• Title/Summary/Keyword: Hydrogen/Air Diffusion Flame

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Particle Characteristics of Flame-Synthesized γ-Al2O3 Nanoparticles (화염법으로 제조된 감마-Al2O3 나노입자의 화염조건에 따른 입자특성 연구)

  • Lee, Gyo-Woo
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.36 no.5
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    • pp.509-515
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    • 2012
  • In this study, ${\gamma}-Al_2O_3$ nanoparticles were synthesized by using coflow hydrogen diffusion flames. The synthesis conditions were varied with using several oxygen concentrations in the oxidizing air. The particle characteristics of the flame-synthesized $Al_2O_3$ nanoparticles were determined by examining the crystalline structure, shape, and specific surface area of the nanoparticles. The measured maximum centerline temperature of the flames ranged from 1507.8 K to 1998.7 K. The morphology and crystal structure of the $Al_2O_3$ nanoparticles were determined from SEM images and XRD analyses, respectively. The particle sizes were calculated from measured BET specific surface areas and ranged from 25 nm to 52 nm. From XRD analyses, it was inferred that a large number of the synthesized nanoparticles were ${\gamma}-Al_2O_3$ nanoparticles including ${\theta}-Al_2O_3$ nanoparticles.