• Journal of Powder Materials
• /
• v.28 no.5
• /
• pp.389-395
• /
• 2021

Oxide dispersion-strengthened (ODS) steel has excellent high-temperature properties, corrosion resistance, and oxidation resistance, and is expected to be applicable in various fields. Recently, various studies on mechanical alloying (MA) have been conducted for the dispersion of oxide particles in ODS steel with a high number density. In this study, ODS steel is manufactured by introducing a complex milling process in which planetary ball milling, cryogenic ball milling, and drum ball milling are sequentially performed, and the microstructure and high-temperature mechanical properties of the ODS steel are investigated. The microstructure observation revealed that the structure is stretched in the extrusion direction, even after the heat treatment. In addition, transmission electron microscopy (TEM) analysis confirmed the presence of oxide particles in the range of 5 to 10 nm. As a result of the room-temperature and high-temperature compression tests, the yield strengths were measured as 1430, 1388, 418, and 163 MPa at 25, 500, 700, and 900℃, respectively. Based on these results, the correlation between the microstructure and mechanical properties of ODS steel manufactured using the composite milling process is also discussed.

• Corrosion Science and Technology
• /
• v.13 no.5
• /
• pp.178-185
• /
• 2014

Alloy 617 is considered as a candidate Ni-based superalloy for the intermediate heat exchanger (IHX) of a very high-temperature gas reactor (VHTR) because of its good creep strength and corrosion resistance at high temperatures. Helium is used as a coolant in a VHTR owing to its high thermal conductivity, inertness, and low neutron absorption. However, helium inevitably includes impurities that create an imbalance in the surface reactivity at the interface of the coolant and the exposed materials. As the Alloy 617 has been exposed to high temperatures at $950^{\circ}C$ in the impure helium environment of a VHTR, the degradation of material is accelerated and mechanical properties decreased. The high-temperature strength, creep, and corrosion properties of the structural material for an IHX are highly important to maintain the integrity in a harsh environment for a 60 year period. Therefore, an alloy superior to alloy 617 should be developed. In this study, the mechanical and high-temperature corrosion properties for Ni-Cr alloys fabricated in the laboratory were evaluated as a function of the grain boundary strengthening and alloying elements. The ductility increased and decreased by increasing the amount of Mo and Cr, respectively. Surface oxide was detached during the corrosion test, when Al was not added to alloy. However the alloy with Al showed improved oxide adhesive property without significant degradation and mechanical property. Aluminum seems to act as an anti-corrosive role in the Ni-based alloy.

• Journal of the Korea Institute of Building Construction
• /
• v.8 no.5
• /
• pp.53-58
• /
• 2008

This study is to investigate experimentally residual strength properties of the high strength concrete containing the hybrid of nylon and polypropylene fiber at elevated temperature. Test results showed that specimens heated up to $300^{\circ}C$ exhibited similar strength properties to the one at room temperature. This result is significantly different from previous studies. but specimens heated over $400^{\circ}C$ showed dramatic decrease indicating similar tendency. For the residual strength properties, one at $300^{\circ}C$ even increased 10%, which is also different from previous studies, but it significantly decreased in $400^{\circ}C$ as widely expected. Melted pores by organic fibers in concrete specimens was observed with FE-SEM. For the density of concrete in elevated temperature, internal system in $200^{\circ}C$ had even denser than in $20^{\circ}C$, but was collapsed in $400^{\circ}C$.

• Transactions of Materials Processing
• /
• v.14 no.7 s.79
• /
• pp.635-641
• /
• 2005

The crystal structure of magnesium was hexagonal close-packed (HCP), so its formability was poor at room temperature. But formability was improved in high temperature with increasing of the slip planes. Purpose of this paper was to know about the mechanical properties of magnesium alloy (AZ31B), before warm and hot forming process. The mechanical properties were defined by the tension and compression tests in various temperature and strain-rate. As the temperature was increased, yield·ultimate strength, K-value, work hardening exponent (n) and anisotropy factor (R) were decreased. But strain rate sensitivity (m) was increased. As strain-rate increased, yield·ultimate strength, K-value, and work hardening exponent (n) were increased. Also, microstructures of grains fined away at high strain-rate. These results would be used in simulations and manufacturing factor fer warm and hot forming process.

• Proceedings of the Korean Powder Metallurgy Institute Conference
• /
• 1997.04a
• /
• pp.35-35
• /
• 1997

High$\cdot$speed steels (HSS) with a combination of good wear resistance and toughness are finding new, non-cutting applications such as rolls and rollers. In this paper, the research interests are focused on the microstructural evolution of a SMo-6W series high speed steel during HIPping and the effect of HIPping process parameters on its microstructure and properties. HIPping process variables includes; temperature, pressure and hold time. The microstructures of the HIPped HSS were examined by SEM, OM and X-ray diffraction whereas the properties measured were the relative density, hardness, and bend strength at room temperature. In HIPped materials, MC and M6C were the major carbides formed in a matrix of martensite. The effect of powder size on the microstructure and mechanical properties of HIPped materials was insignificant. However, HIPping temperature and hold time strongly affected the carbide size and distribution. The results show that at proper HIPping temperature and pressure conditions, the final products approach the full density ( > 99% RD). The particle boundaries were completely eliminated without an eminent microstructural coarsening. The bend strength was about 2.3 Gpa, which is superior to cast HSS. At excessive HIPping temperatures, rapid carbide coarsening occurred, thus deteriorating the mechanical properties of the P/M steels.

