui-Sik;Cho, Seung-Yeon
    • Nuclear Engineering and Technology
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    • 제27권2호
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    • pp.234-247
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    • 1995
  • Trace elements in airborne particulates were analyzed by instrumental neutron activation analysis (INAA) under the optimum analytical condition. Neutron irradiation for sample was done at the irradiation hole(neutron flux 1$\times$10$^{13}$ n/$\textrm{cm}^2$.s) of TRIGA MARK-III research reactor in the Korea Atomic Energy Research Institute. For the verification of the analytical method, NIST SRM-1648 and NIES CRM No.8 ore chosen and analyzed. The accuracy and precision of the analysis of 40 and 24 trace elements in the samples were compared with the certified and reported values, respectively. The analytical method was found to be reliable enough when the analytical data of NIES sample were compared with those of different counties. In the analytical result of two or both of standard reference materials, relative standard deviation wes within the 15% except a few elements and the relative error was within the 10%. We used this method to analyze 30 trace elements in airborne particulates collected with the high volume air sampler(PM-10) at too different locations and also confirmed the possibility to use this method as a routine monitoring tool to find out environmental pollution sources.

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The Factors Affecting on Elderly' Life Satisfaction in the Residential Environments

  • Jeong, Jae Hoon
    • Architectural research
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    • 제16권4호
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    • pp.149-156
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    • 2014
  • This research is designed to identify factors that affect life satisfaction of the Korean elderly by studying residential environments and individual personalities as independent variables, and life satisfaction of the elderly as a dependent variable. It also includes emotional and instrumental support to describe relations between variables as mediating variables. It utilizes a questionnaire survey as its research method and studies those aged 65 and over living in urban, suburban and rural areas. In addition, regression and path analysis is used to identify casual links between different variables. The results are as follows: (1) Direct factors that impact emotional support are home ownership (direct effect= -.18) and transportation services (.15). That is, those who own their home and have easy access to public transpiration show increased levels of emotional support. (2) Direct factors that affect instrumental support are economic status (direct effect= .311) and living arrangement (.17). In other words, those who are financially stable and live with their children have more instrumental support. (3) Factors linked directly to life satisfaction of the elderly are their age (direct effect= -.10), health status (.19), economic status (.25), region of living (.22) and housing type (.19). (4) Among the mediating variables, emotional support has direct effect (.45) while instrumental support has indirect effect (.16).