• 제목/요약/키워드: Hot solution method

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Sol-Gel법에 의한 Pb($Zr_{0.52}Ti_{0.48}$)$O_3$박막의 유전 및 전기적 특성 (Dielectric and Electrical Properties of the Pb($Zr_{0.52}Ti_{0.48}$)$O_3$ Thin Film by Sol-Gel Method.)

  • 정장호;류기원;배선기;이영희
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1995년도 춘계학술대회 논문집
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    • pp.14-16
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    • 1995
  • Pb($Zr_{0.52}Ti_{0.48}$)$O_3$ ceramic thin films were fabricated from an alkoxide-based solution by Sol-Gel method. Pb($Zr_{0.52}Ti_{0.48}$)$O_3$ co-ramic thin films were formed by spin coating method on Pt/$SiO_2$/Si substrate at 4000[rpm] for 30 [sec]. Coated specimens were dried on the hot-plate at 400[$^{\circ}C$] for 10[min]. The coating process was repeated 6 times and then sintered at temperature between 500 ~ 800[$^{\circ}C$] for 1 hour. The ferroelectric perovskite phases precipitated under the sintering of 700[$^{\circ}C$] for 1 hour. Pb($Zr_{0.52}Ti_{0.48}$)$O_3$ thin film sintered at 700[$^{\circ}C$] for 1hour showed good dielectric constant (2133) and dielectric loss (2.2[%]) Properties. The switching voltage, switching time and leakage currents density were 3.0[V], 1.7[${\mu}$sec] , 160[pA/$\textrm{cm}^2$] repectively.

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Sol-Gel법으로 제조한 PLT박막의 초전 특성 (Pyroelectric Properties of the PLT Thin Films Prepared by Sol-Gel Method)

  • 김양선;정장호;박인길;이성갑;이영희
    • E2M - 전기 전자와 첨단 소재
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    • 제10권6호
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    • pp.541-547
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    • 1997
  • (Pb$_{1-x}$ La$_{x}$)Ti$_{1-x}$ $_4$O$_3$(x=0, 0.02, 0.04, 0.08) ceramic thin films were fabricated by Sol-Gel method. A stock solution of (Pb, La)TiO$_3$ with excess Pb 10 mol% was made and spin-coated on the Pt/Ti/SiO$_2$/Si substrate at 400rpm for 30 seconds. Coated specimens were dried on the hot-plate at 35$0^{\circ}C$ for 10 min and sintered at 500~75$0^{\circ}C$ for 1 hour. The dielectric constant, remanent polarization and coercive field of the PLT(6at.%) thin films sintered at $650^{\circ}C$ were 884, 13.95$\mu$C/$\textrm{cm}^2$ and 8.7kV/cm, respectively. Pyroelectric coefficient, figure of merit of pyroelectric current, voltage responsivity and detectivity of PLT(6at.%) thin films were 3.2$\times$10$^{-8}$ C/$\textrm{cm}^2$K, 1.02$\times$10$^{-8}$ C.cm/J, 2.9 $\times$10$^{-11}$ C.cm/J, 0.29$\times$10$^{-8}$ C.cm/J, respectively.ely.

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슈퍼픽셀 DBSCAN 군집 알고리즘을 이용한 용융아연도금 강판의 부식이미지 분석 (Corrosion image analysis on galvanized steel by using superpixel DBSCAN clustering algorithm)

  • 김범수;김연원;이경황;양정현
    • 한국표면공학회지
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    • 제55권3호
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    • pp.164-172
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    • 2022
  • Hot-dip galvanized steel(GI) is widely used throughout the industry as a corrosion resistance material. Corrosion of steel is a common phenomenon that results in the gradual degradation under various environmental conditions. Corrosion monitoring is to track the degradation progress for a long time. Corrosion on steel plate appears as discoloration and any irregularities on the surface. This study developed a quantitative evaluation method of the rust formed on GI steel plate using a superpixel-based DBSCAN clustering method and k-means clustering from the corroded area in a given image. The superpixel-based DBSCAN clustering method decrease computational costs, reaching automatic segmentation. The image color of the rusty surface was analyzed quantitatively based on HSV(Hue, Saturation, Value) color space. In addition, two segmentation methods are compared for the particular spatial region using their histograms.

