• Title/Summary/Keyword: Instrumental Analysis Method

Search Result 200, Processing Time 0.021 seconds

Application of Image Analysis to the Evaluation of Natural Soils (천연오염 평가에 대한 화상분석의 응용)

  • 이일심;차옥선
    • Journal of the Korean Society of Clothing and Textiles
    • /
    • v.21 no.1
    • /
    • pp.194-205
    • /
    • 1997
  • The typical instrumental assessment of ununiform natural soils has been carried out by yellowing of the specimens instead of the surface reflectance or the calculated formula. However, the regular instrumental area of sample holder is necessary for the measure of yellowing. Therefore, this study attempted to apply image analysis which had full color image by scanning of one time without limitation of instrumental area. The test samples were analyzed pseudo and full color image. This paper evaluated soil with hue of yellowing and gradation of gray level with color image analysis. Then, it was studied propriety of image analysis with correlation of yellowing, hue and gray level. Ultimately, the proposed image analysis in this paper was advanced method against the typical instrumental assessment.

  • PDF

ACTIVATION ANALYSIS OF ENVIRONMENTAL SAMPLES USING THE MT-25 MICROTRON OF THE FLNR

  • Maslov, O.D.;Belov, A.G.;Starodub, G.Ya.;Dmitriev, S.N.
    • Analytical Science and Technology
    • /
    • v.8 no.4
    • /
    • pp.815-820
    • /
    • 1995
  • Instrumental neutron and gamma activation analysis of coal and combustion products, determination of platinum content in natural samples by radiochemical gamma activation analysis and high-sensitive track method of thorium determination has been studied with the use of the MT-25 microtron.The optimal conditions for complete elemental analysis of coal and combustion products, isolation and determination of platinum and thorium are recommended.

  • PDF

Determination of trace elements in food reference materials by instrumental neutron activation analysis

  • Cho, K.H.;Zeisler, R.;Park, K.W.
    • Analytical Science and Technology
    • /
    • v.18 no.6
    • /
    • pp.520-528
    • /
    • 2005
  • Two biological Certified Reference Materials (CRMs), KRISS 108-04-001 (oyster tissue) and 108-05-001 (water dropwort stem), were prepared by Korea Research Institute of Standards and Science (KRISS)during FY '01. The certified values of these materials had been determined by Isotope Dilution Mass Spectrometry (IDMS) for six elements (Cd, Cr, Cu, Fe, Pb and Zn). Additional analytical works are now progressing to certify the concentrations of a number of the environmental and nutrimental elements in these CRMs. The certified values in a CRM are usually determined by using a single primary method with confirmation by other method(s) or using two independent critically-evaluated methods. Instrumental Neutron Activation Analysis (INAA) plays an important role in the determination of certified values as it can eliminate the possibility of common error sources resulting from sample dissolution. In this study INAA procedure was used in determination of 23 elements in these two biological CRMs to acquire the concentration information and the results were compared with KRISS certified values.

An Analysis on the Employment Relationship of Domestic and Foreign Workers in the Regional Labor Market Using Instrumental Variable Method (도구변수법을 이용한 지역 노동시장의 내외국인근로자 고용관계 분석)

  • Cho, Eunji;Lee, Chanyoung
    • Journal of Labour Economics
    • /
    • v.44 no.2
    • /
    • pp.33-69
    • /
    • 2021
  • This study estimates the employment relationship of domestic and foreign workers by establishing 16 municipal and provincial panel data for the period 2010-2018. It attempts to analyze industry-specific (manufacturing and construction), scale-specific (5-29, 5-29, 5-299 and 5 above) and uses the foreign worker's national share (foreigner's concentration index) as an instrumental variable to control the endogeneity of foreign workers. Finally, it compares the results of panel GLS, which does not consider the endogeneity of foreign workers, with the results using instrumental variable method that considers it. As a result of the analysis, the complementary relationship between domestic and foreign workers was confirmed in the panel GLS analysis. However, although the employment relationship between domestic and foreign workers was not statistically significant in the instrumental variable method, the analysis of the combination of manufacturing and construction industry showed a statistically significant substitute relationship. This study is highly regarded for the first time in Korea that an instrumental variable method was created to identify and control the endogeneity of foreign workers in estimating employment relationships between domestic and foreign workers.

