• 제목/요약/키워드: In-situ characterization

검색결과 252건 처리시간 0.035초

Nicalon/CAS 세라믹 복합재료의 인장특성 (Tension Behavior of Nicalon/CAS Ceramic Composites)

  • 김정국;김원경
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2004년도 추계학술대회
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    • pp.232-237
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    • 2004
  • The tension behavior of Nicalon/CAS glass-ceramic matrix composites was investigated. Infrared (IR) thermography was employed for two different types of $Nicalon^{TM}/CAS$ composites, i.e., cross-ply and unidirectional specimens. During tensile testing, an IR camera was used for in-situ monitoring of progressive damages of $Nicalon^{TM}/CAS$ samples. The IR camera provided the temperature changes during tensile testing. Microstructural characterization using scanning electron microscopy (SEM) was performed to investigate the fracture mechanisms of $Nicalon^{TM}/CAS$ composites. In this investigation, the thermographic NDE technique was used to facilitate a better understanding of the fracture mechanisms of the $Nicalon^{TM}/CAS$ composites during tensile testing.

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Binding energy study from photocurrent signal in HgCdTe layers

  • Hong, Kwang-Joon
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2010년도 하계학술대회 논문집
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    • pp.379-379
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    • 2010
  • $Hg_{1_x}Cd_xTe$ (MCT) was grown by hot wall epitaxy. Prior to the MCT growth, the CdTe (111) buffer layer was grown on the GaAs substrate at the temperature of $590^{\circ}C$ for 15 min. When the thickness of the CdTe buffer layer was $5\;{\mu}m$ or thicker, the full width at half maximum values obtained from the x-ray rocking curves were found to significantly decrease. After a good quality CdTe buffer layer was grown, the MCT epilayers were grown on the CdTe (111) /GaAs substrate at various temperatures in situ. The crystal quality for those epilayers was investigated by means of the x-ray rocking curves and the photocurrent experiment. The photoconductor characterization for the epilayers was also measured. The energy band gap of MCT was determined from the photocurrent measurement and the x composition rates from the temperature dependence of the energy band gap were turned out.

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Tensile Characterization of Ceramic Matrix Composites (CMCs) with Nondestructive Evaluation (NDE) Techniques

  • Kim, Jeongguk;Lee, Joon-Hyun
    • 한국복합재료학회:학술대회논문집
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    • 한국복합재료학회 2003년도 추계학술발표대회 논문집
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    • pp.190-194
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    • 2003
  • Two different types of nondestructive evaluation (NDE) techniques were employed to investigate the tensile behavior of ceramic matrix composites (CMCs). Two NDE methods, ultrasonic testing (UT) and infrared (IR) thermography, were used to assess defects and/or damage evolution before and during mechanical testing. Prior to tensile testing, a UTC-scan and a xenon flash method were performed to obtain initial defect information in light of UT C-scans and thermal diffusivity maps, respectively. An IR camera was used for in-situ monitoring of progressive damages. The IR camera measured temperature changes during tensile testing. This paper has presented the feasibility of using NDE techniques to interpret structural performance of CMCs.

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R-Curve Behavior of Silicon Carbide-titanium Carbide Composites

  • An, Hyun-Gu;Kim, Young-Wook
    • 한국세라믹학회지
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    • 제38권12호
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    • pp.1075-1079
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    • 2001
  • The R-curve for in situ-toughened SiC-30 wt% TiC composites was estimated by the indentation-strength method and compared to that of monolithic SiC with toughened microstructure. Both materials exhibited rising R-curve behavior. The SiC-TiC composites, however, displayed better damage tolerance and higher resistance to crack growth. Total volume fractions of SiC key grains, which take part in toughening mechanisms such as crack bridging and crack deflection, were 0.607 for monolithic SiC ceramics and 0.614 for SiC-TiC composites. From the microstructural characterization and the residual stress calculation, it was inferred that this superior performance of SiC-TiC composites can be attributed to stress-induced microcracking at heterophase (SiC/TiC) boundaries and some contribution from carck deflection by TiC grains.

