• 제목/요약/키워드: High separation efficiency

검색결과 409건 처리시간 0.026초

Preparative Chromatographic Separaction: Simulated Moving Bed and Modified Chromatography Methods

  • Yi Xie;Koo, Yoon-Mo;Nien-Hwa Linda Wang
    • Biotechnology and Bioprocess Engineering:BBE
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    • 제6권6호
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    • pp.363-375
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    • 2001
  • Chromatography has been method of choice for the separation complex biologi-cal mixtures fro analytical purpose, particularly for the last fifty years. Its use has recently been extended to preparative separation where the productivity relative to the amount of resin and sol-vent used is a matter of concern. To overcome the inherent thermodynamic inefficiency of batch chromatography, as exemplified by the partial temporal usage of the resin and dilution of the product with the solvent, chromatography has been continually modified by separation engineers. Column switching and recycling represnet some of the process modifications that have brought high productivity to chromatography. Recently, the simulated moving bed (SMB) method, which claims a high separation efficiency based on counter-current moving bed chromatography. has be-come the mainstay of preparative separation, especially in chiral separation. Accordingly, this pa-per reviews the current status of SMB along with several chromatographic modification, which may be helpful in routine laboratory and industrial chromatographic practices.

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용존공기부상(DAF) 공정을 이용한 생물학적 플록의 부상분리 (Flotation Separation of Biological Floc Using the Dissolved Air Flotation Process)

  • 곽동희;김성진;임영환
    • 상하수도학회지
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    • 제18권5호
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    • pp.649-655
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    • 2004
  • The behavior of biological particles in DAF (dissolved air flotation) process was analyzed by employing PBT (Population balance theory). After decline growth phase of activated sludge, the value of the initial collision-attachment efficiency was increased over than 0.35 corresponding relatively high value in the whole life cycle of microorganism. For practical application of DAF as a solid separation process. It is desirable that microbial particles should be operated to perform high solid removal efficiency in biological wastewater treatment.

경사각을 갖는 적층판식 유수분리기의 유수분리 효율에 관한 연구 (A Study on the Oil/Water Separation Efficiency of Laminated Plate Type Oily water Separator with Inclined Angle)

  • 한원희;김준효;최민선
    • Journal of Advanced Marine Engineering and Technology
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    • 제25권2호
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    • pp.365-374
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    • 2001
  • Its a tendency to strengthen related international was as the importance on marine oil pollution recently becomes the issue. According to the regulation of IMO, oil discharge from ships is allowed under 15PPM only and oil filtering equipment is essential. Oily water separator of laminated plate type which is one of gravity type separator can be use as assistant equipment for the oil filtering system to meet the present IMO standard, because it fits well to process large amount of rich oil with high specific gravity. The purpose of this paper is to investigate an efficiency of oil/water separation with the characteristics of laminated plate arrangement. The analyse of oil contents for oil-water mixture were carried out in order to find an efficiency of oil/water separation and an experimental study was simultaneously carried out to investigate internal flow characteristics of separator by visualization method and PIV(Particle Image Velocimetry) measurement at three spaces of plates for 5, 10 and 15 mm with variation of inlet flow rates of $0.25m^3$/h and $0.5m^3$/h. The experimental results showed that the space of the plates acts a significant role in the separating process.

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제작된 모세관 전기영동 시스템의 유기물 분석에의 응용 (Application of Home-made Capillary Zone Electrophoresis System to the Separation of Organic Molecules)

  • 이공주;허귀석
    • 대한화학회지
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    • 제35권3호
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    • pp.219-225
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    • 1991
  • 고도로 효율적인 분석방법인 모세관 전기영동 시스템을 최적의 감도를 갖는 상태의 기기로 국내에서 제작하였다. 50 ${\mu}m$ 내경을 가진 모세관을 완충용액으로 채워준 후 모세관의 양끝에 20∼35 kV의 전압을 걸어주는 이 분석방법은 20분 이내에 10 nl 이하의 소량의 시료를 이론단수가 20∼50만 정도가 되도록 분리할 수 있는 매우 좋은 분리능으 가지고 있다. 모세관 전기영동법의 분리능과 분리도를 증가시키는데 영향을 주는 요소들을 알아보기 위하여 catecholamine과 adenine 유도체를 분석하였다.