  • PDF

The Review of Instrumental Neutron Activation Analysis by $k_0$-standardization method ($k_0$-표준화방법에 의한 기기중성자방사화 분석법의 고찰)

  • Moon, Jong-Hwa;Chung, Yong-Sam;Kim, Sun-Ha
    • Analytical Science and Technology
    • /
    • v.14 no.4
    • /
    • pp.1075-1081
    • /
    • 2001
  • Instrumental Neutron Activation Analysis as a representative method of nuclear analytical technique, has advantages of non-destructive, simultaneous multi-element analysis with the characteristics of absolute measurement method. Up to date, $k_0$-quantitative method which is accurate, convenient and user-friendly, has been generalized world-widely. In this study, it is intented to introduce the general concept of $k_0$-method and to measure $k_0$-parameters for the future implementation to our NAA system. For this objectives, the definition of relevant factors for the quantitative analysis and the equation for the experimental determination of parameters such as $Q_0$(${\alpha}$) and f were summarized. Furthermore, a foundation for the $k_0$-standardization method was prepared through the measurement of ${\alpha}$ and f-value which depend on the specific character of irradiation hole at NAA#1-hole of HANARO research reactor.

  • PDF

Evaluation Method of NFR Slider Using Modal Analysis Method and Instrumental Variable Method (모드해석법과 보조변수법을 이용한 NFR 슬라이더 평가방법)

  • 안채헌;임경화
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
    • /
    • 2002.05a
    • /
    • pp.688-693
    • /
    • 2002
  • Identification method is formulated to evaluate the dynamic characteristics of air bearings under NFR(Near Field Recording) sliders. Impulse responses and frequency response functions of NFR sliders are obtained on numerical non-linear models including rigid motion of slider and fluid motion of air bearing under the slider. Modal parameters and system parameters are identified by modal analysis method and instrumental variable method. The parameters of sliders are utilized to evaluate the dynamic characteristics of air bearings. Also, this study shows the difference between the dynamic characteristics of NFR and HDD slides, and squeeze effect of air bearings.

  • PDF

A Comparative Study of Odors between Air Dilution Sensory Test and Instrumental Detection Method Using Industrial and Food Waste Samples (공기희석관능법과 기기분석법에 기초한 악취감지기술의 연계성 비교: 산단지역 및 음식물 부패시료를 중심으로)

  • Park, S.Y.;Kim, K.H.
    • Journal of Korean Society for Atmospheric Environment
    • /
    • v.23 no.4
    • /
    • pp.420-429
    • /
    • 2007
  • In this study, we attempted to evaluate the relationship between air dilution sensory test and instrumental detection method for individual odorous compound. For the purpose of our comparative study, we conducted the analysis of malodor on total of 46 samples collected from both industrial and food waste sectors using the two independent approaches. The results of instrumental analyses were explained after modification to several parameters such as: the sum of odor concentration (SOC), sum of odor quotient (SOQ) and sum of odor intensity (SOI). When we compared dilution ratio values (DRV) of threshold limit (TL) with the modified instrumental data sets, pearson coefficient of SOC, SOQ, and SOI were 0.556 (p=5.83E-05), 0.911 (p=9.64E-19) and 0.847 (p=8.93E-14), respectively. The results of this study thus suggest that the DRV of TL sensitively reflects odor strength measured intuitive.