벼 키다리병 방제에 관한 황토유황의 종자소독 효과 (Effect of Rice Seed Disinfection of Loess-sulfur on the Suppression of Bakanae disease caused by Fusarium fujikuroi)

  • 소현규;김용기;홍성준;한은정;박종호;심창기;김민정;김석철
    • 한국유기농업학회지
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    • 제25권2호
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    • pp.345-355
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    • 2017
  • 본 연구는 황토유황을 활용하여 벼 키다리병 발병을 최소화할 수 있는 최적 종자소독조건을 선발하기 위해 수행되었다. 키다리병에 이병된 '신동진' 품종 벼 종자를 공시하였고 황토유황 농도, 침지온도, 시간, 온탕여부를 구분하여 실내 및 온실검정을 통해 침지시간은 48시간, 침지농도는 1%로 최적 소독조건을 선발하였다. 그리고 모판과 포장시험을 수행하여 온탕처리 후 $20^{\circ}C$, 1% 황토유황에 48시간 침지 처리구와 $30^{\circ}C$, 1% 황토유황에 48시간 단독 침지할 때 가장 효과가 높았다는 것을 확인하였고 위 처리조건으로 소독한 종자가 육묘, 이앙, 출수기를 거치면서도 100%의 높은 방제효과가 유지되는 것을 확인할 수 있었다. 그러나 $20^{\circ}C$에서 1% 황토유황으로 침지한 처리구에서는 포장에서 78.2%의 낮은 방제가를 보였다. 또한, 온탕소독만 수행한 처리구에서도 $60^{\circ}C$, 10분간 충실히 수행될 경우 효과적인 벼 키다리병 방제가 가능함을 보여주었지만 온탕처리 후 황토유황으로 추가 침지함으로서 많은 양의 종자를 소독할 때 좀 더 나은 키다리병 방제 효과를 가져다 줄 수 있을 것으로 판단된다. 이상의 결과를 종합하여 볼 때 농가에서 온탕소독기와 종자소독기 둘 중 한가지만 구비하더라도 황토유황을 이용하여 충분한 소독효과를 낼 수 있기 때문에 현장에서 보다 쉽게 활용될 수 있을 것으로 판단되며 제조방법이 쉽고 비용이 적게 드는 황토유황의 특성상 농가의 경영비 절감효과도 클 것으로 기대된다.

부분 체적 효과에서 회복 계수를 이용한 보정 전과 후 SUV의 비교 분석 (A Comparative Analysis of Standard Uptake Value Using the Recovery Coefficient Before and After Correcting Partial Volume Effect)

