• Journal of the Korean Society for Heat Treatment
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• v.6 no.4
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• pp.213-222
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• 1993

This research was performed to investigate the transformation behavior and shape memory effect of Cu-13.5Al-4.5Ni(wt%) alloy with various aging temperature and time. The results obtained in this study are as follows: Transformation temperature was very increased when aging temperature is at $250^{\circ}C$. The variation of transformation temperature in first reverse transformation cycle and second was very significant, but there was little difference in case of 2nd and 3rd. Transformation temperature at various aging temperature was increased with increasing of aging temperature and time. Microvickers hardness was increased with increasing of aging temperature and time. It was found that ${\alpha}$ and ${\gamma}_2$ phase were created by aging of long time at high temperature.

• Journal of the Korean Society for Heat Treatment
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• v.31 no.5
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• pp.213-219
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• 2018

This study was carried out to investigate the effect of hot forging ratio and solution treatment temperature on the mechanical properties of incoloy 825 alloy. With an increasing of the hot forging ratio, grain size and range of grain size was decreased. With an increasing of the solution treatment temperature after 90% forging, grain size and range of grain size was increased. Cr carbides and Ti nitrides was precipitated at below $900^{\circ}C$ and volume fraction of precipitate was increased with an decreasing of the solution treatment temperature. With an increasing of the hot forging ratio, hardness, tensile strength and elongation, toughness was increased. With an increasing of the solution treatment temperature after 90% forging, hardness and strength was increased, elongation and toughness was decreased by grain refinement. With an increasing of the forging ratio, effect of solution treatment temperature on the hardness, strength and elongation was small, but on the toughness was large.

• Journal of the Korean Society for Heat Treatment
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• v.26 no.5
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• pp.233-240
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• 2013

Rapid and homogeneous heating in heat treatment has been a challenging engineering issue throughout a heating temperature over $1,000^{\circ}C$. Induction heating has been widely used in field of heat treatment compared with conventional heating system. Advantages in homogeneous heating, simple fabrication, and repeatable use can be efficiently made with the induction heater. In this paper, numerical analysis of an induction coil system for heat flux gauge heating is performed. The effect of configuration on the heating performance was considered in various cases of the coil radius, distance between the winding, relative height difference between the heat flux gauge and the coil, and the applied current frequency. Temperature distribution within the heat flux gauge at frequency-steady state was calculated with a finite element method. Sensitivity analysis was also performed and the relative importance of 2 key parameters; coil radius, distance between the winding, were taken as main contributors for induction heating.

• Journal of the Korean Society of Fisheries and Ocean Technology
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• v.48 no.1
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• pp.20-28
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• 2012

The monofilament with 0.304mm of diameter was produced using a polybutylene succinate (PBS) resin, and a gill net was made by it. We investigated the impact of heat setting temperature on the mechanical properties, knot state and height of gill net. Heat treatment was carried out using the high pressure steam machine for 20 minutes at temperature of $55^{\circ}C$, $60^{\circ}C$, $70^{\circ}C$ and $75^{\circ}C$. Before heat treatment, the strength and elongation of PBS monofilament were estimated to be $48.1kg/mm^2$, 23.8% at unknot, $37.6kg/mm^2$, 18.8% at single knot, $26.6kg/mm^2$, 22.9% at double knot in dry condition, respectively. The strength and elongation of PBS monofilament with double knot were decreased as heat setting temperature increased, and the decreasing rate of strength was showed to be higher than that of elongation. It was not found any differences in strength and elongation of PBS monofilament yarn with double knot at the $65^{\circ}C$ and $70^{\circ}C$ of heat setting temperature by 5% significance of T-test, but there was a significant difference at the $70^{\circ}C$ and $75^{\circ}C$ of heat setting temperature. The net's height and length from leg to leg appeared no differences at the $70^{\circ}C$ and $75^{\circ}C$ of heat setting temperature. In results, it was investigated that the PBS monofilament gill net with the maximized physical properties could be manufactured at $70^{\circ}C$ of heat setting temperature using a high pressure steam machine for 20 minutes.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2008.10a
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• pp.431-434
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• 2008

In the present study, direct quenching of alloyed steel after hot forging was simulated using commercial finite element program, $FORGE^{TM}$. A typical heat treatment of alloyed steels consists of quenching for hard martensite and subsequent tempering for toughness. In the practice, forgings which cool down to room temperature are heated to temperature of austenite regime. As investigated in the present study, direct quenching of hot forged stock would be beneficial in terms of energy saving. This process has already been propose and termed as ausforging or forged hardening. However, it is well known that quenching temperature would be the most critical factor to control heat treated forging properties. And it is very difficult to control quenching temperature when forged stock gets directly quenched after forging. In this study, we have calculated final forging temperature of stock. Also, quenching simulation was conducted using a series of material parameter which were also calculated using JMATpro, a commercial program for physical properties of materials.

