• Title/Summary/Keyword: Heat of sublimation

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A Review on Swirling Flow by Using Flow Visualization Techniques in the Circular Tubes (원형관 내에서 유동가시화 기법을 이용한 선회유동에 관한 연구고찰)

  • Chang, Tae-Hyun;Doh, Deog-Hee;Lee, Kwoon-Soo
    • Journal of the Korean Society of Visualization
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    • v.8 no.3
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    • pp.12-21
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    • 2010
  • Swirling flows are found in very wide range of applications, for examples, cyclone separators, spraying machines, heat exchangers and jet pumps, ect. Relatively, little work has been done on the swirl flow using flow visualization techniques. This study deals with many visualization techniques to study on swirling flow. These techniques are related to oil films methods, smoke, dye liquids, liquid crystal, stroboscope light, smoke wire, white light, naphthalene sublimation, LDV(lase doppler Velocimetry) and PIV(particle image velocimetry). The present work has handled single, annular, carved tube, swirl expansion and swirl wake using several visualization methods in the vertical and horizontal circular tube.

Fabrication of Porous Ti by Freeze-Drying and Heat Treatment of TiH2/Camphene Slurries (TiH2/camphene 슬러리의 동결건조 및 열처리에 의한 Ti 계 다공체의 제조)

  • Seo, Han Gil;Kim, Young Do;Suk, Myung-Jin;Oh, Sung-Tag
    • Korean Journal of Materials Research
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    • v.23 no.6
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    • pp.339-343
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    • 2013
  • Porous Ti-systems with unidirectionally aligned channels were synthesized by freeze-drying and a heat treatment process. $TiH_2$ powder and camphene were used as the source materials of Ti and sublimable vehicles, respectively. Camphene slurries with $TiH_2$ content of 10 and 15 vol% were prepared by milling at $50^{\circ}C$ with a small amount of oligomeric polyester dispersant. Freezing of the slurry was done in a Teflon cylinder attached to a copper bottom plate cooled at $-25^{\circ}C$ while unidirectionally controlling the growth direction of the camphene. Pores were generated subsequently by sublimation of the camphene during drying in air for 48 h. The green body was heat-treated at $1100^{\circ}C$ for 1 h in a nitrogen and air atmosphere. XRD analysis revealed that the samples composed of TiN and $TiO_2$ phase were dependent on the heat-treatment atmosphere. The sintered samples showed large pores of about 120 mm which were aligned parallel to the camphene growth direction. The internal wall of the large pores had relatively small pores with a dendritic structure due to the growth of camphene dendrite depending on the degree of nucleation and powder rearrangement in the slurry. These results suggest that a porous body with an appropriate microstructure can be successfully fabricated by freeze-drying and a controlled sintering process of a camphene/$TiH_2$ slurry.

Effects of Bleeding on Heat/Mass Transfer in a Rotating Channel with Transverse Ribs (90도 요철이 설치된 회전덕트에서 유출이 열/물질전달에 미치는 영향)

  • Park, Suk-Hwan;Jeon, Yun-Heung;Kim, Kyung-Min;Lee, Dong-Hyun;Cho, Hyung-Hee
    • The KSFM Journal of Fluid Machinery
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    • v.9 no.1 s.34
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    • pp.25-31
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    • 2006
  • The present study investigates the effects of bleed flow on heat/mass transfer and pressure drop in a rotating channel with transverse rib turbulators. The hydraulic diameter $(D_h)$ of the square channel is 40.0mm. The bleed holes are located between the rib turbulators on leading surface and the hole diameter (d) is 4.5 mm. The square rib turbulators are installed on both leading and trailing surfaces. The rib-to-rib pitch is 10.0 times of the rib height(e) and the rib height-to-hydraulic diameter ratio $(e/D_h)$ is 0.055. The tests were conducted at various rotation numbers (0, 0.2, 0.4), while the Reynolds number and the rate of bleed flow to main flow (BR) were fixed at 10,000 and $10\%$, respectively. The results suggest that the heat/mass transfer characteristics in the internal cooling passage are influenced by rib turbulators, bleed flow and the Coriolis force induced by rotation. For the rotating ribbed passage with bleed flow, the heat/mass transfer on the leading surface is hardly affected by bleed flow, but that on the trailing surface decreases due to the diminution of main flow. The results also show that the friction factor decreases with the bleed flow.