  • 고현수;박순기;최재민;김정선;정우영
    • 핵의학기술
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    • 제15권1호
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    • pp.10-16
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    • 2011
  • 추적 검사에서의 PET/CT 재구성 영상은 추적자의 분포를 균일하고 정확하게 표현하여야 일관된 정량분석 값을 제공 할 수 있을 것이다. 그러나 PET/CT 장비의 제한된 공간분해능 때문에 발생하는 부분 체적 효과(Partial Volume Effect: PVE)로 인해 관심영역의 방사능 농도가 실제의 값보다 낮게 측정될 가능성이 있고, 따라서 관심부위의 SUV가 실제 값보다 낮게 측정 될 가능성이 있다. 본 연구에서는 PET/CT 스캐너의 PVE를 보정하는 회복계수(Recovery Coefficient: RC)를 팬텀 실험을 통해 산출하고, 실제 PET/CT 검사 자료에 적용하여 보정 전과 후 SUV를 비교 분석 하고자 한다. ACR phantom을 이용하여 1000 mL의 증류수에 20.72 MBq (0.56 mCi)을 균일하게 희석하고 열소 원통 (hot cylinder-2.5, 1.6, 1.2, 0.8 cm in diameter)에 주입하였다. 또한 6440 ml의 증류수에 33.30 MBq (0.90 mCi), 22.20 MBq (0.60 mCi), 16.65 MBq (0.45mCi)을 균일하게 희석하고 배후 방사능을 채워 열소 원통과 배후방사능이 각각 4:1, 6:1, 8:1 (Hot/Background ratio: H/B ratio)이 되도록 만들어 3회 반복 실험하였다. 서울아산병원의 Biograph Truepoint 40 (SIEMENS, Germany) 장비로 whole body protocol을 사용하여 phantom 실험 및 환자 검사를 시행하였다. 2010년 7월부터 8월까지 서울아산병원에서 PET/CT 검사 후 폐암으로 판정 받은 환자 30명을 대상으로, 본 연구의 결과에서 산출된 RC를 적용하여 PVE 보정 전과 후 SUV를 비교 분석하였다. 열소 원통과 배후방사능이 4:1일 때 2.5, 1.6, 1.2, 0.8 cm 에서의 RC는 각각 0.75, 0.72, 0.40, 0.27이었고, 6:1일 때 0.74, 0.59, 0.55, 0.43이었으며, 8:1일 때 0.77, 0.76, 0.58, 0.42로 열소 영역의 크기가 작아질수록 RC가 감소하였다. 폐암으로 판정 받은 환자 중에서 30명의 환자를 무작위 표본 추출하여 보정 전과 후의 SUV 최대값을 비교 분석 한 결과, 보정 전 평균은 7.83이었고 보정 후 평균은 10.31이었다. 또한 보정 전과 후의 SUV 최대값을 대응 표본 t 검정으로 차이를 분석한 결과, 통계적으로 유의한 차이가 있었다(t=7.21, p=0.000). PVE에 의해서 과소 평가 되었던 보정 전의 SUV가 보정 후에는 증가되는 것을 확인할 수 있었다. 병변의 크기와 H/B ratio가 환자마다 제각기 다른 값을 갖기 때문에, RC를 사용하여 PVE를 보정한 SUV가 정확한 값이라고 판단하기는 어려우나 PVE에 의해 감소된 SUV를 실제 값과 유사하게 보정할 수 있는 방법일 것으로 생각된다.

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Diamond Crystal Growth Behavior by Hot Filament Chemical Vapor Deposition According to Pretreatment Conditions

  • Song, Chang Weon;You, Mi Young;Lee, Damin;Mun, Hyoung Seok;Kim, Seohan;Song, Pung Keun
    • 한국표면공학회지
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    • 제53권5호
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    • pp.241-248
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    • 2020
  • The change of the deposition behavior of diamond through a pretreatment process of the base metal prior to diamond deposition using HFCVD was investigated. To improve the specific surface area of the base material, sanding was performed using sandblasting first, and chemical etching treatment was performed to further improve the uniform specific surface area. Chemical etching was performed by immersing the base material in HCl solutions with various etching time. Thereafter, seeding was performed by immersing the sanded and etched base material in a diamond seeding solution. Diamond deposition according to all pretreatment conditions was performed under the same conditions. Methane was used as the carbon source and hydrogen was used as the reaction gas. The most optimal conditions were found by analyzing the improvement of the specific surface area and uniformity, and the optimal diamond seeding solution concentration and immersion time were also obtained for the diamond particle seeding method. As a result, the sandblasted base material was immersed in 20% HCl for 60 minutes at 100 ℃ and chemically etched, and then immersed in a diamond seeding solution of 5 g/L and seeded using ultrasonic waves for 30 minutes. It was possible to obtain optimized economical diamond film growth rates.

Sol-Gel법에 의한 Pb(Zr,Ti)$O_3$ 박막의 제조 및 유전 특성 (Preparation and Dielectric properties of the Pb(Zr,Ti)$O_3$ Thin Film by Sol-Gel Method)

  • 정장호;박인길;류기원;이성갑;이영희
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1995년도 하계학술대회 논문집 C
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    • pp.1022-1024
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    • 1995
  • In this study, $Pb(Zr_xTi_{1-x})O_3$(x=0.65, 0.52, 0.35) thin films were fabricated by Sol-Gel method. A stock solution with excess Pb 10[mol.%] of $Pb(Zr_xTi_{1-x})O_3$ was made and spin-coated on the Pt/$SiO_2$/Si substrate at 4000[rpm] for 30[sec.]. Coated specimens were dried on the hot-plate at $400[^{\circ}C]$ for 10[min.]. Sintering temperature and time were $500{\sim}800[^{\circ}C]$ and $1{\sim}60$[min.]. To investigate crystallization condition, PZT thin films were analyzed with sintering temperature, time and composition by the XRD. The microstructure of thin films were investigated by SEM. The ferroelectric perovskite phases precipitated under the sintering of $700[^{\circ}C]$ for 1 hour. In the PZT(52/48) composition, dielectric constant and dielectric loss were 2133, 2.2[%] at room temperature, respectively.

