• Title/Summary/Keyword: High-pressure experiment

Search Result 984, Processing Time 0.028 seconds

The Effect of Barrel Vibration Intensity to the Plating Thickness Distribution

  • Lee, Jun-Ho;Roselle D. Llido
    • Proceedings of the Korean Institute of Surface Engineering Conference
    • /
    • 1999.10a
    • /
    • pp.15-15
    • /
    • 1999
  • In chip plating, several parameters must be taken into consideration. Current density, solution concentration, pH, solution temperature, components volume, chip and media ratio, barrel geometrical shape were most likely found to have an effect to the process yields. The 3 types of barrels utilized in chip plating industry are the conventional rotating barrel. vibrational barrel (vibarrel), and the centrifugal type. Conventional rotating barrel is a close type and is commonly used. The components inside the barrel are circulated by the barrel's rotation at a horizontal axis. Process yield has known to have higher thickness deviation. The vibrational barrel is an open type which offers a wide exposure to electrolyte resulting to a stable thickness deviation. It rotates in a vertical axis coupled with multi-vibration action to facilitate mixed up and easy transportation of components, The centrifugal barrel has its plated work centrifugally compacted against the cathode ring for superior electrical contact with simultaneous rotary motion. This experiment has determined the effect of barrel vibration intensity to the plating thickness distribution. The procedures carried out in the experiment involved the overall plating process., cleaning, rinse, Nickel plating, Tin-Lead plating. Plating time was adjusted to meet the required specification. All other parameters were maintained constant. Two trials were performed to confirm the consistency of the result. The thickness data of the experiment conducted showed that the average mean value obtained from higher vibrational intensity is nearer to the standard mean. The distribution curve shown has a narrower specification limits and it has a reduced variation around the target value, Generally, intensity control in vi-barrel facilitates mixed up and easy transportation of components, However, it is desirable to maintain an optimum vibration intensity to prevent solution intrusion into the chips' internal electrode. A cathodic reaction can occur in the interface of the external and internal electrode. $2HD{\;}+{\;}e{\;}{\rightarrow}20H{\;}+{\;}H_2$ Hydrogen can penetrate into the body and create pressure which can cause cracks. At high intensity, the chip's motion becomes stronger, its contact between each other is delayed and so plating action is being controlled. However, the strong impact created by its collision can damage the external electrode's structure thereby resulting to bad plating condition. 1 lot of chip was divided into two equal partion. Each portion was loaded to the same barrel one after the other. Nickel plating and tin-lead plating was performed in the same station. Portion A maintained the normal barrel vibration intensity and portion B vibration intensity was increased two steps higher. All other parameters, current, solution condition were maintained constant. Generally, plating method find procedures were carried out in a best way to maintained the best plating condition. After plating, samples were taken out from each portion. molded and polished. Plating thickness was investigated for both. To check consistency of results. 2nd trial was done now using different lot of another characteristics.

  • PDF

Intercomparison between Temperature and Humidity Sensors of Radiosonde by Different Manufacturers in the ESSAY (Experiment on Snow Storms At Yeongdong) Campaign (대설관측실험(Experiment on Snow Storms At Yeongdong: ESSAY) 기간 중 두 제조사 라디오존데 기온과 습도 센서 상호 비교)

  • Seo, Won-Seok;Eun, Seung-Hee;Kim, Byung-Gon;Seong, Dae-Kyeong;Lee, Gyu-Min;Jeon, Hye-Rim;Choi, Byoung-Cheol;Ko, A-reum;Chang, Ki-Ho;Yang, Seung-Gu
    • Atmosphere
    • /
    • v.26 no.2
    • /
    • pp.347-356
    • /
    • 2016
  • Radiosonde is an observation equipment that measures pressure (geopotential height), temperature, relative humidity and wind by being launched up from the ground. Radiosonde data which serves as an important element of weather forecast and research often causes a bias in a model output due to accuracy and sensitivity between the different manufacturers. Although Korean Meteorological Administration (KMA) and several institutes have conducted routine and intensive radiosonde observations, very few studies have been done before on the characteristics of radiosonde performance. Analyzing radiosonde observation data without proper understanding of the unique nature of those sensors may lead to a significant bias in the analysis of results. To evaluate performance and reliability of radiosonde, we analyzed the differences between two sensors made by the different manufacturers, which have been used in the campaign of Experiment on Snow Storm At Yeongdong (ESSAY). We improved a couple of methods to launch the balloon being attached with the sensors. Further we examined cloud-layer impacts on temperature and humidity differences for the analysis of both sensors' performance among various weather conditions, and also compared daytime and nighttime profiles to understand temporal dependence of meteorological sensors. The overall results showed that there are small but consistent biases in both temperature and humidity between different manufactured sensors, which could eventually secure reliable precisions of both sensors, irrespective of accuracy. This study would contribute to an improved sounding of atmospheric vertical states through development and improvement of the meteorological sensors.

