• Title/Summary/Keyword: High-pressure experiment

Search Result 984, Processing Time 0.026 seconds

Analysis of $Si_3N_4$ Ultra Fine Powder Using High-pressure Acid Digestion and Slurry Injection in Inductively Coupled Plasma Atomic Emission Spectrometry

  • Kim, K.H.;Kim, H.Y.;Im, H.B.
    • Bulletin of the Korean Chemical Society
    • /
    • v.22 no.2
    • /
    • pp.159-163
    • /
    • 2001
  • Si3N4 powder has been analyzed by inductively coupled plasma atomic emission spectrometry (ICP-AES). The sample was dissolved by high-pressure acid digestion with HF, H2SO4 (1+1), and HNO3 mix ture. This technique is well suited for the impurity analysis of Si3N4 because the matrix interference is eliminated. A round-robin samples trace elements, such as Ca, W, Co, Al, Fe, Mg, and Na, were determined. For the direct analysis, slurry nebulization of 0.96 mm Si3N4 powder also has been studied by ICP-AES. Emission intensities of Fe were measured as ICP operational conditions were changed. Significant signal difference between slurry particles and aqueous solution was observed in the present experiment. Analytical results of slurry injection and high-pressure acid digestion were compared. For the use of aqueous standard solution for calibration, k-factor was determined to be 1.71 for further application.

Open-Loop Responses of Droplet Vaporization to Linear Normal Acoustic Modes

  • Kim, S.Y.;W.S. Yoon
    • Proceedings of the Korean Society of Propulsion Engineers Conference
    • /
    • 2004.03a
    • /
    • pp.155-164
    • /
    • 2004
  • In order for studying pressure-coupled dynamic responses of droplet vaporization, open-loop experiment of an isolated droplet vaporization exposed to pressure perturbations in stagnant gaseous environment is numerically conducted, Governing equations are solved for flow parameters at gas and liquid phases separately and thermodynamic parameters at the interfacial boundary are matched for problem closure. For high-pressure effects, vapor-liquid interfacial thermodynamics is rigorously treated. A series of parametric calculations in terms of mean pressure level and wave frequencies are carried out employing a n-pentane droplet in stagnant gaseous nitrogen. Results show that wave instability in view of pressure-coupled vaporization response seems more susceptible at higher pressures and higher wave frequencies. Mass evaporation rate responding to pressure waves is amplified with increase in pressure due to substantial reduction in latent heat of vaporization. Augmentation of perturbation frequency also enhances amplification due to the reduction of phase differences between pressure perturbation and surface temperature fluctuation.

  • PDF

Effect of Injection Pressure on Atomization Characteristics of Fuel Spray in High-Pressure Gasoline Injector (가솔린 인젝터의 연료 분무 미립화 특성에 미치는 분사 압력의 영향)

  • Lee, Chang-Sik;Choi, Soo-Chon;Kim, Min-Kyu;Kwon, Sang-Il
    • Transactions of the Korean Society of Mechanical Engineers B
    • /
    • v.24 no.4
    • /
    • pp.555-560
    • /
    • 2000
  • This paper describes the macroscopic behavior and atomization characteristics of the high-pressure gasoline injector in direct-injection gasoline engine. The global spray behavior of fuel injector was visualized by shadowgraph technique. The atomization characteristics of gasoline spray such as mean diameter and mean velocity of droplet were measured by the phase Doppler particle analyzer system. In order to obtain the influence of fuel injection pressure, the macroscopic visualization and experiment of particle measurement on the fuel spray were investigated at 3,5 and 7 MPa of injection pressure under different surrounding pressure in the spray chamber. The results of this work show that the fuel injection pressure of gasoline injector in GDl engine has influence upon the mean droplet diameter, mean velocity of spray droplet, the spray tip penetration, and spray width under the elevated ambient pressure.

