• 제목/요약/키워드: ICP-OES

검색결과 200건 처리시간 0.029초

Korean solar salts reduce obesity and alter its related markers in diet-induced obese mice

  • Ju, Jaehyun;Song, Jia-Le;Park, Eui-Seong;Do, Myoung-Sool;Park, Kun-Young
    • Nutrition Research and Practice
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    • 제10권6호
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    • pp.629-634
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    • 2016
  • BACKGROUND/OBJECTIVE: The aim of this experiments was to show anti-obesity effects of Korean solar salt from different salt fields in diet-induced obese mice. MATERIALS/METHODS: Diet-induced obesity (DIO) was induced by a high-fat diet (HFD; 45% cal from fat) in C57BL/6J mice for eight weeks. The mice were fed with the designated diets (chow diet for Normal, HFD for Control, 0.47%-salt-mixed HFD for purified salt (PS), Guerande solar salt from France (SS-G), solar salt from Y salt field (SS-Y), solar salts from T salt field (SS-T) and S salt field (SS-S)) for another eight weeks. We checked body weight, food efficiency ratio (FER) and tissue weights (liver and epididymal adipose tissue (EAT)), and observed serum concentrations of triacylglycerol (TG), total cholesterol (TC), leptin and insulin. We also evaluated gene expressions of adipogenic / lipogenic mRNAs of $C/EBP{\alpha}$, $PPAR{\gamma}$ and FAS and beta-oxidation-related factors ($PPAR{\alpha}$ and CPT-1) in liver and EAT. The mineral composition of salt samples were analyzed using inductively coupled plasma optical emission spectrometry (ICP-OES). RESULTS: SS-T and SS-S significantly reduced body weight gain, FER, and weight of EAT compared to control and other samples (P < 0.05). SS-T and SS-S also significantly decreased serum levels of TG, TC, leptin and insulin (P < 0.05). SS-T and SS-S suppressed expressions of adipogenic / lipogenic mRNAs in liver and EAT, while promoting expression of beta-oxidation-related factors. The lowest sodium concentration was observed in SS-T ($30.30{\pm}0.59%$), and the lowest sodium-to-potassium (Na/K) ratio was found in SS-S (17.81). CONCLUSIONS: Our study shows that well-processed Korean solar salt may have anti-obesity effects in vivo, probably owing to its differences in mineral composition and other components, presumably resulting from the manufacturing processes. Further research is needed into the mechanism and to explore optimal manufacturing processes.

Investigation on Translocation of De-icing Salts influenced by the Intensity of Foliar Damage of Roadside Trees in Chung-ju City (충주시 가로수의 황변정도에 따른 토양 내 제설제 성분의 흡수이행성 평가)

  • Kim, Jae-Young;Kim, Won-Tae;Yoon, Young-Han;Ju, Jin-Hee
    • Journal of the Korean Society of Environmental Restoration Technology
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    • 제21권4호
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    • pp.1-10
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    • 2018
  • Use of de-icing salts results in accumulation of high concentrations of ions on roadside soils and tree. The purpose of this study isto determine translocation of seasonal impact of exchangeable cations originating from de-icing salt on roadside surface soil-plant influenced by the intensity of foliar damage (NY = 0-25%, SY = 26-50%, CY = 51-75%) of trees. This paper investigated the concentration of four exchangeable cations ($K^+$, $Ca^{2+}$, $Na^+$, and $Mg^{2+}$) on the roadside surface soil. The tree (Ginko biloba) samples were collected from the Konkuk and Judeok intersections in Chung-ju city. The sequential extraction procedure was applied to 120 soil samples of the soilsurface and 30 tree samples. Four cation exchange ions were determined by ICP-OES. The content of four exchangeable cations present on roadside soil was found to be the lowest in NY but highest in CY from tree pits in the order of NY < SY < CY. Especially, the results were apparent during spring time compared to other seasons. Soil collected from tree pits had the highest concentration of $Ca^{2+}$ possibly due to a higher volume of traffic on those streetsresulting in splashing of more calcium chloride ($CaCl_2$). The analysis of three exchangeable cations ($K^+$, $Mg^{2+}$, and $Na^+$) in the tree leaves revealed higher levels than roadside surface soil when foliar damage ratio increased in the order of NY < SY < CY in summer. In addition, a strong positive linear relationship was observed between the concentration of exchangeable cations in soil and trees. It is hypothesized that the results of this study can be a valuable baseline for managing de-icing salt on roadside soil and trees, in order to mitigate the salt stress that can damage the roadside soil and trees.