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Preparation and characterization of high transmittance and low resistance index matched transparent conducting oxide coated glass for liquid crystal on silicon panel

  • Jang, Chang-Young;Paik, Woo-Sung;Choi, Bum-Ho;Kim, Young-Back;Lee, Jong-Ho
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2009년도 9th International Meeting on Information Display
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    • pp.1415-1417
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    • 2009
  • High transmittance and low resistance index matched transparent conducting oxide (IMTCO) coated glass was prepared and characterized. IMTCO was deposited by RF magnetron sputtering with the thickness of 15nm and 90nm thick anti-reflection layer was evaporated. To modify surface to hydrophilic, in-situ plasma treatment was also performed. IMTCO coated glass exhibited 96.6% of transmittance in the wavelength range of 400~700nm which is relatively high value compared to commercially available IMTCO glass. The sheet resistance uniformity was measured to be 1.53%.

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기능화된 다중벽 탄소나노튜브 복합재료의 제조 및 물성 평가에 대한 연구 (Manufacturing and Characterization of Nano-composites with Chemically Functionalized Multiwalled Carbon Nanotubes)

  • 박주혁;김태구
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2004년도 춘계학술대회
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    • pp.126-131
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    • 2004
  • Chemically modified multiwalled carbon nanotubes with acids were incorporated into a epoxy matrix by in situ polymerization process, to improve the transfer of mechanical load through chemical bonds, which were demonstrated by infrared spectroscopy. And the mechanical properties of epoxy/carbon nanotube composites were measured to investigate the role of carbon nanotubes. The epoxy/carbon nanotube composites shows higher tensile strength and wear resistance than existing epoxy, with 1 or 2 wt. % addition of functionalized carbon nanotubes. The tensile strength with 7 wt. % carbon nanotibes is increased by a 28% and the wear resistance in exceptionally increased by an outstanding 100 times.

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Drosophila sp.(robusta species group)의 난황 단백질의 분리 및 부분적 화학적 특성 (Isolation and Partial Chemical Characterization of the Yolk Proteins from Drosophila sp. (robusta species group))

  • Kim, Se-Jae;Gi
    • 한국동물학회지
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    • 제35권1호
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    • pp.17-22
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    • 1992
  • The three yolk polypeptides have been isolated and partially characterized. Their molecular weights of YPI, YP2, and YP3 were 48, 000, 47, 000, and 46, 000, respectivelv, as judged by SDS-polyacrvlamide gel electrophoresis. They have different digestion products upon in situ peptide mapping by limited proteolysis. Two-dimensional gel electrophoresis showed that their isoelectric points were heterogeneous from 5.92 to 6.54. And thew showed three different antigen-antibody reactions when each polvpeptides is reacted with antisera made to a mixture of all of three. These data reported here indicate that the yolk proteins are consisted of distinctive polypeptides in Drosophlla sp. (robusta species group).

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크로스홀 형태의 동적 콘 관입기를 이용한 노반의 강성특성 평가 (Stiffness Characterization of Subgrade using Crosshole-Type Dynamic Cone Penetrometer)

  • 홍원택;최찬용;임유진;이종섭
    • 한국지반공학회논문집
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    • 제34권2호
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    • pp.55-63
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    • 2018
  • 열차의 하중을 적절한 강성으로 지지하기 위하여 다짐시공된 노반의 효과적인 강성특성 평가 기법에 대한 연구가 요구된다. 본 연구에서는 상부노반에 대하여 크로스홀 형태의 동적 콘 관입기(CDCP)를 적용함으로써 심도에 따른 강성특성을 평가하고자 하였다. CDCP의 적용을 위하여 세 단면의 다짐시공 완료된 상부노반이 대상 현장으로 선택되었으며, 각각의 개소에 대하여 CDCP 관입실험 및 들밀도시험, 동평판재하시험(LFWD)이 수행되었다. CDCP 관입실험 결과, 심도에 따른 탄성파 발신시간 및 전단파 수신시간을 획득하였으며, 이를 이용하여 노반의 전단파속도 주상도를 획득하였다. 또한, 동일 개소에서 들밀도시험으로부터 획득한 노반의 밀도 및 전단파속도 주상도를 이용하여 심도에 따른 최대전단강성계수($G_{max}$)를 평가할 수 있었다. CDCP 관입실험 및 들밀도시험으로부터 평가된 최대전단강성계수와 LFWD시험으로부터 획득한 동탄성계수($E_{vd}$)를 상호비교한 결과 매우 우수한 선형관계를 보이므로, CDCP 관입실험으로부터 유효한 강성특성을 평가할 수 있을 것이라 판단되었다. 또한, CDCP 관입실험으로부터 도출되는 결과는 일정 심도에 대한 대표 강성특성이 아닌 심도에 따른 연속적인 강성특성 이므로 노반의 강성특성 평가에 효과적으로 이용될 수 있을 것이라 기대된다.

