• 열처리공학회지
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• 제13권6호
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• pp.405-411
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• 2000

The effects of added elements, such as Co or Nb, on wear properties of high speed steel by powder metaliurgy(PM-HSS) had been eluminated in auther's previous paper. In addition, it is generally known that the wear properties of materials have been influenced by heat-treating conditions as well. Therefore, a study has been done to clarify the effects of heat-treating conditions on wear properties of PM-HSS. The wear tests have been performed under the same conditions as the previous paper using heat-treated PM-HSS(5%Co-1%Nb) with different quenching and tempering temperatures. The result of this paper shows that wear resistance of PM-HSS is improved with relatively high quenching temperature. However, tempering temperature is not sensitive to the wear resistance in the range of high quenching temperature. It may be deduced by the fact that the shear strength of matrix by strengthening mechanisms due to not only the quenching aging but also dispersion-hardening is improved.

• Journal of Advanced Marine Engineering and Technology
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• 제26권1호
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• pp.90-98
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• 2002

In this paper, the annealing heat treatments for the best corrosion resistant of Ti(Grade 2) were studied in a 3.5% NaCl solution by electrochemical methods. The annealing heat treatments were accomplished at 650, 700 and $750^{\circ}C$ with different time of 30min., 1hour and 2 hours in a vacuum condition. The obtained results are: 1) in the case of solution heat treated $930^{\circ}C$ for 2 hours in a vacuum and air, the corrosion potentials were -348.7 and -567. 1mV, and current densities 2.32 and $22.62\mu\textrm{A}$, respectively, 2) as increase both annealing heat treatment temperature 650, 700, $750^{\circ}C$ and time 30min., 1 hour, 2 hours, the corrosion potential were decreased, whereas corrosion current density increased, 3) in the case of cyclic polarization, the measured charges were increased as increasing solution heat treatment temperature and time, 4) on the bases of corrosion potential, current density and charge, the best annealing temperature and time were measured as $700^{\circ}C$ and 30min. for Ti(Grade 2) material.

• 한국식품저장유통학회:학술대회논문집
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• 한국식품저장유통학회 2003년도 제23차 추계총회 및 국제학술심포지움
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• pp.167.1-167
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• 2003

To maintain high quality and to extend the shelf life of intact and minimally processed apple cubes, the effect of heat shock on the texture and color of apple cubes (Fuji) was evaluated in this study. After peeled and cored, the apples were cut into cubes of 1.5 cm. The heat shock was immersion in heated water from 25$^{\circ}C$ to 95$^{\circ}C$ in 10$^{\circ}C$ increments for 2 min and cooling to storage temperature as soon as possible after heat treatment. The effect of heat treatment in terms of color and texture measurements with respect to time was investigated, respectively during 7 days storage at in LDPE film bags without sealing at 4$^{\circ}C$, and 95% relative humidity air. Results suggest that heat shock (55$^{\circ}C$, 2 min) may have effectively delayed browning, and there were significant changes in color of apple cube when the temperature of heat shock is above 75$^{\circ}C$. And hardness, stiffness and firmness, which were used to describe texture, behaved similarly in the textural qualities. It was shown that the texture of the apple cubes was decreased with temperature increase. The value of them were most decreased to 70% of the initial ones after treated with 85$^{\circ}C$ and 95$^{\circ}C$ on the lust day.

• 열처리공학회지
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• 제34권5호
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• pp.226-232
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• 2021

The relationship between precipitation and coefficient of thermal expansion of Al-6%Si-0.4%Mg-0.9%Cu-(Ti) alloy (in wt.%) after various heat treatments were studied by the thermodynamic analyzer (TMA) and differential scanning calorimetry (DSC). Solution heat treatment of the alloy was carried out at 535℃ for 6 h followed by water quenching, and the samples were artificially aged in the air at 180℃ and 220℃ for 5 h. The coefficient of thermal expansion (CTE) curve showed some residual strain and decreased with increasing aging temperature. The CTE curves changed sharply in the temperature range of 200℃ to 400℃, and the corresponding peak shifted for the aged samples due to the change in the precipitation behavior of the secondary phase. These transformation peaks in the aged sample are related to the volume of the precipitation of the Si phase as determined by DSC analysis. The change in CTE is mainly caused by the precipitation of the Si phase in the Al-Si alloy, and the size of the change occurs simultaneously with the size of the precipitate.

• 소성∙가공
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• 제27권2호
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• pp.123-129
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• 2018

In the present study, the mechanical behavior of the spray-formed high speed steel was investigated employing the internal variable theory of inelastic deformation. Special attention was focused on the effect of the microstructure evolution during the hot working process, such as the distribution of carbides to provide a basic database for the production condition of high speed steels with excellent properties. The billets of high speed steel ASP30TM were fabricated by a spray forming, and the subsequently hot-rolled and heat-treated process to obtain uniformly distributed carbide structure. As noted the spray-formed high speed steel showed relatively coarser carbides than hot-rolled and heat-treated one with fine and uniformly distributed carbide structure. The step strain rate tests and high temperature tensile tests were carried out on both the spray-formed and the hot-rolled specimens, to elucidate their high temperature deformation behavior. The spray-formed high speed steel showed much higher flow stress and lower elongation than the hot-rolled and heat-treated steel. During the tensile test at $900^{\circ}C$, the interruption of the deformation for 100 seconds was conducted to reveal that the recovery was a main dynamic deformation mechanism of spray formed high speed steel. The internal variable theory of the inelastic deformation was used to analyze data from the step strain rate tests, revealing that the activation energies for hot deformation of as-spray-formed and hot-worked steels, which were 157.1 and 278.9 kJ/mol, and which were corresponding to the dislocation core and lattice diffusions of ${\gamma}-Fe$, respectively.