• Korean Journal of Materials Research
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• v.16 no.5
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• pp.312-317
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• 2006

Binary skutterudite $CoSb_3$ compounds were prepared by the encapsulated induction melting (EIM) process, and their thermoelectric, microstructural and mechanical properties were examined. Single-phase ${\delta}-CoSb_3$ was successfully produced by the EIM and subsequent heat treatment at 773 K-873 K for 24 hours in vacuum. Seebeck coefficient increased with increasing heat treatment temperature up to 673 K, showing the positive signs in the range of measuring temperature. However, the samples heat-treated at 773 K-873 K showed negative Seebeck coefficient from room temperature to 400 K, while it showed positive signs above 400 K. Electrical resistivity decreased with increasing temperature, showing typical semiconducting conductivity. Thermal conductivity decreased drastically with increasing heat-treatment temperature. This is closely related with the phase transition to ${\delta}-CoSb_3$.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2004.08a
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• pp.27-36
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• 2004

Contemporary objectives for steel rod rolling processing are increasingly complex and often contrasting i.e. obtaining a desired product with optimum combination of properties such as strength, toughness and formability at lower cost. Low-alloy steel rods have been produced with several heat treatments for drawing and forging processes at room temperature. In order to reduce these heat treatments much of the researches concerning of high temperature mechanical behavior of steel rods have been conducted at wire rod mill of POSCO. In this present work, optimizations of rolling temperature and cooling rate for JS-SCM435 are performed to eliminate softening heat treatment(Low Temperature Annealing) for drawing process. The results from the optimization changed the microstructure of rods after rod rolling from Bainite with high tensile strength of 1000Mpa to Pearlite and Ferrite with appropriate strength of 750Mpa that is equivalent tensile strength after softening heat treatment.

• Journal of the Korean Society for Heat Treatment
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• v.33 no.1
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• pp.13-19
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• 2020

Annealing effects on the properties of Bi-doped ZnO thin films were investigated. Bi- doped ZnO thin films were deposited on quartzs substrates at 300℃ by using radio-frequency magnetron sputtering system. Post heat treatments at 600, 700, and 800℃ were performed to evaluate the effect of annealing temperatures on the structural, optical, and electrical properties of Bi-doped ZnO thin films. FE-SEM images showed the dramatic surface morphology changes by rearrangement of elements at high heat treatment temperature of 800℃. X-ray diffraction analysis indicated that the peaks of the Bi-doped ZnO thin films were same as the peaks of the (002) planes of ZnO peak-positioned at 2θ=34.0° and peak intensities and FWHMs were improved as the annealing temperatures increased. The optical transmittance was improved with increasing annealing temperatures and was over 80% in the wavelength region between 435 and 1100 nm at the annealing temperature of 700 and 800℃. With increasing annealing temperature, the electron concentrations and electron mobilities were increased. On the other hand, electric resistivity of the films were decreased with increasing annealing temperatures. These results showed that the heat treatment temperature is an important parameter to improve the structural, optical, and electrical properties of Bi-doped ZnO thin films.

• Korean Journal of Metals and Materials
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• v.50 no.4
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• pp.316-323
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• 2012

The aim of this study is to investigate the effect of post heat treatment on bonding properties of roll cladded Ti/MS/Ti materials. First grade Ti sheets and SPCC mild steel sheets were prepared and then Ti/MS/Ti clad materials were fabricated by a cold rolling and post heat treatment process. Microstructure and point analysis of the Ti/MS interfaces were performed using the SEM and EDX Analyser. Diffusion bonding was observed at the interfaces of Ti/MS. The thickness of the diffusion layer increased with post heat treatment temperature and the diffusion layer was verified as having $({\epsilon}+{\zeta})+({\zeta}+{\beta}-Ti)$ intermetallic compounds at $700^{\circ}C$ and an $({\zeta}+{\beta}-Ti)$ intermetallic compound at $800^{\circ}C$, respectively. The micro Knoop hardness of mild steel decreased with post heat treatment temperature; however, those of Ti decreased at a range of $500{\sim}600^{\circ}C$ and showed a uniform value until $800^{\circ}C$ and then increased rapidly up to $900^{\circ}C$. The micro Knoop hardness value of the diffusion layer increased up to $700^{\circ}C$ and then saturated with post heat treatment. A T-type peel test was used to estimate the bonding forces of Ti/Mild steel interfaces. The bonding forces decreased up to $800^{\circ}C$ and then increased slightly with post heat treatment. The optimized temperature ranges for post heat treatment were $500{\sim}600^{\circ}C$ to obtain the proper formability for an additional plastic deformation process.

• Journal of the Korean Society for Heat Treatment
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• v.11 no.4
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• pp.258-267
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• 1998

For the purpose of investigating the growth characteristics and composition of nitrides, gas nitridings of the austenitic stainless steel, STR 36 heat resisting steel and martensitic stainless steel are investigated at the temperature ranges between $500^{\circ}C$ and $675^{\circ}C$ for 5hours under the $75%NH_3+5%CO_2+20%$Air gas atmosphere. When gas nitriding the austentic stainless steel and STR 36 heat resisting alloy, the abnormal growth behavior of compound layer deviating from the conventional diffusion law with increasing temperature appears, while the compound layer of martensitic stainless steel shows the normal diffusional growth behavior. From the examination of microstructure, X-ray diffraction and hardness test, it is concluded that the abnormal growth behavior of compound layer with increasing temperature induces from the formation and dissolution of CrN and ${\gamma}^{\prime}-Fe_4N$ at the nitriding temperature ranges of $600{\sim}650^{\circ}C$.