• Title/Summary/Keyword: Inconel alloys

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Effect of Solution Annealing Heat Treatment on the Localized Corrosion Resistance of Inconel 718 (Inconel 718의 국부 부식 저항성에 미치는 용체화 열처리의 영향)

  • Yoonhwa Lee;Jun-Seob Lee;Soon Il Kwon;Jungho Shin;Je-hyun Lee
    • Corrosion Science and Technology
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    • v.22 no.5
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    • pp.359-367
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    • 2023
  • The localized corrosion resistance of the Ni-based Inconel 718 alloy after solution heat treatment was evaluated using electrochemical techniques in a solution of 25 wt% NaCl and 0.5 wt% acetic acid. Solution heat treatment at 1050 ℃ for 2.5 hours resulted in an increased average grain diameter. Both Ti carbides (10 ㎛ diameter) and Nb-Mo carbides (1 - 9 ㎛ diameter) were distributed throughout the material. Despite heat treatment, the shape and composition of these carbides remained consistent. An increase in solution temperature led to a decrease in pitting potential value. However, the pitting potential value of solution heat-treated Inconel 718 was consistently higher than that of as-received Inconel 718 at all tested temperatures. Localized corrosion initiation occurred at 0.4 VSSE in a temperature environment of 80 ℃ for both as-received and solution heat-treated Inconel 718 alloys. X-ray photoelectron spectroscopic analysis indicated that the composition of the passive film formed on specimen surfaces remained largely unchanged after solution heat treatment, with O1s, Cr2p3/2, Fe2p3/2, and Ni2p3/2 present. The difference in localized corrosion resistance between as-received and solution heat-treated Inconel 718 alloys was attributable to microstructural changes induced by the heat treatment process.

Estimation of Machinability for Super Heat-resistant Alloys Inconel 600 in Turning Process (선삭가공에서 초내열합금 Inconel 600의 가공성 평가)

  • Won, Jong-Sik;Lim, Eun-Seong;Jung, Yoon-Gyo
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.10 no.6
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    • pp.1-8
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    • 2011
  • Recently, super heat-resistant alloy Inconel 600 come into spotlight as the material of airplane parts but this material causes lots of problems that is, reduction of machinability and attritious wear and breakage of cutting tool during turning processing due to high temperature strength and cohesion between tool material and Inconel 600. Therefore, in this study, it was purposed to determine tool material kind and to select of proper cutting range when turning process was carried out for Inconel 600. In order to these Purpose, coated carbide tool and ceramic tool was used in this experiment and the machinability of Inconel 600 was investigated from perspective of the cutting force, chipping and wear of tool and deposition phenomenon of chip.

A Study on the Cracking Behavior in the Welds of Ni-Cr-Fe and Ni-Fe-Cr-Mo Alloys (Ni-Cr-Fe 및 Ni-Fe-Cr-Mo계 합금의 용접부 균열특성에 관한 연구 Part II : 열영향부의 액화균열)

  • 김희봉;이창희
    • Journal of Welding and Joining
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    • v.15 no.5
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    • pp.46-55
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    • 1997
  • This study has evaluated the liquation cracking behavior in the heat affected zone of several Ni base superalloys (Incoloy 825, Inconel 718 and Inconel 600). 304 and 310S austenitic stainless steels were also included for comparison. In addition, the mechanism of liquation cracking in the HAZ was postulated based on the extensive microstructural examinations with SEM, EDAX and TEM. The liquation cracking resistance of Ni base alloys was found to be far inferior to that of austenitic stainless steels. The liquation cracking of Incoloy 825 and Inconel 718 was believed to be closely related with the Laves-austenite(Ti rich in 825 and Nb rich in 718) and MC-austenitic eutectic phases formed along the grain boundaries by constitutional liquation and incipient melting under rapid welding thermal contraction. Further, liquation cracking resistance of the HAZ was dependent not only upon the type and amount of low melting phases but also on the grain size.