Investigation of Heavy Metal Contents by Milling Degrees of Rice (쌀의 도정도에 따른 중금속 함량 변화)

  • Kim, Jin-Kug;Lee, Ji-Hwan;Kim, Ji-Eun;Bae, In-Ae;Kim, Kwang-Seon;Lee, Eun-Suk;Kwon, Soon-Duck;Park, Ju-Hwan;Lee, Kyu-Seung
    • Korean Journal of Environmental Agriculture
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    • 제34권4호
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    • pp.303-308
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    • 2015
  • BACKGROUND: Recently, various rice by milling degree is sold for health and taste. To provide safe food to consumers, it is need to know the change of heavy metal contents according to milling degree of rice.METHODS AND RESULTS: This study was to investigate residual the levels of cadmium (Cd), lead (Pb), copper (Cu) and zinc (Zn) as stated in the milling degree of the rice contaminated Cd and Pb from 2011 to 2012 in Chungcheongnam-do. Rice samples exceeded the maximum residue limits (MRL) of Cd and Pb were milled by five degrees (0.0, 2.45, 8.02, 10.48, 15.09%). Milled rice was digested by microwave method, and analyzed heavy metal contents using ICP-OES. Recovery ratios of 4 heavy metals such as Cd, Pb, Cu and Zn were ranged for 79.7-98.9%, and limits of detection (LOD) and limits of quantitation (LOQ) were fulfilled with the normal analytical standards. Concentrations of Cd, Pb, Cu and Zn were ranged 0.416-0.433 mg/kg, 0.183-0.26 mg/kg, 3.639- 3.882 mg/kg and 16.868-19.801 mg/kg, respectively.CONCLUSION: From these results, conforming with increase of milling degree of rice, Cd, Pb, Cu, and Zn contents tended to decrease. The contents of heavy metals were decreased 3.1% in Cd, 29.3% in Pb, 6.4% in Cu and 15.1% in Zn, in according to the highest milling degree of 15.09%.

Study on the Copper Electro-refining from Copper Containing Sludge (저품위 동(Cu) 함유 슬러지로부터 동 전해정련에 관한 연구)

  • Lee, Jin-Yeon;Son, Seong Ho;Park, Sung Cheol;Jung, Yeon Jae;Kim, Yong Hwan;Han, Chul Woong;Lee, Man-seung;Lee, Ki-Woong
    • Resources Recycling
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    • 제26권6호
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    • pp.84-90
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    • 2017
  • The electro-refining process was performed to recovery high purity copper from low grade copper containing sludge in sulfuric acid. The surface morphologies and roughness of electro-refining copper were analyzed with variation of the type and concentration of organic additives, the best surface morphology was obtained 5 ppm of the gelatin type and 5 to 10 ppm of the thiol type organic additive. The crude metal consisted of copper with 86.635, 94.969 and 99.917 wt.%, several impurity metals of iron, nickel, cobalt and tin by pyro-metallurgical process. After electro-refining process, the purity of copper increases to 3N or 4N grade. The impurity concentrations and copper purities of copper crude metals, electrolyte and electro-refining copper were analyzed using ICP-OES, the electro-refining time and purity of copper crude metal to recover 4N grade copper were deduced.