Performance of Absorption Diffuser Silencers (흡음형 디퓨저 소음기의 성능)

  • 정갑철;현승일;이종우;권영필
    • Journal of KSNVE
    • /
    • v.4 no.3
    • /
    • pp.377-384
    • /
    • 1994
  • This paper is an investigation of the performance of absorption diffusers to suppress the vent noise emitted when high pressure gas is throttled. First, experiment for the static performance is carried out. When there is no through-flow, the insertion loss has been obtained in terms of 1/3 octave band spectrum and the effect of the number of diffusers and the thickness of the absorption material on the static performance has been obtained. And the similarity in the spectrum of the static insertion loss is confirmed by comparing two similar models with different size. Second, the dynamic performance has been obtained by experiment using blow-down of compressed air from a storage tank through an orifice of diameter 10 mm. The back pressure by the diffuser is measured and compared with that of a single diffuser. It is found that the insertion loss of asingle diffuser is very low around 3 dB at high frequencies with negative value at low frequencies. By absorption material between the diffuser tubes, however, the performance is increased considerably. Without flow the static insertion loss increases by 3 - 4 dB by doubling the thickness or the density of the absorptionmaterial. With flow, however, the dynamic insertion loss increases. While, the back pressure by the diffuser is small enough to be neglected.

  • PDF

Air Similarity Test and Analysis of Steam Turbine Labyrinth Seal for Leakage Verification (스팀터빈용 래비린스 실의 누설량 규명을 위한 공기상사 실험 및 해석)

  • Ahn, Sang-Kyu;Kim, Seung-Jong;Lee, Yong-Bok;Kim, Chang-Ho;Ha, Tae-Wong
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
    • /
    • 2006.05a
    • /
    • pp.1149-1149
    • /
    • 2006
  • The leakage characteristic is an important factor in power plant. However, most of power plant have efficiency problem which is occurred leaking between high pressure steam turbine axle and stator. The labyrinth seal which is used between the main turbine axle and stator in the power plant. Because it is able to be non-contact seal and it is minimize clearance to decrease the leakage. But its actual system is too huge to experiment. Therefore, most steam turbine seal performance tests were conducted by air similarity test. This paper described a test facility and program for air similarity test of high pressure steam turbine seal. A test facility has been designed and built to evaluate leakage verification of labyrinth seal. The test facility consist of air compressor, anti-swirl labyrinth seal for 1/3 air similarity model, pressure transducer, air flow measure system, instrumentation and auxiliary system. For evaluation of steam turbine seal performance, the air similarity test of labyrinth seal leakage verification was conducted and we compared experiment data and analysis result.

  • PDF

Mass Transfer and Hydraulic Kinematic Character Using Lattices Packings by Countercurrent Flow of Gas-Liquid Phase in Packing Column (격자형 충진물을 이용한 충진탑내 기액상의 역류에 의한 물질전달과 수력학적 동특성)

  • Kim, Jang-Ho;Ha, Sang-An
    • Journal of Ocean Engineering and Technology
    • /
    • v.2 no.2
    • /
    • pp.130-137
    • /
    • 1988
  • This thesis introduced that character of a treatment technique for a mading synthetic resin Hifiow-Ring. The material system of packings make an experiment air$NH_{3}$/air$H_{2}SO_{4}$, $SO_{2}$-air/NaOH, $NH_{3}$-air/$/H_{2}SO_{4}$ under general conditions. Lattices packing compared with conventional packings was proved low pressure loss and high separation efficiency for high loading per trans unit. And an inflow materal tested for absorption and rectification, it made an experiment under a range regular temperature, low energy and small amount of money. That made possible in simple equation, volume material tranfer coefficient$\beta_{L}$ . a by absorption or $\beta_{V}$ .a calculated in all range loading. The peculiarity pressure loss $\Delta\;P/NUT_{ov}$ for Hiflow-ring contributed to a fall cost of energy, a grade number of a vacuum rectification and absorption calculation.

  • PDF

A study on the oyster shucking machine using super-high pressure (초고압력을 이용한 굴 박신기계에 관한 연구)

