• 한국세라믹학회지
• /
• 제29권11호
• /
• pp.863-869
• /
• 1992

A SOG(spin glass) solution with excellent wetting to Si wafers was prepared by acid-hydrolysis of Si(OEt)4 and Me2Si(OEt)2. The solution was spin coated on Si wafers, and effects of heat treatment of the film were characterized by TG/DTA, FTIR and Ellipsometry. Silica film was obtained by heat treatment at $600^{\circ}C$ within one hour, but heat treatment at 80$0^{\circ}C$ caused interfacial oxidation of the silicon substrate. Unexpectedly silica films with much better adhesion were obtained by curing at $600^{\circ}C$ for over 30 min. than those obtained by thermal oxidation.

• 한국식품영양학회:학술대회논문집
• /
• 한국식품영양학회 2001년도 동계 학술심포지움
• /
• pp.131-131
• /
• 2001

The enzyme activity and organoleptic properties of Korean pickled cucumber were studies for their changes during fermentation. The Korean pickled cucumber were prepared by blanching and high temperature soaking in salt solution and trehalose treatment The results shelved that the effect of combined heat and trehalose treatment significantly reduced the fermentation rate and softening rate of texture while a rather rapid fermentation was for those pleserved with salt. The effect of trehalose treatment enhenced fermentation and it was significantly reduced softening rate of texture by 2% treatment. The sensory evaluation of Korean pickled cucumber was found that combined heat treatment with blanching and hot solution had a positive effect for reduction of softening of cucumber tissue, however, odor and taste were not significantly affected. This study suggested that combined heat and trehalose treatment might have potential for affording protection against softness of cucumber tissue during the fermentation time.

• 열처리공학회지
• /
• 제31권5호
• /
• pp.213-219
• /
• 2018

This study was carried out to investigate the effect of hot forging ratio and solution treatment temperature on the mechanical properties of incoloy 825 alloy. With an increasing of the hot forging ratio, grain size and range of grain size was decreased. With an increasing of the solution treatment temperature after 90% forging, grain size and range of grain size was increased. Cr carbides and Ti nitrides was precipitated at below $900^{\circ}C$ and volume fraction of precipitate was increased with an decreasing of the solution treatment temperature. With an increasing of the hot forging ratio, hardness, tensile strength and elongation, toughness was increased. With an increasing of the solution treatment temperature after 90% forging, hardness and strength was increased, elongation and toughness was decreased by grain refinement. With an increasing of the forging ratio, effect of solution treatment temperature on the hardness, strength and elongation was small, but on the toughness was large.

• 열처리공학회지
• /
• 제33권6호
• /
• pp.277-283
• /
• 2020

Cu-Co-Si based alloy has a strengthening mechanism for Co₂Si intermetallic compounds deposited on the copper matrix after aging treatment and the solution treatment has a key influence on the strength and electrical conductivity of the final products. In this paper, the Cu-1.6%Co-0.38%Si alloy was fixed at the time and the solution treatment temperature was set at a temperature in the range of 800 to 950℃, and the change in mechanical properties was observed by fixing the temperature at 950℃ and changing the time. The microstructure was observed using an electron microscope and an optical microscope, and the changes in hardness, electrical conductivity, and bending workability after aging treatment were investigated. When the solution treatment time is less than 20 seconds, the solution treatment is not sufficient and the formation of precipitates contributing to the increase in hardness decreases and the hardness decreases after the aging treatment, and in more than 50 seconds, the hardness decreases due to the coarsening of the grains and the bending workability got worse.

• 열처리공학회지
• /
• 제6권4호
• /
• pp.185-193
• /
• 1993

The effect and Condition of heat treatment on the tensile strength of welded joint was investigated in 300 grade 18% Ni-Co-Mo-Ti maraging steel sheets welded with electron beam. A good tensile strength of welded joint was obtained by following heat treatment cycle ; At $1100^{\circ}C$ the specimen was high temperature solution treated for 1 hour and then it was repeated solution treated at $900^{\circ}C$, $820^{\circ}C$ for 1 hour respectively to recrystallize the coarsened ${\gamma}$ grain. These heat treatment cycle was completed by an final aging heat treatment at $480^{\circ}C$ for 4 hour. Moreover, dissolution of dendrite, a significant decrease in seregation of Mo, Ti in weld metal were observed and also the coarsened ${\gamma}$ grain formed at $1100^{\circ}C$, $1200^{\circ}C$ changed to fine grain due to the effect of recrystallization.