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Research and development of new magnetic filter for high gradient magnetic separation

  • Shigehiro Nishijima;Naoki Nomura;Fumihito Mishima
    • 한국초전도ㆍ저온공학회논문지
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    • 제25권3호
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    • pp.1-6
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    • 2023
  • We have been developing a new magnetic filter so that small sized paramagnetic substances can be separated even in a low magnetic field (lower than 2T). The developed filter is a packed ferromagnetic filament with a triangular cross section. The filament has a diameter of 120 ㎛ and a length of 3 mm, and is mechanically packed with a volume ratio of 17.6%. Using this filter, a magnetic separation experiment of hematite was carried out using a superconducting magnet at the field of 2T. Similarly, magnetic separation was performed using a conventional magnetic filter. It became clear that the separation efficiency of newly developed filter is high as that of conventional mesh filter. The smaller sized hematite (<3 ㎛) could be separated though conventional mesh filter could not separate.

Study on multi-stage magnetic separation device for paramagnetic materials operated in low magnetic fields

  • F. Mishima;Aoi Nagahama;N. Nomura;S. Nishijima
    • 한국초전도ㆍ저온공학회논문지
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    • 제25권3호
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    • pp.13-17
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    • 2023
  • Magnetic separation technology for small paramagnetic particles has been desired for the volume reduction of contaminated soil from the Fukushima nuclear power plant accident and for the separation of scale and crud from nuclear power plants. However, the magnetic separation for paramagnetic particles requires a superconducting high gradient magnetic separation system applied, hence expanding the bore diameter of the magnets is necessary for mass processing and the initial and running costs would be enormous. The use of high magnetic fields makes safe onsite operation difficult, and there is an industrial need to increase the magnetic separation efficiency for paramagnetic particles in as low a magnetic field as possible. Therefore, we have been developing a magnetic separation system combined with a selection tube, which can separate small paramagnetic particles in a low magnetic field. In the previous technique we developed, a certain range of particle size was classified, and the classified particles were captured by magnetic separation. In this new approach, the fluid control method has been improved in order to the selectively classify particles of various diameters by using a multi-stage selection tube. The soil classification using a multi-stage selection tube was studied by calculation and experiment, and good results were obtained. In this paper, we report the effectiveness of the multi-stage selection tube was examined.

Removal of iron scale from feed-water in thermal power plant by magnetic separation - Introduction to chemical cleaning line -

  • Yamamoto, Junya;Mori, Tatsuya;Hiramatsu, Mami;Akiyama, Yoko;Okada, Hidehiko;Hirota, Noriyuki;Matsuura, Hideki;Namba, Seitoku;Sekine, Tomokazu;Mishima, Fumihito;Nishijim, Sigehiro
    • 한국초전도ㆍ저온공학회논문지
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    • 제20권2호
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    • pp.6-10
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    • 2018
  • Removal of iron oxide scale from feed-water in thermal power plant can improve power generation efficiency. We have proposed a novel scale removal system utilizing High Gradient Magnetic Separation (HGMS). This system can be applied to high temperature and pressure area. We have conducted the lab-scale model experiments using ${\varphi}50mm$ filters and it demonstrated high removal efficiency in HGMS, but scale-up of the system is required toward practical use. In this study, we conducted a large scale mock-up HGMS experiment. We used the superconducting solenoidal magnet with ${\varphi}400mm$ bore and demonstrated that our HGMS system can achieve sufficient scale removal capacity that is required to introduce into both off-line and on-line system.

Detection of planetary signals in extremely weak central perturbation microlensing events via next-generation ground-based surveys

