• 한국해양공학회지
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• 제18권2호
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• pp.58-63
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• 2004

Reduced Activation Ferritic/Martensitic Steels (RAFs) are leading candidntes for structural materials of a D-T fusion reactor. One of the RAFs, JLF-l (9Cr-2W-V, Ta) has been developed and has shown to have good resistance against high-fluency neutrino irradiation and good phase stability. Recently, in order to clarify the strengthening mechanisms at high temperatures, a new scheme to improve high temperature mechanical properties is desired. Therefore, the test technique development of high temperature creep behaviors for this material is very important. In this paper, the creep properties and creep life prediction, using the Larson-Miler parameter method for JLF-l to be used for fusion reactor materials or other high temperature components, are presented at the elevated temperatures of 50$0^{\circ}C$, 55$0^{\circ}C$, $600^{\circ}C$, $650^{\circ}C$ and 704$^{\circ}C$. It was confirmed, experimentally and quantitatively, that a creep life predictive equation, at such various high temperatures, is well derived mr the LMP method.

• 한국세라믹학회지
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• 제53권5호
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• pp.494-499
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• 2016

In this work, the effects of different sintering inhibitors added to $La_{0.8}Sr_{0.2}MnO_{3-{\partial}}$ (LSM) were studied to obtain an optimum cathode material for cathode-supported type of Solid oxide fuel cell (SOFC) in terms of phase stability, mechanical strength, electric conductivity and porosity. Four different sintering inhibitors of $Al_2O_3$, $CeO_2$, NiO and gadolinium doped ceria (GDC) were mixed with LSM powder, sintered at $1300^{\circ}C$ and then they were evaluated. The phase stability, sintering behavior, electrical conductivity, mechanical strength and microstructure were evaluated in order to assess the performance of the mixture powder as cathode support material. It has been found that the addition of $Al_2O_3$ undesirably decreased the electrical conductivity of LSM; other sintering inhibitors, however, showed sufficient levels of electrical conductivity. GDC and NiO addition showed a promising increase in mechanical strength of the LSM material, which is one of the basic requirements in cathode-supported designs of fuel cells. However, NiO showed a high reactivity with LSM during high temperature ($1300^{\circ}C$) sintering. So, this study concluded that GDC is a potential candidate for use as a sintering inhibitor for high temperature sintering of cathode materials.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2008년도 제39회 하계학술대회
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• pp.1238-1239
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• 2008

The high Tc supeconductor of ceramic oxides type was studied for finding its application field. The results reportaed in this paper on the stability of the ceramic superconductors and the resistance to ripening in the BCO liquid phase at elevated temperature opens a processing window for engineering the microstructure of large superconductor at the nanoscale level. The results suggest further that the introduction of highly efficient artifical pinning center to bulk ceramics superconductor.

• 한국해양공학회:학술대회논문집
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• 한국해양공학회 2003년도 추계학술대회 논문집
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• pp.146-151
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• 2003

Reduced Activation Ferritic/Martenstic (RAFs) are leading candidates for structural materials of D-T fusion reactor. One of The RAFs, JLF-1 (9Cr-2W-V, Ta) has been developed and proved to have good resistance against high-fluency neutrino irradiation and good phase stability. Recently, in order to clarify the strengthening mechanical at high temperature, a new scheme to improve high temperature mechanical properties is desired. Therefore, the creep properties and creep life prediction by Larson-Miller Parameter method for JLF-1 to be used for fusion reactor materials or other high temperature components were presented at the elevated temperatures of $500^{\circ}C$, $550^{\circ}C$, $600^{\circ}C$, $650^{\circ}C$ and $704^{\circ}C$. It was confirmed experimentally and quantitatively that a creep life predictive e벼ation at such various high temperatures was well derived by LMP.

• International Journal of Industrial Entomology and Biomaterials
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• 제45권2호
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• pp.93-98
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• 2022

To assess the feasibility of silk sericin for non-textile application, the storage stability and biological safety of sericin were examined. It was extracted at 37℃, 70℃, 100℃, and 121℃ for 1, 3, and 5 h to elucidate the effect of extraction condition on the stability and safety of silk sericin. The solubility was increased till approximately 26% with extraction temperature of 121℃ for 1 h. Sodium dodecyl sulfate-polyacrylamide gel electrophoresis (SDS-PAGE) showed that the molecular weight distribution depended on the extraction conditions. Extracted sericin displayed typical UV absorption bands upon spectrometric analysis. To examine the reproducibility of its obtained conformation, sericin was extracted thrice and its circular dichroism (CD) spectra was measured each time. Most CD spectra showed reproducibility regardless of temperature and time except under 100℃ extraction condition. The diversity of CD spectrum showed gradual reduction and was finally coincident with extraction time from 1 to 5 h. Notably, sericin has a negative peak of approximately 200 nm attributed to random coil conformation, regardless of extraction condition. However, at the 100℃ extraction condition, sericin showed both bands to be negative bands of approximately 200 and 220 nm, respectively. Sericin was centrifuged to determine the stability of storage conditions. The sericin extracted at 100℃ and 121℃ for 1 h was found to form gel rapidly within 1 h, but at 121℃ condition, the gel fraction was approximately 20% within 1 h which retained its phase regardless of storage time. The gel fraction of sericin extracted at 100℃ for 5 h increased with time, however at the 121℃ for 5 h condition, the gel fraction was measured to be less than 10% regardless of increase in storage time. Petriflim^TM AC plates test showed that sericin was safe from aerobic bacteria activity by extraction under high temperature.

