• 열처리공학회지
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• 제12권2호
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• pp.117-128
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• 1999

This study was carried out to investigate the surface characteristics of SCM440 steel nitrided with various nitrogen contents for 7 hours at $520^{\circ}C$ by using micro-pulse plasma nitriding apparatus of hot wall type. The effects of oxidation treatment was also investigated on plasma nitrided in 30% nitrogen and post oxidized SCM440 steel at $500^{\circ}C$ in $H_2O$ atmosphere. The ${\gamma}^{\prime}-Fe_4N$ and ${\varepsilon}-Fe_{2-3}N$ phases were detected in compound layer of the nitrided steel. As the content of nitrogen in plasma gas increased with 30, 50, 70% on the micro-pulse plasma nitriding for SCM440 steel, the thickness of compound, diffusion layer and the surface hardness were increased. From the wear test results, the best wear resistance was appeared in the condition of ductile ${\gamma}^{\prime}-Fe_4N$ phase formed specimen at 30% nitrogen, whereas that of the treated with 50% and 70% nitrogen decreased owing to the exfoliation of brittle ${\varepsilon}-Fe_{2-3}N$ phase in the compound layer. On the nitrided and subsequently oxidized SCM440 steel, the surface layer consisted of $Fe_3O_4$, ${\gamma}^{\prime}-Fe_4N$, and ${\varepsilon}-Fe_{2-3}N$ phases. In these treatments, the dissolution of nitrides affect hardness and hardening depth in compound and diffusion layers. For the nitrided in 30% nitrogen and post oxidized specimen at $500^{\circ}C$ for 1 hour, the wear resistance was lower than that of the only nitrided one in 30% nitrogen but higher than those of the nitrided ones in 50 and 70% nitrogen.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.597-598
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• 2006

Gas filtration at high temperature from industrial processes offers various advantages such as increasing process efficiency, improving heat recovery and materials resource recovery, etc. At the same time, it is an advanced environment protection technology. This paper describes a newly developed metallic filter element. The manufacturing process of sintered $Fe_3Al$ metallic powder and the mechanical and filtration characteristics of this filter element were investigated. In this work, the phase constituent changes of the $Fe_3Al$ powder during sintering were studied. The newly developed filter elements were found to have excellent corrosion resistance, good thermal resistance, high strength and high filtration efficiency.

• 열처리공학회지
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• 제29권6호
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• pp.284-291
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• 2016

High temperature alloy steel such as Ni-Cr-Mo-V material has excellent properties of high strength and high heating resistance. It has been used for several military weapon components such as gun barrel of a warship, turbine rotor and turbine disk for nuclear power plant. Being curious about this material required excellent wear resistance and durability in extreme environmental conditions. A dry wear test at the ambient air and Ar gas conditions in the room temperature were performed in this study. What's more a lubricant wear test at different temperature was conducted. In addition that DLC was coated on Ni-Cr-Mo-V alloy steel substrate with a thickness of $3{\mu}m$, a property of it was compare with lubricant conditions. All the coefficient of friction and wear volume, comparing with DLC coated specimens. The test parameters were selected as follows: 10 N for normal load; 80 rpm for sliding wear speed; and 300 m for the sliding wear distance.

• Corrosion Science and Technology
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• 제19권1호
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• pp.37-42
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• 2020

Even though 304 low-carbon (304L) stainless steel was developed to enhance the resistance to intergranular corrosion and stress corrosion cracking, it is occasionally subject to degradation in harsh environments. The degree of sensitization (DOS) of 304L stainless steel was studied as a function of sensitization using a double-loop electrochemical potentiokinetic reactivation (DL-EPR) method. Sensitizing heat treatment was performed in an Ar atmosphere at 500℃, 600℃, and 700℃, with heat treatment times varying from 0 to 96 h. DOS was measured by the ratio of the peak current density value of the forward scan to that of the reverse scan. After the EPR experiment, the specimen surface was observed by scanning electron microscopy and energy dispersive spectroscopy. The DOS of the specimens heat-treated at 600℃ increased with heat treatment times up to 48 h and then decreased due to a self healing effect. The DOS was higher in specimens heat-treated at 600℃ than those at 500℃ or 700℃. Corrosion of the sensitized specimens occurred mainly at the δ-γ phase boundary. The corrosion morphology at the δ-γ phase boundary changed with sensitizing heat-treatment conditions due to differences in chromium activity in γ austenite and δ ferrite.

• 한국표면공학회지
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• 제48권6호
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• pp.329-334
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• 2015

The aim of this paper is to determine the proper heat treatment temperature for SDSS tube production without ${\sigma}$-phase precipitation. When Mother steel tube was heat treated at $800^{\circ}C$ temperature, relatively a large amount of ${\sigma}$-phase precipitated and grain refinement of ferrite phase occurred simultaneously. However, in Pilgered and Drawn steel tubes, grain refinement of the ferrite phase did not occur and a small amount of ${\sigma}$-phase precipitated. For all three types of steel tubes, the pitting potential was reduced to 2/5 or less compared with the untreated one and corrosion also occurred in the salt spray test due to the precipitation of ${\sigma}$-phase. When heat treatment temperature was $900^{\circ}C$, grain refinement of the ferrite phase occurred and very little ${\sigma}$-phase precipitated in Pilgered and Drawn steel tubes. But when heat treatment was done at $1,000^{\circ}C$ temperature, all three types of steel tubes had a similar corrosion properties of that of untreated one and also corrosion did not occur in the salt spray test, as ${\sigma}$-phase did not precipitate. Therefore, the optimum heat treatment temperature range is determined to be more than $1000^{\circ}C$ for the SDSS at which corrosion does not occur.