Effect of Free Stream Turbulence Intensity on Heat/Mass Transfer Characteristics Around a Film Cooling Hole (주유동의 난류강도가 막냉각홀 주위의 열/물질전달 특성에 미치는 영향)

  • 이동호;김병기;조형희
    • Journal of the Korean Society of Propulsion Engineers
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    • v.2 no.2
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    • pp.56-63
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    • 1998
  • The present study investigated local heat transfer characteristics around a film cooling hole with variations of free stream turbulence intensity The film cooling jet is injected through a single hole inclined at $30^{\cire}$ to the surface and laterally at $45^{\cire}$ for the blowing rates of 0.5, 1.0 and 2.0. Turbulence generating grids are used at upstream of the film cooling hole to change the turbulence intensity of free stream. Free stream turbulence intensity without grids is 0.5%. Two different turbulence generating grid is installed at different at locations upstream of the film cooling hole so that turbulence intensity of free stream varies from 3% to 10%. The naphthalene sublimation technique has been employed to determine local heat/ mass transfer coefficients. With low free stream turbulence intensity, heat/mass transfer augmented area by coolant or free stream is distinguished evidently. However, when free stream turbulence intensity is high, heat transfer is enhanced in all region and heat transfer enhanced regions are not clearly divided due to vigorous mixing of coolant and free stream. The peak values of heat/mass coefficients are decreased and the distributions of heat/mass transfer coefficients are more uniform with high turbulence intensity. The effect of turbulence intensity on heat transfer characteristics is more evident as blowing rate is higher.

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Effect of Powder Characteristic and Freeze Condition on the Pore Characteristics of Porous W (텅스텐 다공체의 기공특성에 미치는 분말특성 및 동결조건의 영향)

  • Kwon, Na-Yeon;Oh, Sung-Tag
    • Journal of Powder Materials
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    • v.19 no.4
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    • pp.259-263
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    • 2012
  • Dependence of the freeze-drying process condition on microstructure of porous W and pore formation mechanism were studied. Camphene slurries with $WO_3$ contents of 10 vol% were prepared by milling at $50^{\circ}C$ with a small amount of dispersant. Freezing of a slurry was done in Teflon cylinder attached to a copper bottom plate cooled at $-25^{\circ}C$. Pores were generated subsequently by sublimation of the camphene during drying in air for 48 h. The green body was hydrogen-reduced at $800^{\circ}C$ for 30 min, and sintered in the furnace at $900^{\circ}C$ for 1 h. After heat treatment in hydrogen atmosphere, $WO_3$ powders were completely converted to metallic W without any reaction phases. The sintered samples showed large pores with the size of about $70{\mu}m$ which were aligned parallel to the camphene growth direction. Also, the internal wall of large pores and near bottom part of specimen had relatively small pores with dendritic structure due to the growth of camphene dendrite depending on the degree of nucleation and powder rearrangement in the slurry.

Fabrication of Porous Cu by Freeze-drying Process of Camphene Slurry with CuO-coated Cu Powders (CuO가 코팅된 Cu 분말을 혼합한 Camphene 슬러리의 동결건조에 의한 Cu 다공체 제조)

  • Bang, Su-Ryong;Oh, Sung-Tag
    • Journal of Powder Materials
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    • v.21 no.3
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    • pp.191-195
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    • 2014
  • This study reports a simple way of fabricating the porous Cu with unidirectional pore channels by freeze drying camphene slurry with Cu oxide coated Cu powders. The coated powders were prepared by calcination of ball-milled powder mixture of Cu and Cu-nitrate. Improved dispersion stability of camphene slurry could be achieved using the Cu oxide coated Cu powders instead of pure Cu powders. Pores in the frozen specimen at $-25^{\circ}C$ were generated by sublimation of the camphene during drying in air, and the green bodies were sintered at $750^{\circ}C$ for 1 h in $H_2$ atmosphere. XRD analysis revealed that the coated layer of Cu oxide was completely converted to Cu phase without any reaction phases by hydrogen heat treatment. The porous Cu specimen prepared from pure Cu powders showed partly large pores with unidirectional pore channels, but most of pores were randomly distributed. In contrast, large and aligned parallel pores to the camphene growth direction were clearly observed in the sample using Cu oxide coated Cu powders. Pore formation behavior depending on the initial powders was discussed based on the degree of powder rearrangement and dispersion stability in slurry.