• 한국주조공학회지
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• 제19권6호
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• pp.456-465
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• 1999

The overall objective of this study is to investigate the effect of Ag addition on the mechanical properties and microstructure of rapid solidified 7000 Al series alloys. Al-Zn-Mg-Cu alloys with small amounts of Ag was fabricated into the powder by gas atomization. The powder was extruded after the cold compaction and degassing and then followed by T6 heat treatment. Microstructure observation, phase analysis, room and high temperature tensile test and hardness test were pursued. The tensile strength and hardness of Ag-added alloy after heat treatment was increased with increasing Ag contents. However, the elongation of extruded alloys was not increased as much as to be expected. The reason of this result seems to be related to $the{\Omega}$ phase, which contribute to the high temperature strength stability of Al-Cu-Zn alloys through the formation of eutectoid with Ag addition.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2018년도 춘계학술대회 논문집
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• pp.129-129
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• 2018

Hard coating application is effective way of cutting tool for hard-to-machine materials such as Inconel, Ti and composite materials focused on high-tech industries which are widely employed in aerospace, automobile and the medical device industry also Information Technology. In cutting tool for hard-to-machine materials, high hardness is one of necessary condition along with high temperature stability and wear resistance. In recent years, high-entropy alloys (HEAs) which consist of five or more principal elements having an equi-atomic percentage were reported by Yeh. The main features of novel HEAs reveal thermodynamically stable, high strength, corrosion resistance and wear resistance by four characteristic features called high entropy, sluggish diffusion, several-lattice distortion and cocktail effect. It can be possible to significantly extend the field of application such as cutting tool for difficult-to-machine materials in extreme conditions. Base on this understanding, surface coatings using HEAs more recently have been developed with considerable interest due to their useful properties such as high hardness and phase transformation stability of high temperature. In present study, the nanocomposite coating layers with high hardness on WC substrate are investigated using high entropy alloy target made a powder metallurgy. Among the many surface coating methods, reactive magnetron sputtering is considered to be a proper process because of homogeneity of microstructure, improvement of productivity and simplicity of independent control for several critical deposition parameters. The N2 is applied to reactive gas to make nitride system with transition metals which is much harder than only alloy systems. The acceleration voltage from 100W to 300W is controlled by direct current power with various deposition times. The coating layers are systemically investigated by structural identification (XRD), evaluation of microstructure (FE-SEM, TEM) and mechanical properties (Nano-indenter).

• 분석과학
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• 제29권4호
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• pp.194-201
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• 2016

본 연구는 수용액 상태에서 정제봉독 (purified bee venom, PBV)과 봉독멜리틴 (bee venom melittin, BVM)을 보관하기 위하여 온도, 용매, 농도의 조건에 따른 안정성을 비교 실험한 결과이다. Prep-HPLC (column: C₄)를 이용하여 정제봉독으로부터 98.2%인 봉독멜리틴을 분리하여 사용하였다. 용매에 따른 안정성 실험에서, 생리식염수의 경우 정제봉독은 안정성이 증가되고 봉독멜리틴은 감소되었다. 증류수의 조건에서 정제봉독의 안정성은 감소되었으나 봉독멜리틴은 증가되는 현상이 확인되었다. 봉독멜리틴의 안정성을 장기간 유지하기 위한 최적조건으로는 보관온도 4 ℃, 증류수, 시료의 농도는 1.0 mg/mL의 결과를 얻었다.

• 한국재료학회지
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• 제29권1호
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• pp.7-10
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• 2019

Cr-Al alloys are attracting attention as oxidation resistant coating materials for high temperature metallic materials due to their excellent high temperature stability. However, the mechanical properties and oxidation resistance of Cr-Al alloys can be further enhanced, and such attempts are made in this study. To improve the properties of Cr-Al alloys, Si is added up to 5 wt%. Casting specimens with different amounts of Si content are prepared by a vacuum arc remelting method and isothermally heated under steam conditions at $1,100^{\circ}C$ for 1 hour. The as-cast microstructure of low Si alloys is mainly composed of only a Cr phase, while $Al_8Cr_5$ and $Cr_3Si$ phases are also observed in the 5 % Si alloy. In the high Si alloy, only Cr and $Cr_3Si$ phases remain after the isothermal heating at $1,100^{\circ}C$. It is found that Si additions slightly decrease the oxidation resistance of the Cr-Al alloy. However, the microhardness of the Cr-Al alloy is observed to increase with an increasing Si content.

• 대한화장품학회지
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• 제38권4호
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• pp.263-270
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• 2012

아스코르빅산(비타민 C)은 수용액상에서 공기와 빛, 알칼리 등에 의해 쉽게 불안정화되는 성질이 있어 화장품에 적용에 있어서 제한적이다. 아스코르빅산은 수용액상에서 불안정성에 영향을 주는 가장 중요한 인자인 공기, 특히 산소와 열, 빛 등의 외부환경에 민감하게 반응하여 산화에 의해 쉽게 분해되는 문제점이 있다. 본 연구에서는 이러한 아스코르빅산의 안정성을 증가시키고자 폴리올과 유화방법을 변화시켜 안정화하는 연구를 수행하였고 실온과 고온에서 색상과 아스코르빅산의 함량변화를 HPLC로 측정하여 비교하였다. 그 결과 실험한 조건들 중 폴리올은 글리세린을 사용한 경우 아스코르빅산의 안정화 가장 좋았으며 비수유화방법을 사용한 경우에 있어서 가장 안정하였다. 이러한 결과들로부터 아스코르빅산이 본 실험의 비수유화로 안정성이 증가하며 안정한 화장품을 만드는 데 적용이 가능하다.