• 한국기계가공학회지
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• 제9권4호
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• pp.44-52
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• 2010

Recently, with the high performance and efficiency of machine, there have been required the multi-functions in various machine parts, such as the heat resistance, the abrasion resistance and the stress resistance as well as the strength. Fatigue crack growth tests were carried out to investigate the fatigue characteristics of high carbon steel (SM53C) experienced by high-frequency induction treatment. The influence of high-frequency induction treatment on fatigue limit was experimentally examined with the specialfocus on the variation of surface microstructure and the fatigue crack initiation and propagation through fractography. Also, the shape of hardening depth, hardened structure, hardness, and fatigue-fracture characteristics of SM53C composed by carbon steel are also investigated.

• Journal of Welding and Joining
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• 제35권3호
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• pp.68-74
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• 2017

Characteristics of dissimilar metal welds between alloy steel ASTM A387 Gr. 91 and carbon steel ASTM A516 Gr.70 made with Flux cored arc welding(FCAW) have been evaluated in terms of microstructure, mechanical strength, chemical analysis by EDS as well as corrosion test. Three heat inputs of 15.0, 22.5, 30.0kJ/cm were employed to make joints of dissimilar metals with E71T-1C wire. Post-weld heat treatment was carried out at $750^{\circ}C$ for 2.5 h. Based on microstructural examination, Intragranular polygonal ferrite and grainboundary ferrite were formed only in first layer of weld metal. Another layers consisted of acicular ferrite and $Widmannst{\ddot{a}}tten$ ferrite. The amount of acicular ferrite was increased with decreasing heat input and layer. Heat affected zone of alloy steel showed the highest hardness due to the formation of tempered martensite and lower bainite. Lower and upper bainite were formed in heat affected zone of carbon steel. Tensile strengths of dissimilar metal welds decreased with increasing heat inputs. Dissimilar metal welds showed a good hot cracking resistance due to the low HCS index below 4. The salt spray test of dissimilar metals welds showed that the weight loss rate by corrosion below 170 hours was decreased with increasing heat inputs due to the increase of the amount of acicular ferrite.

• Design & Manufacturing
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• 제16권1호
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• pp.9-14
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• 2022

A lot of research is being done on metal materials to improve the lifespan of molded parts. As a result, excellent mold materials have been developed that withstand high hardness at high temperatures and frictional heat generated from high-speed cutting. In this study, the press mold life of powder high-speed tool steel and general high-speed tool steel was compared. Powdered high-speed steel is composed of alloying elements such as tungsten, maldividene, cobalt, chromium, and vanadium in steel, which improves wear resistance compared to high-hardness and high-speed tool steels. The mold parts of both steel types were manufactured in the same way from heat treatment to machining, and the powder high-speed tool steel was 66HRC and the high-speed tool steel was 61HRC. As a result of the experiment, it was observed that the number of punching of powder high-speed tool steel was improved by 40-50%, and powder high-speed tool steel had fewer impurities, uniform texture, and excellent surface structure. It has a microscopic structure.

• 소성∙가공
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• 제24권4호
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• pp.256-263
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• 2015

Electric resistance spot welding has been used to join overlapped steel sheets in automotive bodies. Recently to reduce weight in automotive vehicles, non-ferrous metals are being used or considered in car bodies for hoods, trunk lids, doors parts, etc. Various welding processes such as laser welding, self-piercing rivet, friction stir welding are being used. In the current study, a new electric resistance heated friction stir spot welding is suggested for the spot welding of non-ferrous metals. The welding method can be characterized by three uses of heat -- electric resistance heating, friction stir heating and conduction heating of steel electrodes -- for the fusion joining at the interfacial zone between the two sheets. The welding process has variables such as welding current, diameter of the steel electrodes, revolutions per minute (rpm) of the friction stir pin, and the insert depth of the stir pin. In order to obtain the optimal welding variables, which provide the best welding strength, many experiments were conducted. From the experiments, it was found that the welding strength could be reached to the required production value by using an electrode diameter of 10mm, a current of 7.6kA, a stirring speed of 400rpm, and an insert depth of 0.8mm for the electric resistance heated friction stir spot welding of 5052 aluminum 1.5mm sheets.

• Journal of Welding and Joining
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• 제32권2호
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• pp.14-17
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• 2014

Ferritic stainless steels are widely used in the construction industry and in exhaust manifolds due to their low cost and relatively superior stress corrosion cracking resistance and pitting corrosion resistance compared to austenite stainless steels. Ferritic stainless steels are currently welded by various welding process including gas tungsten arc welding (GTAW), electron resistance welding (ERW) and laser beam welding. However, when these stainless steels are welded by fusion welding, some problems occur in the fusion zone (FZ) and heat affected zone (HAZ). First, the ductility of the weld is reduced due to the grain growth in the FZ and HAZ. Second, as its HAZ is frequently sensitized during welding, corrosion resistance deteriorates in this region due to the Cr depletion zone. To prevent these problems, it is recommended that ferritic stainless steels be welded with a low heat input. In this study, recent researches in the view of friction stir welded ferritic stainless steels are briefly reviewed.