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CORROSION BEHAVIOR OF NI-BASE ALLOYS IN SUPERCRITICAL WATER

  • Zhang, Qiang;Tang, Rui;Li, Cong;Luo, Xin;Long, Chongsheng;Yin, Kaiju
    • Nuclear Engineering and Technology
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    • v.41 no.1
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    • pp.107-112
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    • 2009
  • Corrosion of nickel-base alloys (Hastelloy C-276, Inconel 625, and Inconel X-750) in $500^{\circ}C$, 25MPa supercritical water (with 10 wppb oxygen) was investigated to evaluate the suitability of these alloys for use in supercritical water reactors. Oxide scales formed on the samples were characterized by gravimetry, scanning electron microscopy/energy dispersive spectroscopy, X-ray diffraction, and X-ray photoelectron spectroscopy. The results indicate that, during the 1000h exposure, a dense spinel oxide layer, mainly consisting of a fine Cr-rich inner layer ($NiCr_{2}O_{4}$) underneath a coarse Fe-rich outer layer ($NiFe_{2}O_{4}$), developed on each alloy. Besides general corrosion, nodular corrosion occurred on alloy 625 possibly resulting from local attack of ${\gamma}$" clusters in the matrix. The mass gains for all alloys were small, while alloy X -750 exhibited the highest oxidation rate, probably due to the absence of Mo.

Joint Properties of Inconel 718 Additive Manufactured on Ti-6Al-4V by FGM method (Ti-6Al-4V 합금 기지 위에 FGM 방식으로 적층제조 된 Inconel 718의 접합 특성 분석)

  • Park, Chan Woong;Park, Jin Woong;Jung, Ki Chae;Lee, Se-Hwan;Kim, Sung-Hoon;Kim, Jeoung Han
    • Journal of Powder Materials
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    • v.28 no.5
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    • pp.417-422
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    • 2021
  • In the present work, Inconel 718 alloy is additively manufactured on the Ti-6Al-4V alloy, and a functionally graded material is built between Inconel 718 and Ti-6Al-4V alloys. The vanadium interlayer is applied to prevent the formation of detrimental intermetallic compounds between Ti-6Al-4V and Inconel 718 by direct joining. The additive manufacturing of Inconel 718 alloy is performed by changing the laser power and scan speed. The microstructures of the joint interface are characterized by scanning electron microscopy, energy-dispersive X-ray spectroscopy, and micro X-ray diffraction. Additive manufacturing is successfully performed by changing the energy input. The micro Vickers hardness of the additive manufactured Inconel 718 dramatically increased owing to the presence of the Cr-oxide phase, which is formed by the difference in energy input.

Magnetic NDE for Sensitization of Inconel 600 Alloy

  • Kikuchi, Hiroaki;Sumimoto, Takaki;Kamada, Yasuhiro;Kobayashi, Satoru
    • Journal of Magnetics
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    • v.18 no.3
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    • pp.348-351
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    • 2013
  • Inconel 600 alloy, Ni base alloy, is widely used for steam generator tubings where sensitization occurs at grain boundaries and sensitization will induce tubing failures. This alloy has usually paramagnetic property, however, it transforms into ferromagnetic property along grain boundaries when sensitization occurs: this means NDE using magnetism for sensitization is possible. Therefore, in this study, Inconel 600 alloys were heat treated at 873 K from 0 to 400 hours so as to generate sensitization and their magnetic properties were investigated in detail. The saturation and the residual magnetization increase with increasing heat treatment time and take a maximum. On the other hand, the coercive force decreases with the increase in time of heat treatment. We confirmed that characteristics at only grain boundaries change into ferromagnetic phase by a MFM observation. As a trial for industrial application, heat treated Inconel 600 alloy was scanned by a magnetic field sensor, and the variations in magnetization were obtained nondestructively. The results indicate a feasibility of magnetic NDE for sensitization of Inconel 600 alloy.

Evaluation of Fretting Fatigue Behavior for Inconel Alloy at 320℃ (320℃에서의 인코넬 합금의 프레팅 피로 거동 평가에 관한 연구)

  • Kwon, Jae-Do;Jeung, Han-Kyu;Chung, Il-Sup;Park, Dae-Kyu;Yoon, Dong-Hwan
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.35 no.8
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    • pp.951-956
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    • 2011
  • Inconel alloys are generally used as steam generator tubes in nuclear power plants. These alloys are highnickel chromium alloys that exhibit excellent resistance to aqueous corrosion. In this paper, the effects of elevated temperatures such as an operating temperature of $320^{\circ}C$ on the fretting fatigue behavior of inconel 600 and 690. We observed that the plain and fretting fatigue limits at $320^{\circ}C$ were slightly lower than those at room temperature. The frictional forces varied depending on the number of load cycles. After each test, we studied the fretting fatigue mechanisms via SEM observations. These results can be used for structural integrity evaluations at elevated temperatures and for studying fretting damage in steam generator systems.