Analytical Method to Quantify Sodium Metasilicate in Shark Fins (샥스핀 가공 중 사용된 메타규산나트륨 분석)

  • Park, Se-Jong;Jang, Su-Jin;Choi, Jae-Chon;Kim, Meehye
    • Korean Journal of Food Science and Technology
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    • 제47권2호
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    • pp.145-148
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    • 2015
  • According to the Korea Food Additives Code, sodium metasilicate is permitted for use as a filtering agent for edible oils and fats. Sodium metasilicate is currently used as a food additives to increase the weight of shark fins. In this study, we developed an analytical method to quantify sodium metasilicate in food. Sodium metasilicate content was estimated by measuring the moisture content, pH and silicon content of shark fins. Silicon content was analyzed using inductively coupled plasma-optical emission spectrometry (ICP-OES) following microwave-assisted digestion with $HNO_3$ (65%) and $H_2O_2$ (30%). Shark fin total silicon content was $7.17{\pm}8.92mg/kg$, while the soluble silicon content was $2.34{\pm}3.80mg/kg$. After soaking raw shark fin in an aqueous solution of sodium metasilicate, fin weight, pH and silicon content were measured. These results would be used as the basic information for shark fins safety management.

Model Development for Estimating Total Soil Contents of Pb and Cd Using Chemical Properties and Extractable Contents in Paddy Soil (논 토양의 이화학적 특성 및 침출성 함량을 이용한 납과 카드뮴의 전함량 예측 모형식 개발)

  • Go, Woo-Ri;Lee, Ji-Ho;Lee, Eun-Yong;Lim, Seong-Mook;Yoo, Ji-Hyock;Kim, Ji-Young;Kim, Kye-Hoon;Im, Geon-Jae;Kim, Won-Il
    • Korean Journal of Soil Science and Fertilizer
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    • 제44권6호
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    • pp.1080-1084
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    • 2011
  • Predictive model for estimating total contents of cadmium (Cd) and lead (Pb) was developed by stepwise multiple-regression analysis using chemical properties and extractable contents of metal in paddy soil adjacent to abandoned mines in 2009 and 2010. Soil properties, e.g. pH, electrical conductivity (EC), organic matter (OM), available phosphorus ($P_2O_5$), and exchangeable cations (i.e. Ca, Na, K, Mg) were measured. Total contents of Cd and Pb as well as extractable contents of metals were analyzed by ICP-OES. Results showed that the total and extractable contents were estimated to be 3.55 and $0.27mg\;kg^{-1}$ in Cd and 83.38 and $24.32mg\;kg^{-1}$ in Pb on the average. From stepwise analysis, it was found that the contents of extractable Cd, Zn, Cu, as well as exchangeable Na were significantly influenced on estimation of the total contents of Cd in soil. Moreover, it also showed that the contents of extractable Pb, Zn, and Cu significantly affected estimation of the total contents of Pb in soil. More significant relationship between estimated and measured value in total contents of Pb was observed than those of Cd ($R^2$=0.87, p<0.0001). This demonstrates that extractable contents of metal are influenced more on estimation of total contents of Cd and Pb in soil than soil properties.

Mineral Components of Water Supply Plants and Spring Waters in Northern Gyeonggi Area (경기북부지역 정수장 및 약수터의 미네랄 성분 분포 연구)