• 열처리공학회지
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• 제21권5호
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• pp.244-250
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• 2008

This study has investigated the surface phase change, hardness variation, surface precipitates, nitrogen content and corrosion resistance in STS 431 (17Cr-2Ni-0.2C-0.01Nb) martensitic stainless steel after high temperature gas nitriding (HTGN) treatment at the temperature range between $1050^{\circ}C$ and $1150^{\circ}C$. The HTGN-treated surface layer appeared $Cr_2N$ of rod type, carbo-nitride of round type and fine precipitates in the austenite matrix. On the other hand the interior region where the nitrogen was not permeated, exhibited martensite phase. The surface hardness showed 250~590 HV, depending on the HTGN treatment conditions, while the interior martensitic phase represented 520 HV. The permeation depth of nitrogen increased with increasing the HTGN-treated temperature. The nitrogen concentration of the surface layer appeared approximately ~0.17% at $1100^{\circ}C$. On comparing the corrosion resistance between solution-annealed and HTGN-treated steels, the corrosion resistance of HTGN-treated steel was superior to that of solution-annealed specimens.

• 한국주조공학회지
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• 제36권5호
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• pp.167-173
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• 2016

The effect of various types of heat-treatment on the mechanical properties of cast Alloy 718 has been investigated. Cast Alloy 718 bars were subjected to 'standard heat-treatment'_(SHT), 'HIP (Hot Isostatic Pressing) heat-treatment'_(HHT), and 'HIP-simulated heat-treatment'_(HS). In the absence of long time high temperature heat-treatment, a small amount of Laves phase remained in the 'SHT' specimen, and needle shaped ${\delta}$ precipitated in the vicinity of the Laves phase. Due to the formation of the Laves and ${\delta}$ phases in the 'SHT' specimen, it exhibited lower tensile properties than those of the others_specimens. On the other hand, the Laves phase was completely dissolved into the matrix after 'HHT' and 'HS' treatments. It is known that isostatic pressure reduces the self-diffusion coefficient, because of the lower self-diffusivity under HIP conditions in the interdendritic region, Nb segregation and the high amount of ${\gamma}^{{\prime}{\prime}}$ precipitation that occurs. Due to the higher fraction of coarse ${\gamma}^{{\prime}{\prime}}$ phases, the 'HHT' treated Alloy 718 showed excellent tensile strength.

• 한국세라믹학회지
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• 제29권2호
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• pp.161-165
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• 1992

Nonlinear exponents and electron trap density variations were observered in ZnO-Bi2O3-MnO2 ternary ZnO varistors as a function of heat treatment temperature. Three kinds of ZnO varistor compositions were selected; i.e. 99.0 ZnO-0.5 Bi2O3-0.5 MnO2, 98.5 ZnO-1.0 Bi2O3-0.5 MnO2, and 98.0 ZnO-1.5 Bi2O3-0.5 MnO2 in mol%. Sintering was done at 1150$^{\circ}C$ for three hours, and heat treatments were done at 500$^{\circ}C$, 700$^{\circ}C$, and 900$^{\circ}C$. When heat treated at 500$^{\circ}C$, nonlinear exponents were increased regardless of the Bi2O3 amount. Increasing heat treatment temperature above 500$^{\circ}C$ resulted in lowering nonlinear exponents. Nonlinear exponents seem to be related to the 0.17 and 0.33 eV electron traps which are possibly of intrinsic origin.

• Carbon letters
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• 제3권1호
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• pp.13-16
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• 2002

The modification of coal-tar pitch has been carried out by heat treatment of pitch at different temperatures in the range ($300^{\circ}-400^{\circ}C$) for different times (2-5 hrs) in air and nitrogen. The pitch heat treated in air at lower temperature ($300^{\circ}C$) exhibit increase in softening point by $20^{\circ}C$ as compared to only $2^{\circ}C$ when treated in nitrogen. The changes are faster in air than in pure nitrogen. Pitch as such as well as after heat treatment were further treated with metal complexes by solution route. Silver intake has been found to increase from 0.5 to 0.8 % in nitrogen treated pitch while the uptake is found to decrease for pitches treated in air at $350^{\circ}C$ for 5 hrs. Experiments have also been made to incorporate silver into PAN and PAN-ox fibers through solution route. The metal intake has been found to be more in PAN-ox fibers than in PAN as such. Metal loaded carbon composites have been made by using metal loaded fibers as well as cokes. These composites as such exhibit higher surface oxygen complexes but decrease after activation.

• 공업화학
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• 제18권2호
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• pp.194-198
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• 2007

실온에서 베니어에 ammonium chloride, ammonium sulfate, monoammonium phosphate, 그리고 diammonium phosphate와 같은 암모늄염으로 도포하고, 도포된 베니어의 물리적 성질과 가연성을 조사하였다. 암모늄염로 처리된 베니어의 가연성을 평가하기 위해서, ISO 5660-1 표준에 따른 콘칼로리미터를 이용하여 베니어의 열방출율을 측정하였다. 암모늄염으로 도포된 베니어판은 미처리된 순수 베니어판에 비하여 가연성을 감소시켰다. 도포된 베니어의 flashover 가능성은 R. V. Petrella에 의한 분류 방법에 따라서 착화시간과 최대열방출율을 이용하여 시험하였다. 비중측정 결과 ammonium sulfate로 처리한 베니어의 비중만 미처리 베니어보다 더 높았다. 또한 암모늄염으로 도포된 베니어는 무처리된 순수 베니어보다 낮은 평형함수율을 보였다.