• Title/Summary/Keyword: Heat-treated temperature

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Effect of Heat-treatment on the Electrical Properties of Polyurethane Resin (열처리조건이 폴리우레탄수지의 전기적 특성에 미치는 영향에 관한 연구)

  • Cho, Jung-Soo;Kwak, Young-Soon;Lee, Jong-Ho;Kwak, Byung-Ku
    • Proceedings of the KIEE Conference
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    • 1987.11a
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    • pp.293-295
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    • 1987
  • This paper deals with the dielectric properties dielectric breakdown strength and mechanical tensile properties according to heat - treatment condition of polyurethane resin. This resin is heat - treated over a range of temperature from $50^{\circ}C$ to $150^{\circ}C$. It is shown that the dielectric dissipation factor decreases with increase of heat - treatment temperature of the sample exept for the sample heat - treated at $150^{\circ}C$. The maximum dielectric breakdown strength is appeared for the sample heat - treated for 10 hours at $100^{\circ}C$, after curing for 24 hours at room temperature. The optimal heat - treatment condition in the view point of the electrical and mechanical properties is appeared for the sample heat - treated for 10 hours at $100^{\circ}C$, after curing for 24 hours at room temperature.

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PTCR Characteristics of BaTiO$_3$Thin Films made by rf/dc Magnetron Sputter Technique

  • Song, Min-Jong;So, Byung-Moom;Kim, Tae-Wan
    • Transactions on Electrical and Electronic Materials
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    • v.1 no.2
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    • pp.28-31
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    • 2000
  • BaTiO$_3$cerameic thin films doped with Mn were manufactured by rf/dc magnetron sputter technique. We have investigated crystal structure, surface morphology and PRCR(positive-temperature coefficient of resistance) characteristics of the specimen depending on second heat-treatment temperature. Second heat treatment of the specimen were performed in the temperature range of 400 to 1350$\^{C}$ X-ray diffraction patterns of BaTiO$_3$ thin films show that the specimen heat treated below 600$\^{C}$ is an amorphous phase and the one heat treated above 1100$\^{C}$ forms a poly-crystallization . In this specimen heat-treated at 1300$\^{C}$, a lattice constant ratio(c/a) was 1.188. Scanning electron microscope(SEM) image of BaTiO$_3$ thin films of the specimen heat treated in between 900 and 1100$\^{C}$ shows a grain growth. At 1100$\^{C}$, the specimen stops grain-growing and becomes a poly-crystallization . A resistivity-temperature characteristics of the specimen depends on the doping concentrations of Mn. A resistivity ratio between the value at room temperature and the one above Curie temperature was 10$^4$ for pure BaTiO$_3$ thin films and 10$\^$5/ fo BaTiO$_3$ : additive 0.127mol% MnO

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The Study for the Crystallization Behavior of Conventionally Heated and Microwave Heat-treated Inorganic Polymers (재래식 열과 마이크로파 에너지에 의해 열처리된 무기고분자의 결정화 거동에 관한 연구)

  • 박성수;차무경;류봉기;신학기;박희찬
    • Journal of the Korean Ceramic Society
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    • v.34 no.9
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    • pp.935-940
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    • 1997
  • This study investigated the crystallization behavior in PbO-ZnO-B2O3-TiO2 system sealing glass, inorganic polymer heat-treated by conventional heat and microwave energy. After determining heat-treated temperature for crystallization and characteristic points by DTA analysis, samples were heat-treated in a classical electric furnace and a home-style microwave oven (LG Electronic Co., 2.45 GHz, 700 W). A microwave heat-treated sample had the growth of PbTiO3 crystal at 45$0^{\circ}C$, 2$0^{\circ}C$ lower than that of a conventionally heat-treated sample. Also, it had crystallinity about 20% higher than the conventionally heat-treated sample. At 49$0^{\circ}C$, the size of PbTiO3 crystal in the conventionally heat-treated sample was larger than that in the microwave heat-treated sample due to longer heat-treated time.