  • Song, Hee-Il;Lim, Han-Su;Park, Gyoung-Su;Park, Hyun-Goo;Lee, Hyun-Jin;Jo, Mi-Hyun;Kim, Young-Yeon;Oh, Jo-Gyo
    • Journal of Environmental Health Sciences
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    • 제45권3호
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    • pp.238-246
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    • 2019
  • Objective: The purpose of this study was to investigate the distribution of mineral components, health and taste index for water supply plants, spring water located in northern Gyeonggi area and bottled waters in market to analyze Ca, K, Mg Na, Si, $F^-$ and $SO_4{^{2-}}$. Method: The samples were source and tap water in 15 water supply plants over 9 river basin, 172 spring water and 20 bottled water. The Ca, K, Mg Na and Si were analyzed by ICP-OES. The $F^-$ and $SO_4{^{2-}}$ were determined by Ion Chromatograph. Then, taste and health index were calculated using Hashimoto equation. Results: The average concentration of major minerals showed in same order of Ca > Na > Mg > K for all kinds of drinking water from water supply plants, spring waters and bottled waters. Total concentration of major minerals (Ca, K, Mg, Na) was calculated that showed 26.79 mg/L of tap water, 21.81 mg/L of spring water, 32.94 mg/L of bottled water on average. So, the spring waters indicated the lowest minerals sum. The tap water from water supply plants was categorized to Group I, II for 33.3, 44.4% according to K-index and O-index. Otherwise, spring water was classified as Group I, II for 44.0, 46.3%. Conclusion: According to the results of K and O-index, water from water supply plant showed higher K-index which means good for the health. Otherwise, spring water indicated higher O-index that people can feel more delicious than tap water. Futhermore, the mineral distribution of source water from water supply plants and spring water had indicated high correlation with geological effect.

Human Risk Assessment for Exposure to Heavy Metals within Finishing Materials of Playground Facilities for Children in Gwangju (광주지역 어린이 놀이시설 마감재의 중금속 노출에 의한 인체 위해성평가)

  • Sang-Hoon Yoon;So-Young Kim;Eun Cho;Tae-Hui Nam;Jin-Hwan Park;Hwa-Jin Kong;Ki-Won Lee;Gwang-Yeob Seo;Jeong-Hun Park;Kyoung-Woo Min
    • Journal of Environmental Health Sciences
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    • 제50권2호
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    • pp.146-156
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    • 2024
  • Background: Children who use playground facilities are exposed to potential risks due to the high concentration of heavy metals contained in the finishing materials of facilities in children's playgrounds. Objectives: The purpose of this study was to investigate the concentration of heavy metals in the finishing materials of outdoor children's playgrounds where harmful heavy metals exist in Gwangju and to conduct human risk assessment for children and adults by age to find the risks and limitations. Methods: The bottom and top layers of double-painted paint were peeled off and collected together from the finishing materials of children's play facilities such as slides, swings, and seesaws in 147 children's parks in Gwangju. Heavy metals were analyzed using ICP-OES, etc., and human risk assessment was performed using the concentrations of heavy metals. Results: Based on 1.0E-04, which requires legal regulation, CTE was found to pose a carcinogenic risk for preschool children and no carcinogenic risk for the rest of the age groups. However, RME showed that both men and women of all ages had a carcinogenic risk. For reference, when the carcinogenic risk was based on 1.0E-06, CTE was found to pose a carcinogenic risk from infants to elementary school students, and RME was found to have a carcinogenic risk in all age groups. It was judged that there is a non-carcinogenic risk if the non-carcinogenic risk exceeds 1 based on the hazard index (HI) 1. In CTE, there was no non-carcinogenic risk, and RME for preschooler males (1.49E+00) and females (1.56E+00) were found to have non-carcinogenic risk. Conclusions: This study was meaningful in that it examines the differences in the current management of heavy metals concentration standards and potential carcinogenic and non-carcinogenic risks to the human body and discusses the relationship between heavy metals and human health effects.

Evaluation of Mineral Content in Convenience Baby Food (간편 이유식의 무기질 함량 평가)

