• 제목/요약/키워드: Hyrothermal Synthesis

검색결과 1건 처리시간 0.013초

열처리 시간에 따른 중적외선 투과 ZnS 세라믹의 합성과 특성 (Synthesis and Characterization of Middle Infrared Transmission ZnS Ceramics by Heat Treatment Time)

  • 권태형;여서영;박창순;김창일;홍연우;백종후
    • 센서학회지
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    • 제26권5호
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    • pp.360-365
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    • 2017
  • In this study, a heat treatment process was applied to ZnS nano-powder to improve the optical properties of ZnS ceramic, and the characteristics of heat treatment time were studied. The ZnS nano-powders were synthesized by hydrothermal synthesis. The heat treatment was carried out at $550^{\circ}C$ for 0.5, 1, 2, and 4 hours in a vacuum atmosphere ($10^{-2}torr$). X-ray diffraction and scanning electron microscope analyzes confirmed the change of crystal phase and grain size to confirm the structural change with heat treatment time. The heat treated ZnS nano-powder was sintered by hot pressing, and the change of optical properties of the ZnS ceramic was analyzed by infrared spectroscopy.