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Temperature Classification of Heat-treated Metals using Pattern Recognition of Ultrasonic Signal (초음파 신호의 패턴 인식에 의한 금속의 열처리 온도 분류)

  • Im, Rae-Muk;Sin, Dong-Hwan;Kim, Deok-Yeong;Kim, Seong-Hwan
    • The Transactions of the Korean Institute of Electrical Engineers A
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    • v.48 no.12
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    • pp.1544-1553
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    • 1999
  • Recently, ultrasonic testing techniques have been widely used in the evaluation of the quality of metal. In this experiment, six heat-treated temperature of specimen have been considered : 0, 1200, 1250, 1300, 1350 and 1387$^{\circ}C$. As heat-treated temperature increases, the grain size of stainless steel also increases and then, eventually make it destroy. In this paper, a pattern recognition method is proposed to identify the heat-treated temperature of metals by evidence accumulation based on artificial intelligence with multiple feature parameters; difference absolute mean value(DAMV), variance(VAR), mean frequency(MEANF), auto regressive model coefficient(ARC), linear cepstrum coefficient(LCC) and adaptive cepstrum vector(ACV). The grain signal pattern recognition is carried out through the evidence accumulation procedure using the distances measured with reference parameters. Especially ACV is superior to the other parameters. The results (96% successful pattern classification) are presented to support the feasibility of the suggested approach for ultrasonic grain signal pattern recognition.

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Effect of Heat Treatment on the Physical Properties of LM PET Jacquard Fabrics (저융점 폴리에스터 자카드직물의 물성에 대한 열처리 효과)

  • Lee, Sun Young;Kim, Jeong Hwa;Kim, Eui Hwa;Lee, Jung Soon;Lee, Seung Goo
    • Textile Coloration and Finishing
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    • v.25 no.3
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    • pp.206-214
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    • 2013
  • There has been an increasing demand for high performance and energy-saving of blind. In order to develop the eco-friendly blind textiles, heat treatment process has been utilized for LM(Low Melting) polyester fabrics and the changes of the physical properties of the treated fabrics were examined according to temperature of heat treatment. Morphology, surface reflectance, contact angle, luster, thermal property and mechanical property of heat treated LM polyester fabrics were investigated. As results, morphology analysis of thermal treated fabrics confirmed that degree of fusion of LM polyester yarns improved with increase of temperature. Surface reflectance of thermal treated fabrics decreased with increase of temperature. Luster and contact angle of a water droplet on thermal treated fabrics increased slightly with increase of temperature. The mechanical properties of the fabrics by KES-FB system were found to be temperature-dependent and especially, bending and shear properties among them were highly related to temperature.

Effects of Preheating Treatment on Physicochemical Properties of Brined Cucumbers (예열처리에 따른 취청오이의 염장 중 특성)

  • 박미원
    • Journal of the East Asian Society of Dietary Life
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    • v.14 no.3
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    • pp.283-287
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    • 2004
  • To investigate the effects of preheating treatment on the properties of salt-preserved cucumber, cucumber were heated in the warm water to 40, 60, and 75$^{\circ}C$ for 15 min. Thereafter, cucumbers were cooled and the ratios of cucumbers: water was adjusted to 1:1.2(w/w) and salt was added to have final salt concentration of 12%. The group which was heated to 6$0^{\circ}C$ showed the highest scores on hardness followed by 4$0^{\circ}C$, no-heat, and 75$^{\circ}C$ treated groups after 60 days of salt-preservation. The yellowness on the surface of cucumber peels was getting intense as temperature was increased during heat treatment, which resulted in the most intense yellowness in no-heat and 4$0^{\circ}C$ treated groups. The intensities of greeness and redness of the groups also differed according to different temperature applied during heat treatments. Regardless of heat treatment, no difference in the absorbance of isopropyl alcohol extracts were found. Activities of pectinesterase were the highest in 6$0^{\circ}C$ treated group followed by 4$0^{\circ}C$, 75$^{\circ}C$, and no-heat treated group until 60 days of preservation, while activities of polygalacturonase in 4$0^{\circ}C$ and 6$0^{\circ}C$ treated groups were lower.

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Effect of crystallinity on the electrochemical properties of carbon black electrodes

  • Yoo, Hye-Min;Heo, Gun-Young;Park, Soo-Jin
    • Carbon letters
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    • v.12 no.4
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    • pp.252-255
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    • 2011
  • Carbon-based electric double-layer capacitors are being evaluated as potential energy-storage devices in an expanding number of applications. In this study, samples of carbon black (CB) treated at different temperatures ranging from $650^{\circ}C$ to $1100^{\circ}C$ were used as electrodes to improve the efficiency of a capacitor. The surface properties of the heat-treated CB samples were characterized by X-ray photoelectron spectroscopy and X-ray diffraction. The effect of the heat-treatment temperature on the electrochemical behaviors was investigated by cyclic voltammetry and in galvanostatic charge-discharge experiments. The experimental results showed that the crystallinity of the CBs increased as the heat-treatment temperature increased. In addition, the specific capacitance of the CBs was found to increase with the increase in the heat-treatment temperature. The maximum specific capacitance was 165 $F{\cdot}g-1$ for the CB sample treated at $1000^{\circ}C$.