Selection of Heater Location in Linear Source for OLED Vapor Deposition (OLED 증착을 위한 선형증발원 히터 위치선정)

  • Joo, Young-Cheol;Han, Choong-Hwan;Um, Tai-Joon;Lee, Sang-Wook;Kim, Kug-Weon;Kwon, Kye-Si
    • Journal of Institute of Control, Robotics and Systems
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    • v.14 no.6
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    • pp.515-518
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    • 2008
  • Organic light emitting diode(OLED) is one of the most promising type of future flat panel display. A linear source is used to deposite organic vapor to a large size OLED substrate. An electric heater which is attached on the side of linear source heats the organic powder for the sublimation. The nozzle of heater, which is attached at the top of the linear source has an optimal temperature. An numerical analysis has been performed to find optimal heater position for the optimal nozzle temperature. A commercial CFD program, FLUENT, is used on the analysis. Two-dimensional and three-dimensional analysis have been performed. The analysis showed that the heater should be attached at the outer side of crucible wall rather than inner side of housing, which was original design. Eighteen milimeter from the top of the linear source was suggested as the optimal position of heater. Improving thermal performance of linear source not only helps the uniformity of organic vapor deposition on the substrate but also increase productibity of vapor deposition process.

Freeze Drying Process and Pore Structure Characteristics of Porous Cu with Various Sublimable Vehicles (다양한 동결제를 이용하여 동결건조 공정으로 제조한 Cu 다공체의 기공구조 특성)

  • Lee, Gyuhwi;Oh, Sung-Tag;Suk, Myung-Jin;Jeong, Young-Keun
    • Journal of Powder Materials
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    • v.27 no.3
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    • pp.198-202
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    • 2020
  • The effect of sublimable vehicles on the pore structure of Cu fabricated by freeze drying is investigated. The 5 vol% CuO-dispersed slurries with camphene and various camphor-naphthalene compositions are frozen in a Teflon mold at -25℃, followed by sublimation at room temperature. After hydrogen reduction at 300℃ and sintering at 600 ℃, the green bodies of CuO are completely converted to Cu with various pore structures. The sintered samples prepared using CuO/camphene slurries show large pores that are aligned parallel to the sublimable vehicle growth direction. In addition, a dense microstructure is observed in the bottom section of the specimen where the solidification heat was released, owing to the difference in the solidification behavior of the camphene crystals. The porous Cu shows different pore structures, such as dendritic, rod-like, and plate shaped, depending on the composition of the camphornaphthalene system. The change in pore structure is explained by the crystal growth behavior of primary camphor and eutectic and primary naphthalene.

Mathematical Relationship between Ice Dendrite Size and Freezing Conditions in Tuna

  • Choi, Mi-Jung;Hong, Geun-Pyo;In, Dae-Sik;Min, Sang-Gi
    • Food Science and Biotechnology
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    • v.18 no.2
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    • pp.330-335
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    • 2009
  • The principal objective of this study was to investigate changes in ice dendrite size during the freezing of tuna, in order to formulate a mathematical model of ice dendrite size. The tuna was frozen via a uni-directional heat transfer. Thermogram analysis allowed us to determine the position of the freezing front versus time, which is referred to as the freezing front rate. The morphology of the ice dendrites was assessed via scanning electron microscopy after freeze-drying, and the retained pore size was measured as ice dendrites. We noted that the mean size of ice dendrites increased with the distance to the cooling plate; however, it decreased with reductions in the cooling rate and the cooling temperature. In addition, shorter durations of the freeze-drying process decreased the freezing front rate, resulting in a larger size of the ice dendrite pores that operate as water vapor sublimation channels. According to our results, we could derive a linear regression as an empirical mathematical model equation between the ice dendrite size and the inverse of the freezing front rate.

Color and Fastness Properties of Nylon Transfer Digital Textile Printing(DTP) using Acrylic-based Polymer as Pre-treatment Agent (나일론 전사 DTP 원단 전처리에 따른 발색성 및 견뢰도 특성)

  • Kim, Hyeok-Jin;Hong, Jin-Pyo;Kwak, Dong-Sup;Seo, Hye-Ji;Kim, Hyun-Jo
    • Textile Coloration and Finishing
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    • v.31 no.2
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    • pp.88-97
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    • 2019
  • In this study, when printed on a nylon material, the color strength and fastness are lower than that of a polyester material, and the nylon material shrinks due to heat and pressure, resulting in poor design and poor compatibility. To overcome this problem, we investigated the possibility of transfer DTP by adding pre-treatment process to nylon transfer DTP process. For the basic study of pre-treatment preparation, we used pure nylon material which is not compounded and dispersion ink and transfer paper applied to existing PET transfer DTP. Pre-treatment preparations were classified into three types of acryl-base polymer and pre-treated with nylon and then applied to transfer DTP to confirm their color strength and fastness. The color strength of the pre-treated nylon material increased and poly-methyl-acrylate amulsion pre-treatment showed the best color at $210^{\circ}C$, 1.5m/min and 0.3MPa. The nylon material pre-treated with washing, friction, and light fastness was judged to be more excellent and stable.