Research for Crack Generation and Propagation of Daejeon Granite under Stress Conditions (대전 화강암에 대한 가압 조건하에서의 암석 균열 발생과 성장에 관한 연구)

  • Choi, Junghae;Kim, Hye-jin;Chae, Byung-gon
    • Economic and Environmental Geology
    • /
    • v.52 no.6
    • /
    • pp.587-593
    • /
    • 2019
  • This study were subjected to accelerated weathering test under freeze-thaw and pressure conditions to observe initiation and propagation of cracks using CLSM. Applied stress was set at 50 MPa, 55 MPa, 70 MPa for 3 samples each by using compressor and freeze-thaw experiment was conducted while samples maintained that condition. In freeze-thaw experiments, a temperature range was set to -20~40℃ which was 1 cycle for 6 hours. The freeze-thaw cycle was composed of time which reached to set temperature for 1 hour and holding time for 2 hours. On the basis of this cycle, surface of samples was observed by CLSM after each 20 freeze-thaw cycle. From this research, according to increase freeze-thaw cycle, there were 7, 10, 19 each cracks and High pressured sample's accumulate length was longer than low pressured sample's. High pressured sample's crack velocities were also faster than low pressured sample's which were calculated by accumulate length and freeze-thaw cycle.

The High temperature stability limit of talc, $Mg_3Si_4O_{10}(OH)_2$ (활석 $Mg_3Si_4O_{10}(OH)_2$의 고온 안정영역에 관한 실험적 연구)

  • 조동수;김형식
    • The Journal of the Petrological Society of Korea
    • /
    • v.6 no.2
    • /
    • pp.123-132
    • /
    • 1997
  • In the system $MgO-SiO_2-H_2O$, Talc[$Mg_3Si_4O_{10}(OH)_2$] has been synthesized hydrothermally at 200 MPa, $600^{\circ}C$ from the oxide mixture of the bulk composition of talc. The oxide mixture of the bulk composition of anthophyllite$[Mg_7Si_8O_{22}(OH)2]$ converted to talc, enstatite $(MgSiO_3)$, quartz at 200 MPa, $750^{\circ}C$ with excess of $H_2O$. In low to medium pressure metramorphism, enstatite-talc assemblage is metastable relative to anthophyllite with the reaction talc + 4 enstatite=anthophyllite (Greenwood, 1963). The high temperature stability of talc is bounded with the dehydration reaction to anthophyllite rather than that to enstatite(Greenwood, 1963; Chernosky et al., 1985). Therefore our experiment result assemblage, enstatite-talc-quatz at 200 MPa, $750^{\circ}C$ from oxide mixture of bulk compostion of anthophyllite is metastable assemblage. The hydrothermal experiment performed at 41 to 243 MPa, 680 to $760^{\circ}C$ with the starting material composed of synthetic talc, enstatite and quartz. Talc or enstatite grows during the runs and no extra phases including anthophyllite nucleated. Based on the increase or decrease of the each phase from run products, one of the possible reactions is talc=3 enstatite+quartz+H_2O$. The reversal bracket of the reaction is 699 to $700^{\circ}C$ at 100 MPa. Talc is stable up to $740^{\circ}C$ at 200 MPa and enstatite grow at $680^{\circ}C$, 40 MPa and at $760^{\circ}C$, 250 MPa. Though the high temperature limit of talc around 200 MPa is bounded thermodynamically by the reaction, 7 talc=3 anthophyllite+4 quartz+4 H_2O$, talc persisted throughout the previous reaction up to the reaction, talc=3 enstatite+quartz+$H_2O$.

  • PDF

Increase of Strawberry Fruit Shelf-life through Preharvest Spray of Calcium-chitosan and Post-harvest Treatment with High Pressure CO2 (수확 전후 칼슘-키토산 및 고농도 CO2 단기처리에 의한 '설향' 딸기 과실의 저장성 증진)

  • Ahn, Sun-Eun;Lee, Ah-Youn;Wang, Mao-Hua;Hwang, Yong-Soo
    • Horticultural Science & Technology
    • /
    • v.32 no.5
    • /
    • pp.636-644
    • /
    • 2014
  • This experiment examined the effects of preharvest Ca-chitosan spraying and short-term post-harvest treatment with high $pCO_2$ on the shelf-life of 'Seolhyang' strawberry fruit. Fruit firmness decreased when harvested late in the season and was little affected by Ca-chitosan spray treatments. Short-term treatment with high $pCO_2$ after harvest, however, significantly increased fruit firmness regardless of preharvest treatment. The combined treatment of Ca-chitosan spray and high $pCO_2$ led to an additional increase in shelf-life through delay of skin disorder, fruit decay incidence and firmness loss during simulated marketing. The residual effects of both treatments, however, were reduced when fruit were harvested late in the season. Fruit firmness was more affected by high $pCO_2$ treatment whereas decay and visual quality were affected by preharvest spraying with Ca-chitosan. Although more research is required to determine the optimum concentration of calcium and chitosan, and the optimal spray interval, our results show that the combined treatment of preharvest Ca-chitosan spray and postharvest high $pCO_2$ is effective in improving strawberry fruit shelf-life by increasing firmness and delaying decay.