The Effect of Solid Solution Heat-Treatment Temperature on the Tensile Property in Intermediate Thermo-Mechanical Treated Al-Li Alloys (중간가공열처리한 AI-Li계 합금의 인장성질에 미치는 용체화처리온도의 영향)

  • Yoo, C.Y.;Lee, K.B.
    • Journal of the Korean Society for Heat Treatment
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    • v.4 no.1
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    • pp.37-41
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    • 1991
  • In this study, the effect of solution treatment temperature on the tensile property in intermediate thermo-mechanical treated Al-Li alloys are investigated. After the intermediate thermo-mechanical treated Al-Li, Al-Li-Mg and Al-Li-Mg-Zr alloys were solution treated at various temperatures (500, 520 and $540^{\circ}C$), these were aged at $190^{\circ}C$, $240^{\circ}C$ and tested tensile properties. The results obtained from the experiment are as follows ; 1) The optimum solution heat-treatment temperature is $540^{\circ}C$ for a Al-Li alloy, and the recrystallized grain size is about $70{\mu}m$. 2) The optimum solution heat-treatment temperature is $500^{\circ}C$ for a Al-Li-Mg alloy, and the recrystallized grain size is the most coarse in all alloys. 3) The tensile property is independent of the solution treatment temperature in a Al-Li-Mg-Zr alloy, and the recrystallized grain size is the finest owing to addition of Zr.

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Effects of Vacuum Heat Treatment and Salt bath Heat Treatment Conditions on Mechanical Properties of High Speed tool Steel (금속도 공구강의 기계적 성질에 미치는 진공열처리와 염욕열처리 조건의 영향)

  • Kim, Je-Don;Kim, Kyung-Sik
    • Journal of the Korean Society for Heat Treatment
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    • v.26 no.1
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    • pp.7-13
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    • 2013
  • Vacuum heat treatment(indirect heating method) has long exposure time at high temperature and low quenching rate. Contrarily salt bath heat treatment (direct heating method) has short exposure time at high temperature and fast cooling rate. With these different features of processes, mechanical properties such as hardness, tensile strength and impact strength of products show very different results. In this study, Salt bath heat treated products showed higher tensile strength and impact strength than vacuum heat treated products but hardness was not much different. These lower mechanical properties of vacuum heat treated products are due to differences in heat process and secondary hardening with high temperature tempering process. Consequently, It indicates that salt bath heat treatment is better way than vacuum heat treatment for product to have high mechanical properties.

Prediction of Microstructure and Hardness of the Ductile Cast Iron Heat-treated at the Intercritical Temperatures (임계간 온도에서 열처리한 구상흑연주철의 미세조직 및 경도 예측)

  • Nam-Hyuk Seo;Jun-Hyub Jeon;Soo-Yeong Song;Jong-Soo Kim;Min-Su Kim
    • Journal of Korea Foundry Society
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    • v.43 no.6
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    • pp.279-285
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    • 2023
  • In order to predict the mechanical properties of ductile cast iron heat treated in an intercritical temperature range, samples machined from cast iron with a tensile strength of 450 MPa were heat-treated at various intercritical temperatures and air-cooled, after which a microstructural analysis and Brinell hardness test were conducted. As the heat treatment temperature was increased in the intercritical temperature range, the ferrite fraction in the ductile cast iron decreased and the pearlite fraction increased, whereas the nodularity and nodule count did not change considerably from the corresponding values in the as-cast condition. The Brinell hardness values of the heat-treated ductile cast iron increased gradually as the heat treatment temperature was increased. Based on the measured alloy composition, the fraction of each stable phase and the hardness model from the literature, the hardness of the ductile cast iron heat treated in the intercritical temperature range was calculated, showing values very similar to the measured hardness data. In order to check whether it is possible to predict the hardness of heat-treated ductile cast iron by using the phase fraction obtained from thermodynamic calculations, the volumes of graphite, ferrite, and austenite in the alloy were calculated for each temperature condition. Those volume fractions were then converted into areas of each phase for hardness prediction of the heat-treated ductile cast iron. The hardness values of the cast iron samples based on thermodynamic calculations and on the hardness prediction model were similar within an error range up to 27 compared to the measured hardness data.