• Journal of Korea Foundry Society
• /
• v.36 no.5
• /
• pp.167-173
• /
• 2016

The effect of various types of heat-treatment on the mechanical properties of cast Alloy 718 has been investigated. Cast Alloy 718 bars were subjected to 'standard heat-treatment'_(SHT), 'HIP (Hot Isostatic Pressing) heat-treatment'_(HHT), and 'HIP-simulated heat-treatment'_(HS). In the absence of long time high temperature heat-treatment, a small amount of Laves phase remained in the 'SHT' specimen, and needle shaped ${\delta}$ precipitated in the vicinity of the Laves phase. Due to the formation of the Laves and ${\delta}$ phases in the 'SHT' specimen, it exhibited lower tensile properties than those of the others_specimens. On the other hand, the Laves phase was completely dissolved into the matrix after 'HHT' and 'HS' treatments. It is known that isostatic pressure reduces the self-diffusion coefficient, because of the lower self-diffusivity under HIP conditions in the interdendritic region, Nb segregation and the high amount of ${\gamma}^{{\prime}{\prime}}$ precipitation that occurs. Due to the higher fraction of coarse ${\gamma}^{{\prime}{\prime}}$ phases, the 'HHT' treated Alloy 718 showed excellent tensile strength.

• Journal of the Korean Ceramic Society
• /
• v.29 no.11
• /
• pp.877-887
• /
• 1992

Tetragonal zirconia powder with 3 mol% Y2O3 mas mixed with up to 30 vol% of ${\beta}$-SiC powders, and the mixtures were hot-pressed at 1500$^{\circ}C$ for 60 min under a pressure of 30 MPa in Ar atmosphere. Flexural strength and fracture toughness were measured at room-and high-temperature (1000$^{\circ}C$). Evolution of microstructure was also conducted to investigate the effects of SiC addition on the properties of 3Y-TZP ceramics. Average grain size of the composites was about 0.5 $\mu\textrm{m}$, and decreased with SiC addition. Both room- and high-temperature mechanical properties of the composites were improved with SiC content. Particularly, high-temperature strength and fracture toughness of 3Y-TZP/30v/o SiC composite were twice as high as those of 3Y-TZP. The hardness of the composites also increased with SiC content and reached maximum value at 3Y-TZP/30v/o SiC composite.

• Proceedings of the Korean Institute of Building Construction Conference
• /
• 2002.11a
• /
• pp.63-66
• /
• 2002

In this study, it does a high volume flyash substituted concrete experiments in two curing temperature circumstances - 35$^{\circ}C$, 2$0^{\circ}C$. High volume flyash concrete is tested in fresh concrete properties and hardeded concrete properties. In the fresh concrete test items, there is slump, air contents, concrete setting tests. 3, 7, and 28 days water curing compressive strength is measured in the hardened concrete test. The purpose of this study is to submit a various flyash concrete data for application to field. The result of this study is that the best strength is developed at the plain concrete cured 2$0^{\circ}C$ and Mixing F43 shows the best strength among specimens which cured at 35$^{\circ}C$

• Proceedings of the Korean Institute of Building Construction Conference
• /
• 2008.11a
• /
• pp.7-12
• /
• 2008

We constructed Seal type waterproofing with adhesive and swelling properties in the field of construction work as yet. But we have many problems of seal type waterproofing with adhesive and swelling properties for construction. Because it has high viscosity, so wokers are too adhered for the work. So, we developed and applied about the high temperature and spray equipments of piston type better than before. We able to be expect that cost reduction and increase construction ability by high temperature and spray equipments of piston type.

• Transactions of Materials Processing
• /
• v.31 no.3
• /
• pp.117-123
• /
• 2022

In this study, a commercial AZ61 magnesium alloy is extruded at 300 ℃ and 400 ℃ and the microstructures, mechanical properties, and high-cycle fatigue properties of the extruded materials are investigated. Both extruded materials have a fully recrystallized microstructure with no Mg₁₇Al₁₂ precipitates. The average grain size and maximum basal texture intensity of the extruded material increase with increasing extrusion temperature. The material extruded at 400 ℃ (AZ61-400) has higher tensile yield strength and lower compressive yield strength than the material extruded at 300 ℃ (AZ61-300) because of the stronger basal texture of the former. Because of coarser grain size, the tensile elongation of AZ61-400 is lower than that of AZ61-300. Despite the differences in microstructures and tensile/compressive properties, the two extruded materials have the same fatigue strength of 110 MPa. This is because the finer grain size of AZ61-300 causes an increase in fatigue strength, but its weaker texture causes a decrease in fatigue strength. In both extruded materials, fatigue cracks initiate at the surface of fatigue specimens at all stress amplitudes tested.