Experimental study on the characteristics of Vacuum residue gasification in an entrained-flow gasifier (습식 분류상 가스화장치를 이용한 중질잔사유(Vacuum residue)의 가스화 특성연구)

  • ;;;;;;;A. Renevier
    • Proceedings of the Korea Society for Energy Engineering kosee Conference
    • /
    • 2002.11a
    • /
    • pp.171-184
    • /
    • 2002
  • Approx. 200,000 bpd vacuum residue oil is produced from oil refineries in Korea. These are supplying to use asphalt, high sulfur fuel oil, and upgrading at the residue hydro-desulfurization unit. Vacuum residue oil has high energy content, however high sulfur content and high concentration of heavy metals represent improper low grade fuel. To meet growing demand for effective utilization of vacuum residue oil from refineries, recently some of the oil refinery industries in Korea, such as SK oil refinery and LG Caltex refinery, have already proceeded feasibility study to construct 435-500 MWe IGCC power plant and hydrogen production facilities. Recently, KIER(Korea Institute of Energy Research) are studing on the Vacuum Residue gasification process using an oxygen-blown entrained-flow gasifier. The experiment runs were evaluated under the reaction temperature : 1,100~1,25$0^{\circ}C$, reaction pressure : 1~6kg/$\textrm{cm}^2$G, oxygen/V.R ratio : 0.8~0.9 and steam/V.R ratio : 0.4-0.5. Experimental results show the syngas composition(CO+H$_2$) : 85~93%, syngas flow rate : 50~110Mm$^3$/hr, heating value : 2,300~3,000 ㎉/Nm$^3$, carbon conversion : 65~92, cold gas efficiency : 60~70%. Also equilibrium modeling was used to predict the vacuum residue gasification process and the predicted values were compared reasonably well with experimental data.

  • PDF

Experimental Study on the Characteristics of Vacuum Residue Gasification in an Entrained-flow Gasifier (습식 분류상 가스화장치를 이용한 중질잔사유(Vacuum Residue)의 가스화 특성연구)

  • ;;;;;;;A. Renevier
    • Journal of Energy Engineering
    • /
    • v.12 no.1
    • /
    • pp.49-57
    • /
    • 2003
  • Approx. 200.000 bpd vacuum residue oil is produced from oil refineries in Korea, and is supplied to use asphalt, high sulfur fuel oil and for upgrading at the residue hydro-desulfurization unit. Vacuum residue oil has high energy content, however its high sulfur content and high concentration of heavy metals represent improper low grade fuel. To meet growing demand for effective utilization of vacuum residue oil from refineries, recently some of the oil refinery industries in Korea, such as SK oil refinery and LG Caltex refinery, have already proceeded feasibility study to construct 435~500 MWe IGCC power plant and hydrogen production facilities. Recently, KIER (Korea Institute of Energy Research) are studying on the Vacuum Residue gasification process using an oxygen-blown entrained-flow gasifier. The experiment runs were evaluated under the reaction temperature: 1.100~l,25$0^{\circ}C$, reaction pressure: 1~6 kg/$\textrm{cm}^2$G, oxygen/V.R ratio: 0.8~0.9 and steam/V.R ratio: 0.4~0.5. Experimental results show the syngas composition (CO+H$_2$): 85~93%, syngas flow rate: 50~l10 Nm$^3$/hr, heating value: 2,300~3,000 k㎈/Nm$^3$, carbon conversion: 65~92, cold gas efficiency: 60~70%. Also equilibrium modeling was used to predict the vacuum residue gasification process and the predicted values were compared reasonably well with experimental data.