  • KIM, Ok-sam;MIN, Eun-bi;HWANG, Doo-jin
    • Journal of the Korean Society of Fisheries and Ocean Technology
    • /
    • v.57 no.4
    • /
    • pp.382-389
    • /
    • 2021
  • By applying super-high pressure (150-250 MPa) to a sealed pressure vessel, it is possible to make oyster shucking machine that automatically opens two-sheet shellfish or oysters. Possibility of developing a shucking machine was confirmed by identifying the working pressure for meat of oysters produced in the southern coast and conducting sensory evaluation of meat oysters. As a result of confirming the shucked oysters under super-high pressure of 150 MPa in the pressure vessel, the number of type A with separated shells and well-separated meat was 22 and type B with both shells and internal meat and shells not separated. For the oysters that were treated at 175 MPa, there were 58 type As with shell separated and meat well separated and 42 type Bs without oyster shells and insides. When looking at the oysters shucked at 200 MPa in the pressure vessel, the number of type A was 86 and type B was 14 accounting for 86% of oysters with good marketability. As a result of shucking oysters by applying 250 MPa, 96% type A oysters and 4% type B oysters were obtained from the total specimen. The total specimen oyster weight used in the conducted experiment was 6 kg, the average oyster shell weight was 3.99 kg and the average oyster meat weight was 1.25 kg. Therefore, the fatness of oyster meat, which measures the added value of oysters, is 20.8%. Sensory evaluation was conducted on thinned oysters by hand and type A oysters shelled by machine with an operating pressure of 200 MPa. The hand-worked oyster sample scored 4.7 points only in salty taste, and scored 5.0 or higher in color, shape, smell, fishy taste, texture and preference.

A Study on Pore Pressure Evaluation of Concrete Lining in Road Tunnel Fire (도로터널 라이닝 화재조건 콘크리트 라이닝 공극압력 특성에 관한 연구)

  • Park, Kyung-Hoon;Kim, Heung-Youl;Yoo, Yong-Ho;Lee, Chul-Ho;Kim, Hyung-Jun
    • Proceedings of the Korea Institute of Fire Science and Engineering Conference
    • /
    • 2008.11a
    • /
    • pp.484-489
    • /
    • 2008
  • We carried out a one-way heating experiment on the PC panel manufactured by changing the filling depths(20,30,40,50mm) of concrete regarding the fire strength in order to measure the inner concrete pressure which is a direct cause of concrete spalling. This fire experiment was conducted under the fire strength conditions of ISO 834 Standard, Modified Hydrocarbon and the maximum value of Pore Pressure was measured. As a result of analyzing the time it took to reach maximum pressure, it showed that the time rising to the maximum pressure of high strength concrete of 40MPa is slower than that of a 24MPa tunnel lining. In case of ISO fire conditions, spalling damage might take place in heating period of $20{\sim}40$ minutes in the range of $100{\sim}200^{\circ}C$ temperature. In case of MHC fire conditions, the area damaged by fire can appear after a lapse of $25{\sim}50$ minutes in the range of $150{\sim}250^{\circ}C$ temperature.

  • PDF

Experimental comparison on the noise characteristics of free and impinging jets (자유분류와 충돌분류의 소음특성에 관한 실험적 비교)

  • 이동훈
    • Journal of the Korean Society of Manufacturing Technology Engineers
    • /
    • v.5 no.2
    • /
    • pp.83-89
    • /
    • 1996
  • The objective of this study is to find experimentally the characteristics of the noise generated by the impinging jet on the normal plate, and also to compare the noise characteristics of the impinging jet with those of the free jet. The experiment is performed for the measurement of the noise specturm, the noise power, and the directivity for the free and impinging jets. From the experiment. it is found that the power of noises generated by the free jet as well as the impinging jet is proportional to the eighth power of the jet velocity through the circular converging nozzle, and that the noise power of the impinging jet is 15dB as high as one of the free jet when the plate distance is about within one to three times the nozzle diameter at the pressure ratio 1.39. The sound pressure level of the impinging jet depends upon the jet pressure and the plate distance. The plate distance with the maximum overall sound pressure level is increased with the jet pressure. The directivities with 1/3 octave band frequency for both the free jet and the impinging jet are greatly influenced by the convection effect.

  • PDF

A Study on the Effect of Filling Ratio on Sloshing Impact Pressure (적재율이 슬로싱 충격압력에 미치는 영향에 관한 연구)

  • Choi, Hu-In;Kwon, Sun-Hong;Park, Jung-Ho;Choi, Young-Myung
    • Journal of Ocean Engineering and Technology
    • /
    • v.24 no.6
    • /
    • pp.30-33
    • /
    • 2010
  • This study presents the effect of filling ratio on sloshing impact pressure. The experiment was done with three filling ratios of 20%, 70%, and 95% of the tank height. The input of the motion was regular excitation. The total number of sensors in use were 53. They were installed on tank top and tank wall. The maximum pressures and the average of one third highest impact pressures for the whole pressure sensors were investigated. The result shows clearly the location of sensors which are exposed to the high impact pressures for different filling ratios. The characteristics of the impact patterns for three filling ratios were also examined.