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강은철;전영건;김길식
- Journal of the Korean institute of surface engineering
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- v.24 no.3
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- pp.151-161
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- 1991
The isothermal oxidation behaviour of commercial superalloys produced in Korea was investigated by using Cahn-2000 microbalance in air at $1000^{\circ}C$ and $1100^{\circ}C$. The effect of alloying elements on the isothermal oxidation was studied by examination of the oxide structures, their morphologies, and EDS linescanning and mapping of cross-section of oxidized specimens. Generally, external Cr2O3 films were formed on all alloy surface, but were not pure, The effect on the oxidation behaviour of refractory elements such as Nb, Mo in Inconel 718 was considered to be deleterious, and the formation of internal Al oxide in Inconel 601 was beneficial.
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Lee, G.H.;Kwon, S.C.;Lee, S.Y.
- Journal of the Korean institute of surface engineering
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- v.32 no.3
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- pp.410-415
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- 1999
The adhesion strength of sputtered copper films to Inconel substrates has been studied using the scratch test. The effects of substrate treatments before deposition such as chemical or ion bombardment etching were investigated by means of a mean critical load derived from a Weibull-like statistical analysis. It was found that the mean critical load was very weak unless the amorphous layer produced by mechanical polishing on the substrate surface was eliminated. Chemical etching in a nitric-hydrochloric acid bath was shown to have practically no effect on the enhancement of the adhesion. In contrast, the addition in this bath of nickel and copper sulphates allowed removal of the amorphous layer and an increase in the values of the mean critical load. However, it was observed that excessive chemical etching could cancel out the mean critical load enhancement. The results obtained in the case of ion bombardment etching pretreatments could be far higher than those obtained with chemical etching. Moreover, for a sufficiently long period of ion bombardment etching, the adhesion strength was so high that it was impossible to observe evidence of an adhesion failure.
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정진만;김민석;박승규;김철중
- Proceedings of the Korean Nuclear Society Conference
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- 1997.05b
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- pp.555-560
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- 1997
원자력발전소의 전열관 보수용접기술은 원전시설의 수명연장을 목적으로 개발된 기술이며, 손상된 Inconel 600 전열관 내부에 Inconel 690 재질의 sleeve tube을 삽입한 후 용접을 하는 방법으로 수행된다. 증기발생기 전열관 sleeve 레이저 용접의 기본개념은 방사능지역 외부의 발진기로부터 발진된 레이저빔을 광섬유를 이용하여 장거리(200미터 이상) 전송하여 전열관 내부의 광학계 및 회전장치를 이용하여 전열관을 용접하는 방법이다. 본 연구에서는 펄스형 레이저의 용접 변수인 펄스폭, 반복율, 첨두출력 및 용접속도를 변화시키면서 용입상태를 측정하였고, 용접된 시편에 열처리 여부와 부식실험을 위한 C-ring 시편을 제작하여 caustic test를 위해 auto-clave vessel에서 1,000 시간 실험을 실시하였다.
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