Effects of Storage Conditions on Rancidity of Perilla and Sesame Seed Oils (저장조건(貯藏條件)이 들깨유(油) 및 참깨유(油)의 산패도(酸敗度)에 미치는 영향(影響))

  • Kim, Hye-Kyung;Lee, Yang-Cha;Lee, Ki-Yull
    • Journal of Nutrition and Health
    • /
    • v.12 no.1
    • /
    • pp.51-58
    • /
    • 1979
  • It is a general trend everywhere that the uses of vegetable oils are increasing due to the fact that they are effective in curing and preventing symptoms of high blood pressure and various heart failure conditions. At the same time the concept that oxidative rancidity is caused by the oxidation of unsaturated fatty acid moieties whose subsequent decomposition gives rise to various undesirable, sometimes toxic compounds is now well accepted. Linolenic acid (C, 18:3) is one of highly unsaturated and readily oxidizable fatty acid. The content of this essential polyunsaturated fatty acid in perilla seed oil (PSO) was found to be as high as 48% while only 1.5% in sesame seed oil (SSO). In this experiment the oxidative stability of PSO was compared with that of SSO. The experimental test group were as follows: A) Stored at different temperatures, namely $4^{\circ}C,\;30^{\circ}C,$ and $60^{\circ}C,$ B) Stored at room temperature $(20{\pm}5^{\circ}C)$ ; a. protected from sunlight and air, b. exposed to air without sunlight c. exposed to sunlight but protected front air, d. completely exposed to both air and sunlight. The following results were obtained; 1) It was found to be most stable against oxidation to store both PSO and SSO under the low temperature $(4^{\circ}C)$ condition. According to P.V. measurements it was found to be safe to keep both oils up to $30^{\circ}C$ for at least 8 weeks. When exposed to air, sunlight and high temperature $(60^{\circ}C)$, P.V. of PSO reached there peak values, which were much higher than those of SSO. This explains much of its instability as compared to SSO against oxidation. 2) The effect of high temperature $(60^{\circ}C)$ on A.V. was found to be more striking than those of all the other storage conditions. The condition of refrigeration was most effective in keeping A.V. low for both oils as was the case in P.V. 3) For both oils, I.V. decreased throughout the experimental period (8 weeks). The range of decrement was larger for PSO than SSO. 4) There was no significant change in the compositions of fatty acids of SSO caused by various experimental storage conditions. But for PSO the compositions of stearic, oleic and linoleic acid were decreased, whereas linolenic acid was increased proportionally.

  • PDF

ARC Discharge Sound Source in Underwater (수중 아-크 방전음원에 관한 연구)

  • Chang, Jea-Hwan;Chang, Jee-Won
    • Journal of the Korean Society of Fisheries and Ocean Technology
    • /
    • v.21 no.1
    • /
    • pp.12-18
    • /
    • 1985
  • In general the impulse sound sources of underwater generated by electric arc discharge had used static energy of the charged capacitors. The author proposed an underwater arc discharge sound source using secondary voltage of high voltage transformer without capacitors. The arc discharge device was composed of a high voltage transformer and a switching system. The impulse current in the primary turn of the high voltage transformer is controlled by the switching system and inductive current of the secondary turn in the high voltage transformer is used in making impulsive arc discharge. A series of experiment have been carried out to observe the acoustic characteristics of the impulse sound source generated by the arc discharge. The results obtained were as follows: 1. Secondary current at the time of arc discharge keeps after ohm's law in the beginning and the maximum current flows out as soon as arc discharge breaks out. 2. A time difference between a start of applied current and a generation of arc discharge sound is the 3msec and it is generated arc sound when breaking down electric insulation at maximum voltage. 3. The sharper the end of electrodes and the higher the secondary voltage, the higher the sound pressure level. 4. Arc discharge sound was generated even at the distance of 100cm between electrodes and was stably reproductive at the gap of 1cm to 100cm. 5. Electric arc discharge sound wave is a shock wave of pulse-width of 0.15msec and spectral distribution of it is plenty of low frequency components less than 10 KHz.

  • PDF

Characteristics of Temperature Control by Hot-gas Bypass Flow Rate on Industrial Water Cooler (핫가스 바이패스 유량에 따른 산업용 냉각기의 온도제어 특성)

  • Baek, Seung-Moon;Choi, Jun-Hyuk;Byun, Jong-Yeong;Moon, Choon-Geun;Lee, Ho-Saeng;Jeong, Seok-Kwon;Yoon, Jung-In
    • Journal of Advanced Marine Engineering and Technology
    • /
    • v.33 no.8
    • /
    • pp.1129-1136
    • /
    • 2009
  • The paper presents the performance characteristics for a cooling system using EEV. The water cooler was used to reduce thermal deformation and contraction due to high speed of machine tools and the EEV was used for capacity control for water cooler. The apparatus was designed for hot-gas bypass system which a hot-gas can flows from outlet of compressor to the inlet of evaporator. This experiment is the intermediary study for precise temperature control through PID control. The results show that the evaporator pressure increased and refrigeration capacity decreased as the EEV opening step of hot-gas bypass increased. These results can be used as basic data for the design of effective water cooler.