현장 탄성파시험 자료 종합을 통한 국내 지반지층의 대표 전단파속도 제안 (Representative Shear Wave Velocity of Geotechnical Layers by Synthesizing In-situ Seismic Test Data in Korea)

  • 선창국;한진태;조완제
    • 지질공학
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    • 제22권3호
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    • pp.293-307
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    • 2012
  • 지구물리학적 현상을 이해하고 지반공학 관련 문제를 해결하기 위한 주요 요소로서 전단파속도가 강조되어 왔다. 특히, 내진설계와 내진성능평가를 위한 지반지진공학 분야에서 전단파속도의 중요성이 보편적으로 인지되고 있다. 국내 183개소 부지들에서의 다양한 현장 탄성파시험 수행을 통해 대상 조사 부지들에서의 대표적 지반 동적물성으로서의 깊이별 전단파속도 분포들을 결정하였다. 대상 부지들의 지하 토사와 암반 지층을 지반지진공학적 간편 활용을 위한 매립토, 퇴적토, 풍화토, 풍화암 및 기반암의 5 종류 지반지층으로 재분류하였다. 현장 탄성파시험의 전단파속도 분포들을 종합하여 5 종류 지반지층들의 평균적인 전단파속도 주상들을 도출하였으며, 이를 토대로 지진학 및 지반지진공학에서의 유용을 위한 각 지층별 대표 전단파속도 값을 도출하였다.

도파민 수송체의 기능적 특성 및 발현에 관한 연구 (Functional Characterization and Regional Expression of Dopamine Transporter)

  • 이상훈;이송득;성기욱;이동섭;이용성;고재경
    • 약학회지
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    • 제39권2호
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    • pp.161-168
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    • 1995
  • Brain dopamine systems play a central role in the control of movement, hormone release, and many complex behavior. The action of dopamine at its synapse is terminated predominately by high affinity reuptake into presynaptic terminals by dopamine transporter (DAT). The dopamine transporter(DAT) is membrane protein localized to dopamine-containing nerve terminals and closely related with cocaine abuse, Parkinsonism, and schizophrenia. In present study, the recombinant plasmid pRc/CMV-DAT, constructed by subcloning of a cDNA encoding a bovine DAT into eukaryotic expression vector pRc/CMV, was stably transfected into CV-1 cells(monkey kidney cell line). The DAT activities in the cell lines selected by Geneticin$^{R}$ were determined by measuring the uptake of $[^3H]$-dopamine. The transfected cell lines showed 30-50 fold higher activities than untransfected CV-1 cell line, and this result implies that DAT is well expressed and localized in transfected cells. The transfected cells accumulated $[^3H]$-dopamine in a dose-dependent manner with a $K_{m}$ of 991.6nM. Even though high doses of norepinephrine, epinephrine, serotonin, and choline neurotransmitters inhibited the uptake of $[^3H]$-dopamine, DAT in transfected cell line was proven to be much more specific to dopamine. The psychotropic drugs such as GBR12909, CFT, normifensine, clomipramine, desipramine, and imipramine inhibited significantly the dopamine uptake in tissue culture cells stably transfected with DAT cDNA. Radioactive in situ hybridization was done to map the cellular localization of DAT mRNA-containing cells in the adult rat central nervous system. The strong hybridization signals were detected only in the substantia nigra pars compacta and ventral tegmental area. The restricted anatomical localization of DAT mRNA-containing cells confirms the DAT as a presynaptic marker of dopamine-containing cells in the rat brain.

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