• 열처리공학회지
• /
• 제3권2호
• /
• pp.52-67
• /
• 1990

• 한국식품영양학회지
• /
• 제14권4호
• /
• pp.333-338
• /
• 2001

In research. which Korean pickled cucumber was treated wish various methods, including blanching. brining in hot solution, and treating with trehalose. I examined the changes of properties of material. The Korean pickled cucumber were fermented 4∼5$^{\circ}C$ for 42 days in 1% salt solution. The physiochemical properties were pH, total acidity, total cell count, lactic acid bacteria and texture properties were also evaluated. The result showed that the effect of blanching and soaking cucumber in 100$^{\circ}C$ hot salt solution significantly reduced the softening rate of texture while a rather rapid fermentation was found for those preserved with salt. The effect of trehalose treatment inhenced fermentation but it was significantly reduced softening rate of texture. The texture evaluation of Korean pickled cucumber was found that heat treatment with blanching after soaked in hot solution and trehalose treatment had a positive effect for reduction of softening of cucumber tissue.

• Food Science and Biotechnology
• /
• 제15권4호
• /
• pp.529-533
• /
• 2006

To produce fresh-cut fruit products of high quality, the combined effects of postharvest calcium and heat treatment on Tsugaru apple were examined. Whole fruits were treated for 20 min at three different conditions: dipping in 3% $CaCl_2$ solution at $45^{\circ}C$ or ambient temperature, or in heated water at $45^{\circ}C$. The calcium content of the apples dipped in $CaCl_2$ solution at $45^{\circ}C$ was higher than that of the control and the non-heated calcium dipping. The fruits with calcium and heat treatment showed the same pattern of respiration rates as the control did during storage. The browning degree of the apple slices increased to approximately 3% after one-day storage, but no significant difference was observed between the treated and untreated apples. The fruits with $CaCl_2$ solution dipping at $45^{\circ}C$ had higher firmness than those with calcium dipping or heat treatment alone.

• 한국재료학회지
• /
• 제26권5호
• /
• pp.287-291
• /
• 2016

The effect of heat treatment on the microstructure and mechanical properties of cast Ti-6%Al-4%V alloy was investigated. Heat treatment of cast Ti-6Al-4V alloy was conducted by solution treatment at $950^{\circ}C$ for 30 min; this was followed by water quenching and then aging at $550^{\circ}C$ for 1 to 1440 min. The highest hardness of the heat-treated specimens was obtained by solution treatment and subsequent aging for 5 min due to precipitates of fine ${\alpha}$ that formed from retained ${\beta}$ phase. The tensile strength of this alloy increased without dramatic decrease of the ductility due to microstructural refinement resulting from the decomposition of ${\alpha}^{\prime}$ martensite into fine ${\alpha}$ and ${\beta}$ phases, and also due to the fine ${\alpha}$ phase formed from the retained ${\beta}$ phase by aging treatment for 5 min. In addition, this strengthening might be caused by the transformation induced plasticity (TRIP) effect, which is a strain-induced martensite transformation from the retained ${\beta}$ phase during deformation, and which occurs even after aging treatment at $550^{\circ}C$ for 5 min.

• 한국해양공학회지
• /
• 제25권6호
• /
• pp.56-59
• /
• 2011

The demand for cold rolled steel (CR) for structural members is gradually increasing. If no surface treatment (coating for corrosion resistance) for CR is conducted, its use is very limited because CR is vulnerable to corrosion. Therefore, we need to develop a coating solution to provide high corrosion resistance for CR. In this study, an organic/inorganic coating solution with Si and Ti (Si polysilicate 7 wt.% + Urethane 13 wt.% + Ti amorphous 0.5 wt.%; LR-0727(1)) was used to evaluate the corrosion resistance of CR under a salt spray test. The specimens with the LR-0727(1) coating were heat treated in a drying oven at $120{\sim}210^{\circ}C$for 5 min. The corrosion resistance was investigated using a salt spray test of 7 h. In addition, an adhesive test was conducted. Rust showed under a heat treatment of $150^{\circ}C$, but no vestiges were found over $160^{\circ}C$. The specimens with heat treatment at $160^{\circ}C$ or more did not experience delamination. From these results, it is considered that the temperature limit for optimum heat treatment is $160^{\circ}C$ considering energy efficiency.