  • Cho, Young-Sun;Kim, Ki-Cheol;Shin, Sang-Woon;Sung, Jin-Hee;Kim, Ji-Eun;Baek, Eun-Jin;Lee, Eun-Bin;Kim, Hye-Jin;Park, Yong-Bae;Yun, Mi-Hye
    • Journal of Food Hygiene and Safety
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    • 제35권5호
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    • pp.489-494
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    • 2020
  • A total of 101 samples of convenience baby food products were analyzed by microwave digestion and mineral nutrients (iron, zinc, calcium, magnesium) were determined by inductively coupled plasma optical emission spectroscopy (ICP-OES). By type, the samples included 44 rice porridges, 40 soft-boiled rices, 11 purees, and 6 powders. The mean values for iron (Fe) content were 0.05 to 0.45 mg/100 g (excepted powder type, mg/l0 g). This was equivalent to 22.35% for rice porridge, 10.55% for soft-boiled rice, 9.88% for puree and 2.74% for powder type compared to the KDRIs (Dietary Reference Intakes for Koreans), respectively. The mean values for zinc (Zn) was 0.06 to 0.28 mg/100 g (excepted powder type, mg/l0 g) and the KDRI ratio was the lowest at 5.94% in puree, with 27.76%, 28.95% and 10.91% in rice porridge, soft-boiled rice and powder type, respectively. Calcium (Ca) content relative to KDRIs was relatively low compared to other minerals, with 6.65% for rice porridge, 3.61% for soft-boiled rice, 6.24% for puree and 3.07% for powder type, respectively. The magnesium (Mg) content of baby food ranged from 13.4% to 39.0% compared to KDRIs, and was included in all baby food as a whole. For balanced nutritional mineral supply to infants, it is recommended that information on mineral sources and ingredients in convenience baby food be clearly provided to ensure proper growth and development.

A Study on the Content of Minerals in Fortified Food (영양강화식품 중 무기질 함량 조사연구)

  • Kim, Myeong-Gil;Kim, Young-Sug;Kim, Young-Su;Lee, Seong-Bong;Ryu, Kyong-Shin;Yoon, Mi-Hye;Lee, Jong-Bok
    • Journal of Food Hygiene and Safety
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    • 제29권2호
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    • pp.99-104
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    • 2014
  • This study was done to analyze the contents of minerals and to investigate the ratio of measured values to labeled values and to analyze the ratio of calcium to other minerals in 68 specimen with minerals - fortified commercial beverages, noodles, cereals and grain products. Content of calcium, iron and zinc in samples after microwave digestion was analyzed with an ICP-OES. The measured values of calcium were ranged 82.2~293.1% of the labeled values in 38 samples composed calcium - fortified commercial beverages, noodles, cereals and grain products. The measured values of iron and zinc were ranged 83.3~301.0%, 90.1~314.1% of the labeled values in minerals - fortified commercial beverages, noodles, cereals and grain products, 42, 24 samples. The Ca : Fe ratios were 90.55 (50.55~220.64) in fruit & vegetable juice, 850.41 in fruit & vegetable beverage, 553.49 in blended beverage, 179.07 (118.37~238.01) in soy milk, 204.39(41.64~397.52) in noodle, 296.97(121.64~868.88) in fried noodle, 30.89(15.69~62.05) in cereal and 7.73(0.22~49.92) in grain product. The Ca : P ratios were 1.44(0.96~1.98) in fruit & vegetable juice, 1.92 in fruit & vegetable beverage, 1.66 in blended beverage, 4.23(2.25~7.72) in soy milk, 1.14(0.28~1.97) in noodle, 1.88(1.17~2.42) in fried noodle, 1.29(0.87~2.92) in cereal and 0.30(0.06~1.57) in grain product. The Ca : Mg ratios were 1.85(0.87~5.04) in fruit & vegetable juice, 28.72 in fruit & vegetable beverage, 2.97 in blended beverage, 5.27(2.93~9.36) in soy milk, 3.97(1.34~7.57) in noodle, 6.77(4.63~10.78) in fried noodle, 4.40(2.30~12.55) in cereal and 1.17(0.23~7.48) in grain product. These results suggest calcium contents and the ratio of calcium contents to other minerals in calcium-fortified food products should be strictly controlled. Moreover, to avoid problems with Excessive nutrition, there must be initiatives for better understanding on food labelling and nutrition for fortified food.