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이중으로 경사진 3차원 캐비티내 자연대류 열전달 특성에 관한 수치해석적 연구 (Numerical Investigation on Heat Transfer Characteristics for Natural Convection Flows in a Doubly-Inclined Cubical-Cavity)

  • 명현국
    • 대한기계학회논문집B
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    • 제33권6호
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    • pp.435-442
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    • 2009
  • Three-dimensional heat transfer characteristics for natural convection flows are numerically investigated in the doubly-inclined cubical-cavity according to the variation of a newly defined orientation angle �� of the hot wall surface from horizontal plane at moderate Rayleigh numbers. Numerical simulations of laminar flows are conducted in the range of Rayleigh numbers($10^4{\leq}Ra{\leq}10^5$) and $0^{\circ}{\leq}{\alpha}90^{circ}$ with a solution code(PowerCFD) employing unstructured cell-centered method. Comparisons of the average Nusselt number at the cold face are made with benchmark solutions and experimental results found in the literature. It is found that the average Nusselt number at the cold wall has a maximum value around the specified orientation ${\alpha}$ at each Rayleigh number. Special attention is also paid to three-dimensional thermal characteristics in natural convection according to new orientation angles at Ra��= $1{\times}10^5$, in order to investigate a new additional heat transfer characteristic found in the range of above Ra = $6{\times}10^4$.

의사공진형 Hybrid IC STR-G9600을 이용한 저 노이즈 역률 개선형 전원 장치 (An Improved PFC & Low Noise Power Supply using Quasi-Resonant Mode Hybrid IC of STR-G9600)

  • 이명준;안준영;신호준;배준성
    • 전력전자학회:학술대회논문집
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    • 전력전자학회 2002년도 전력전자학술대회 논문집
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    • pp.233-236
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    • 2002
  • The solution for PFC(Power Factor Correction), as a regulation in energy Policy, is becoming a hot Issue in every country because of the shortage of electrical energy. Therefore, a new improved idea for PFC problem has been introduced in this study. A lot of merits, effective cost by simple circuit, reduced PCB size, lighter than reactor in the view of weight, lower level of screen noise by leakage inductance in CTV applications, have been stated by comparing to the earlier method of using a Reactor. All test results in this statement were done by using a power device of STR-G9600 series based on the real load condition of color television. furthermore, the study shows that the test results also meets the IEC-1000-3-2 class D, which regulates the PFC when input power of a set is more than 75watts. More improved PFC in other applications hopes to be implemented by using the proposed method.

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Condensable InP Quantum Dot Solids

  • Tung, Dao Duy;Dung, Mai Xuan;Jeong, Hyun-Dam
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2012년도 제42회 동계 정기 학술대회 초록집
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    • pp.541-541
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    • 2012
  • InP quantum dots capped by myristic acid (InP-MA QDs) were synthesized by a typical hot injection method using MA as stablizing agent. The current density across the InP-MA QDs thin film which was fabricated by spin-coating method is about $10^{-4}A/cm^2$ at the electric field of 0.1 MV/cm from I-V measurement on a metal-insulator-metal (MIM) device. The low conductivity of the InP-MA QDs thin film is interpreted as due to the long interdistances among the dots governed by the MA molecules. Therefore, replacing the MA with thioacetic acid (TAA) by biphasic ligand exchange was conducted in order to obtain TAA capped InP QDs (InP-TAA). InP-TAA QDs were designed due to: 1) the TAA is very short molecule; 2) the thiolate groups on the surface of the InP-TAA QDs are expected to undergo condensation reaction upon thermal annealing which connects the QDs within the QD thin film through a very short linker -S-; and 3) TAA provides better passivation to the QDs both in the solution and thin film states which minimizing the effect of surface trapping states.

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