Thermal properties of the surface-modified Inconel 617 (표면 처리에 따른 Inconel 617 합금의 고온 특성)

  • Cho, Hyun;Bang, Kwang-Hyun;Lee, Byeong-Woo
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.19 no.6
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    • pp.298-304
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    • 2009
  • The effect of the surface treatments on the high temperature properties of the Inconel 617, one of the promising candidate alloys for high temperature heat-transport system, has been studied. Various surface modification methods including a rapid thermal process(RTP), a hydrothermal treatment, and a physical vapor deposition($2{\mu}m$ thick TiAlN film by an arc discharge) were applied to the Inconel 617. The morphological and the structural properties of the surface-modified Inconel 617 samples after heat treatment at $1000^{\circ}C$ in the air were compared to find out whether inhomogeneous formation of $Cr_2O_3$ crust at the surface region was suppressed or not. TiAlN-coated Inconel 617 showed homogeneous microstructure and the lowest wear loss compared to bare, RTP- and hydrothermally-treated Inconel 617 by suppressing the $Cr_2O_3$ crust formation.

Design of Nickel Alloys Using the Theoretical Values Calculated from the Electronic State Energies (에너지 전자상태 계산으로 도출된 이론값을 이용한 니켈 합금 설계)

  • Baek, Min-Sook;Kang, Pub-Sung;Baek, Kyeong-Cheol;Kim, Byung-Il;Yoon, Dong-Joo
    • Korean Journal of Materials Research
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    • v.25 no.11
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    • pp.642-646
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    • 2015
  • Super alloys, which can be divided into three categories, i.e. Ni-base, Co-base, and Fe-base alloys, are widely used for high temperature applications. Since superalloys contain many alloying elements and precipitates, their chemistry and processing parameters need to be carefully designed. In this study, we designed a new Ni alloy to prevent corrosion due to water vapor and gases at high temperatures. The new alloy was designed using the theoretical value of the resulting energy electronic state calculation($DV-X{\alpha}$ method). The components that were finally used were Cr, Mo, and Ti, with Ni as a base. For these alloys, elements were selected in order to compare their values with that of the average theoretical basis for an Inconel 625 alloy. Finally, two kinds of Ni alloy were designed: Ni-28Cr-4Mo-2Ti and Ni-20Cr-10Mo-1Ti.

Study of oxidation behavior and tensile properties of candidate superalloys in the air ingress simulation scenario

  • Bin Du;Haoxiang Li;Wei Zheng;Xuedong He;Tao Ma;Huaqiang Yin
    • Nuclear Engineering and Technology
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    • v.55 no.1
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    • pp.71-79
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    • 2023
  • Air ingress incidents are major safety accidents in very-high-temperature reactors (VHTRs). Air containing a high volume fraction of oxygen may cause severe oxidation of core components at the VHTR, especially for the significantly thin alloy tube wall in the intermediate heat exchanger (IHE). The research objects of this study are Inconel 617 and Incoloy 800H, two candidate alloys for IHE in VHTR. The air ingress accident scenario is simulated with high-temperature air flow at 950 ℃. A continuous oxide scale was formed on the surfaces of both the alloys after the experiment. Because the oxide scale of Inconel 617 has a loose structure, whereas that of Incoloy 800H is denser, Inconel 617 exhibited significantly more severe internal oxidation than Incoloy 800H. Further, Inconel 617 showed a significant decrease in ultimate tensile strength and plasticity after aging for 200 h, whereas Incoloy 800H maintained its tensile properties satisfactorily. Through control experiment under vacuum, we preliminarily concluded that serious internal oxidation is the primary reason for the decline in the tensile properties of Inconel 617.