Studies on Analysis of Gallium and Indium in Zinc Ores by Inductively Coupled Plasma Atomic Emission Spectrometry (유도결합 플라즈마 원자방출 분광법에 의한 아연광 중 Ga 및 In의 분석에 관한 연구)

  • Hwang, Youn-Ok;Sim, Sang-Kwon;Sung, Hack-Je;Yang, Myung-Kwon
    • Analytical Science and Technology
    • /
    • v.6 no.1
    • /
    • pp.131-139
    • /
    • 1993
  • The separation of gallium and indium from the matrix elements such as zinc and other ions, especially form Fe(III) ion was studied for the determination of trace level of them in zinc ores and zinc blendes by inductively coupled plasma atomic emission spectrometry(ICP-AES). Gallium and indium were extracted from the sample solution with a solvent of tributyl phosphate(TBP). The type and concentration of acid, interferences of other ions, the ratio of aqueous phase to organic phase, TBP concentration, sripping efficiency were optimized for the effective extraction. Gallium and indium were separated from other ions in the 5N hydrochloric acid solution of the samples by the extraction with 100% TBP. In this time, Fe(III) was reduced to Fe(II) with hydroxylamine hydrochloride to prevent its coextraction prior to the main extraxtion. After stripped from organic phase by the back-extraction with 0.02N HCl, they were determined in the aqueous phase by ICP-AES. This method was known to be quantitative from the overall extraction of more than 95%.

  • PDF

Determination of Trace Elements in Airborne Particulates by Instrumental Neutron Activation Analysis (중성자 방사화분석법을 이용한 대기분진시료의 정량)

  • Chung, Yong-Sam;Chung, Young-Ju;Jeong, Eui-Sik;Cho, Seung-Yeon
    • Nuclear Engineering and Technology
    • /
    • v.27 no.2
    • /
    • pp.234-247
    • /
    • 1995
  • Trace elements in airborne particulates were analyzed by instrumental neutron activation analysis (INAA) under the optimum analytical condition. Neutron irradiation for sample was done at the irradiation hole(neutron flux 1$\times$10$^{13}$ n/$\textrm{cm}^2$.s) of TRIGA MARK-III research reactor in the Korea Atomic Energy Research Institute. For the verification of the analytical method, NIST SRM-1648 and NIES CRM No.8 ore chosen and analyzed. The accuracy and precision of the analysis of 40 and 24 trace elements in the samples were compared with the certified and reported values, respectively. The analytical method was found to be reliable enough when the analytical data of NIES sample were compared with those of different counties. In the analytical result of two or both of standard reference materials, relative standard deviation wes within the 15% except a few elements and the relative error was within the 10%. We used this method to analyze 30 trace elements in airborne particulates collected with the high volume air sampler(PM-10) at too different locations and also confirmed the possibility to use this method as a routine monitoring tool to find out environmental pollution sources.

  • PDF

The Factors Affecting on Elderly' Life Satisfaction in the Residential Environments

  • Jeong, Jae Hoon
    • Architectural research
    • /
    • v.16 no.4
    • /
    • pp.149-156
    • /
    • 2014
  • This research is designed to identify factors that affect life satisfaction of the Korean elderly by studying residential environments and individual personalities as independent variables, and life satisfaction of the elderly as a dependent variable. It also includes emotional and instrumental support to describe relations between variables as mediating variables. It utilizes a questionnaire survey as its research method and studies those aged 65 and over living in urban, suburban and rural areas. In addition, regression and path analysis is used to identify casual links between different variables. The results are as follows: (1) Direct factors that impact emotional support are home ownership (direct effect= -.18) and transportation services (.15). That is, those who own their home and have easy access to public transpiration show increased levels of emotional support. (2) Direct factors that affect instrumental support are economic status (direct effect= .311) and living arrangement (.17). In other words, those who are financially stable and live with their children have more instrumental support. (3) Factors linked directly to life satisfaction of the elderly are their age (direct effect= -.10), health status (.19), economic status (.25), region of living (.22) and housing type (.19). (4) Among the mediating variables, emotional support has direct effect (.45) while instrumental support has indirect effect (.16).