  • Chung, Sun-Ju;Lee, Chung-Uk
    • 천문학회보
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    • 제38권2호
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    • pp.72.1-72.1
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    • 2013
  • Even though current microlensing follow-up observations focus on high-magnification events due to the high efficiency of planet detection, it is very difficult to do a confident detection of planets in high-magnification events with extremely weak central perturbations (i.e., the fractional deviation is ${\delta}{\leq}0.02$). For the confident detection of planets in the extremely weak central perturbation events, it is needed both the high cadence monitoring and the high photometric accuracy. A next-generation ground-based observation project, KMTNet (Korea Microlensing Telescope Network), satisfies both the conditions. Here we investigate how well planets in high-magnification events with extremely weak central perturbations are detected by KMTNet. First, we determine the probability of occurrence of events with ${\delta}{\leq}0.02$. From this, we find that for ${\leq}100M_E$ planets in the separation of $0.2AU{\leq}d{\leq}20AU$, events with ${\delta}{\leq}0.02$ occur with a frequency of more than 70%, in which d is the projected planet-star separation. Second, we estimate the efficiency of detecting planetary signals in the events with ${\delta}{\leq}0.02$ via KMTNet. We find that for main-sequence and subgiant source stars, ${\geq}1M_E$ planets can be detected more than 50% in a certain range that has the efficiency of ${\geq}10%$ and changes with the planet mass.

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트레이형 현립분리기의 분리성능에 관한 연구 (Study on the Separation Performance of a Tray-type Paddy Separator)

  • 정창주
    • Journal of Biosystems Engineering
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    • 제5권1호
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    • pp.43-50
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    • 1980
  • The milling plants in Korea have been generally used the paddy-separator that operated in accordance with the principle of sieving action. This type of paddy separator was considered as inefficient, especially in relation to the new high-yielding varieties which have different size characteristics within their varieties and also as compared to traditional varieties. With the installation of modern paddy separator it may be possible to increase the overall milling system efficiency and to reduce the grain loss. This study was intended to identify and define important parameters required for assessing the separation performance of a tray-type paddy separator and to determine the optimum conditions of the inclination of separator-table. The results of the study were summarized as follows : (1) Separation performance can be given by use of many parameters found from the measurement of separator outputs. such as upper-tail recovery $(\varepsilon)$, purity of upper-tail $(\gamma)$ , separation recovery of brown rice $(\alpha)$, separation recovery paddy $(\beta)$, and efficiency of separator $(\epsilon)$, Among these para-meters , $\varepsilon$, $\gamma$, $\alpha$ and $\beta$, were designated , respectively, their independent properties of the paddy separator. In addition, their modes of variation due to a varied inclination of the separation table did not indicated in the same direction . However, the efficiency of separator had an advantage to indicate the overall characteristics of the separator performance with a clear optimum inclination condition of the separator table. (2) The optimum feed rate and maximum efficiency of the separator did not occur at the identical inclination of the separator table. Thus, for its practical operation it is necessary to compromise between the qualitative and quantitative performances of the separator. (3) The optimum setting of the separator table tested in the study showed to occur at its inclination of approximately $26^\circ<$/TEX> for the front and $8^\circ<$/TEX> for lateral.

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Immobilization of Styrene-acrylamide Co-polymer on Either Silica Particles or Inner Surface of Silica Capillary for the Separation of D-Glucose Anomers

  • Ali, Faiz;Kim, Yune Sung;Cheong, Won Jo
    • Bulletin of the Korean Chemical Society
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    • 제35권2호
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    • pp.539-545
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    • 2014
  • Styrene-acrylamide co-polymer was immobilized on porous partially sub-$2{\mu}m$ silica monolith particles and inner surface of fused silica capillary ($50{\mu}m$ ID and 28 cm length) to result in ${\mu}LC$ and CEC stationary phases, respectively, for separation of anomeric D-glucose derivatives. Reversed addition-fragmentation transfer (RAFT) polymerization was incorporated to induce surface polymerization. Acrylamide was employed to incorporate amide-functionality in the stationary phase. The resultant ${\mu}LC$ and CEC stationary phases were able to separate isomers of D-glucose derivatives with high selectivity and efficiency. The mobile phase of 75/25 (v/v) acetonitrile (ACN)/water with 0.1% TFA, was used for HPLC with a packed column (1 mm ID, 300 mm length). The effects of pH and ACN composition on anomeric separation of D-glucose in CEC have been examined. A mobile phase of 85/15 (v/v) ACN/30 mM sodium acetate pH 6.7 was found the optimized mobile phase for CEC. The CEC stationary phase also gave good separation of other saccharides such as maltotriose and Dextran 1500 (MW~1500) with good separation efficiency (number of theoretical plates ~300,000/m).