• Journal of Powder Materials
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• v.9 no.6
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• pp.381-393
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• 2002

Recent developments in nanocrystalline and nanocomposite rare earth-transition metal magnets are reviewed and emphasis is placed on research work at IFW Dresden. Principal synthesis methods include high energy ball milling, melt spinning, mold casting and hydrogen assisted methods such as reactive milling and hydrogenation-disproportionation-desorption-recombination. These techniques are applied to NdFeB-, PrFeB- and SmCo-type systems with the aim to produce high remanence magnets with high coercivity. Concepts of maximizing the energy density in nanostructured magnets by either inducing a texture via anisotropic HDDR or hot deformation or enhancing the remanence via magnetic exchange coupling are evaluated. With respect to high temperature applications melt spun $Sm(Co_{0.74}Fe_{0.1}Cu_{0.12}Zr_{0.04})_{7.5}$ ribbons were prepared, which showed coercivities of up to 0.53 T at 50$0^{\circ}C$. Partially amorphous $Nd_{60}Fe_xCo_{30-x}Al_{10}(0{\leq}x{\leq}30)$ alloys were prepared by copper mold casting. The effect of transition metal content on the glass-forming ability and the magnetic properties was investigated. The $Nd_{60}Co_{30}Al_{10}$ alloy exhibits an amorphous structure shown by the corresponding diffraction pattern. A small substitution of Co by 2.5 at.% Fe results In the formation of Fe-rich crystallites embedded in the Nd-rich amorphous matrix. The Fe-rich crystallites show hard magnetic behaviour at room temperature with a coercivity value of about 0.4 T, relatively low saturation magnetization and a Curie temperature of 500 K.

• Textile Coloration and Finishing
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• v.30 no.3
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• pp.199-207
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• 2018

In this study, the properties of polypropylene(PP) non-woven fabric spun under various conditions by the Melt-blown method were verified, and the deodorant content and deodorization of PP non-woven fabric after deodorant-treatment were investigated. PP non-woven fabrics are manufactured by varying the temperature of spin beam, hot air temperature and amount, the RPM of collector R/O and the distance between collector and spinneret, which affects the structure of the non-woven fabric. After that, the structural characteristics and air permeability of the non-woven fabric were measured. The experimental results show that the amount of air, the distance between the collector and the spinneret significantly affect the structural characteristics and air permeability of the PP non-woven fabric. And, regardless of the weight of the PP non-woven fabric, the deodorizing effect of UiO-66 MOF deodorant add-on ratio and content was higher.

• Membrane Journal
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• v.28 no.6
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• pp.395-405
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• 2018

Poly(ethylene-co-vinylalcohol) EVOH hollow fiber membranes were successfully fabricated via a thermally induced phase separation (TIPS) method. It was observed that all membranes fabricated under different spinning conditions had interconnected and bicontinuous structures through liquid-liquid phase separation. Glycerol and poly(ethylene glycol) 200 were used as diluents for the TIPS method. Glycerol was used as a mixing component in quenching bath to control pores on the outer surface of the hollow fiber membrane. Hot quenching bath with a mixing component to generate large pores on the outer surface of the hollow fiber membrane. The effects of polymer concentration, diluent and quenching bath on the morphologies, water permeabilities, and mechanical properties of the EVOH hollow fiber membranes were systematically investigated. The relationship between water permeability, mechanical properties and spinning conditions was discussed in detail.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.32 no.6
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• pp.465-473
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• 2008

Type II compressed natural gas(CNG) storage vessels for automobiles have been acknowledged for their excellence and have recently become established in local regions. Their supply is not only to automakers in Korea such as Hyundai Motors but they are being increasingly exported. Although the available products have undergone safety evaluations and are certified by an authorized institution they are still short of the optimal design that is possible for such storage vessels. This research investigates the shape and thickness of the dome with the aim of optimizing the type II CNG storage vessels by using a finite element analysis technique. CNG storage vessels can be largely divided into 3 parts namely, the hear part, the cylinder part and the dome part. The head part is designed by means of a hot spinning process and this method is safer than that used in the design of the dome part even though its shape is similar. The thickness of the liners and reinforcing materials was optimized based on the requirements of the cylinder and dome parts. In addition, the shape of the dome, which is most suitable for Type II CNG storage vessels, is proposed by a process of review and analysis of various existing shape, and then conducting a structural stability evaluation to ensure the optimal design plan.

• Tribology and Lubricants
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• v.35 no.1
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• pp.77-86
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• 2019

The present study focuses on the effect of staggered integration factor (SIF) on Morton effect simulation results. The Morton effect is a synchronous rotordynamic instability problem caused by the temperature differential across the journal in fluid film bearings. Convection and conduction of heat in the thin film displaces the hot spot, which is the hottest circumferential position in the thin film, from -20 to 40 degrees ahead of the high spot, where the minimum film clearance is experienced. The temperature differential across the journal causes a bending moment and the corresponding thermal bow in the rotating frame acts like a distributed synchronous excitation in the fixed frame. This thermal bow may cause increased vibrations and continued growth of the synchronous orbit into a limit cycle. The SIF is developed assuming that the response of the rotor-lubricant-bearing dynamic system is much quicker than that of the bearing-journal thermal system, and it is defined as the ratio between the simulation time of the thermal system and the rotor-spinning period. The use of the SIF is unavoidable for efficient computing. The value of the SIF is chosen empirically by the software users as a value between 100 and 400. However, the effect of the SIF on Morton effect simulation results has not been investigated. This research produces simulation results with different values of SIF.

• Composites Research
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• v.37 no.3
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• pp.162-169
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• 2024

In this study, PAN(polyacrylonitrile)-based precursor fibers were produced through a wet-spinning process, and their morphologies and graphitization behavior were investigated in the presence of two graphitization catalysts (Ca, Ni). The graphitization catalysts were introduced into the formed pores during hot-water stretching of wet-spun PAN-based precursor fibers. The catalytic effects of graphitization catalysts were examined through crystal structure and Raman analysis. At a relatively low temperature of 1500℃, the graphitization was not significantly affected, whereas at a high temperature of 2400℃, the obtained I_D/I_G value of graphite fiber (GF-Ni100) was decreased by about twice (~0.28) compared to the untreated fibers (GF-AS~0.54). By comparing the I_D/I_G values (GF-Ca100~0.42: GF-Ni100~0.28) of Ca and Ni graphitization catalyst, it was found that the degree of graphitization of Ni graphitization catalyst showed higher influence than that of Ca graphitization catalyst. Moreover, 2D band was also observed, indicating that the graphite plane structures composed of multiple layers were developed. XRD results confirmed that the crystal inter-planar distance (d₀₀₂) of the graphite crystal was slightly decreased after the treatment with the graphitization catalyst, But, the crystal size of Ca-treated graphite fiber (GF-Ca100) was increased by up to ~5 nm.