• 한국주조공학회지
• /
• 제14권1호
• /
• pp.45-51
• /
• 1994

The possibility of using bulk talc as molding material was reviewed and tested with the measurement of thermal properties and computer simulations. The measured thermal conductivity and heat diffusivity($k{\rho}c$) of talc were $2.4W/m^{\circ}C$ and $6.6{\times}10^6J^2/m^4^{\circ}C^2s$, respectively. Thermal properties of talc could be ranked between those of sand mold and iron mold. Talc transforms into cristobalite and enstatite at $910^{\circ}C$, During the transformation volume and structure change, cracks appear on the surface and distortion occurs. Therefore talc can be used for molding material below $910^{\circ}C$ if carefully treated. Computer simulation was carried out to test whether talc insert could promote directional solidification in sand mold and iron mold. In sand mold, it was possible to achieve directional solidification of thin plate casting with the length to thickness ratio of 15, if both iron insert and talc insert were used. In iron mold, it was possible to achieve directional solidification only with talc insert.

• 한국세라믹학회지
• /
• 제46권5호
• /
• pp.493-496
• /
• 2009

Phase stabilized leucite, which has high coefficient of thermal expansion, was synthesized, and its thermal expansion behavior was investigated. The homogeneous leucite phase was synthesized by solid state reaction from the mixture of $K_2CO_3-Al_2O_3-SiO_2$. and its stabilization from tetragonal to cubic phase was attempted by adding $Cs_2CO_3$ into starting materials. And fine powder with an average particle size of a few hundreds ${\mu}m$ were fabricated by planetary milling. During milling, amorphization of leucite was observed and recrystallized after heat treatment. The thermal expansion behavior of tetragonal and cubic leucite has measured and discussed. The average coefficient of thermal expansion of tetragonal and cubic phase leucite from room temperature to $750^{\circ}C$ was $21.4{\times}10^{-6}/^{\circ}C$ and $14.5{\times}10^{-6}/^{\circ}C$, respectively.

• 한국세라믹학회지
• /
• 제53권6호
• /
• pp.610-614
• /
• 2016

Tyranno SA (SiC-polycrystalline fiber, Ube Industries Ltd.) shows excellent heat-resistance up to $2000^{\circ}C$ with relatively high mechanical strength. This fiber is produced by the conversion process from a raw material (amorphous Si-Al-C-O fiber) into SiC-polycrystalline fiber at very high temperatures over $1500^{\circ}C$ in argon. In this conversion process, the degradation reaction of the amorphous Si-Al-C-O fiber accompanied by a release of CO gas for obtaining a stoichiometric composition and the subsequent sintering of the degraded fiber proceed. Furthermore, vaporization of gaseous SiO, phase transformation and active diffusion of the components of the Si-Al-C-O fiber competitively occur. Of these changes, vaporization of the gaseous SiO during the conversion process results in an abnormal SiC-grain growth and also leads to the non-stoichiometric composition. However, using a modified Si-Al-C-O fiber with an oxygen-rich surface, vaporization of the gaseous SiO was effectively prevented, and then consequently a nearly stoichiometric SiC composition could be obtained.

• 한국군사과학기술학회지
• /
• 제13권1호
• /
• pp.114-119
• /
• 2010

There are a number of studies on chemically strengthened glass. Most of them are strengthened in molten salt bath below transformation range of glass. This research is distinguished from the aforementioned studies in that single $KNO_3$ powder was used by employing screen printing technique. In this study soda-lime-silicate(SLS) glasses for bulletproof glass application with various thicknesses were used. The maximum value of the bending strength is 791MPa heat treated at $480^{\circ}C$, which is about 4.3 times higher than the parent glass, which is the highest strength of all soda-lime glasses. In this study, it is also observed that Vickers hardness increased to $657H_v$, which is about 15% higher than the parent glass($568.7H_v$) and fracture toughness was not changed. Depth profiles measured by electron probe micro analyzer(EPMA) showed a correlation between the migrations of $K^+$ ions with bending strength of ion exchanged glasses.

• 한국전기전자재료학회:학술대회논문집
• /
• 한국전기전자재료학회 2003년도 춘계학술대회 논문집 초전도 자성체 연구회
• /
• pp.69-72
• /
• 2003

Bi-2223 superconducting wires were fabricated by stacking, drawing process with different precursor powders and different heat-treatment histories. The precursor powders were 2 kinds of Pb content. And a part of the tapes were experienced pre-annealing process which caused tetragonal structure of Bi-2212 phase to orthorhombic structure of it was during drawing process. We confirmed the transformation of Bi-2212 phase from tetragonal structure to orthorhombic structure and reduction of second phases. XRD and DC magnetization analysis were performed in order to investigate the fraction of Bi-2223 phase in Bi-2223/Ag HTS tape. We could achieve best Ic of 70 A class at the Bi-2223/Ag tape using low Pb content of precursor powder and experienced pre-annealing process. DC magnetization analysis was useful to investigate the fraction of Bi-2223 phase in the Bi-2223/Ag tape.

• 설비공학논문집
• /
• 제27권10호
• /
• pp.552-557
• /
• 2015

The nanostereolithography process using a femtosecond laser has been shown to have strong merits for the direct fabrication of 2D/3D micro structures. In addition, a femtosecond laser provides efficient tools for precise micromachining owing to the advantages of a small and feeble heat effect zone. In this paper, we report an effective fabrication process of 3D micro optical and fluidic devices using nanostereolithography process composed of a dual stage system. Process conditions for additive and subtractive fabrication are examined. The Piezo stage scanning system is used for 3D micro-fabrication in unit area of sub-mm scale, and the motor stage is employed in fabrication on the scale of several mm. The misalignment between the pizeo- and motor- stages is revised through rotational transformation of CAD data in the unit domain. Here, the effectiveness of the proposed process is demonstrated through examples using 3D optical and microfluidic structures.

• 한국콘크리트학회:학술대회논문집
• /
• 한국콘크리트학회 2004년도 추계 학술발표회 제16권2호
• /
• pp.517-520
• /
• 2004

Concrete Filled steel Tube pipe structure is a rational type of structure that maximizes performance by combining the strong points of steel frame and concrete. In the structure, the confining effect of steel pipes increases the bearing power of infilled concrete and the strengthening of local bucking of steel pipes by infilled concrete increases the bearing power of members. and these result in the reduction of cross-sectional area and high transformation capacity. Moreover. the structure is economically efficient and widely applicable that it is used from super-high buildings to residential, business and apartment buildings. It enables the construction of multi-story buildings with long spans using columns of small cross-sectional area. In case of diaphragm, however, it is difficult to confirm the compactness of the closed inside of steel pipes. The present study examined the properties of super-high strength concrete over 80MPa by comparing it with 40MPa concrete through heat conductivity and length change tests based on a mixture ratio satisfying the mixture goal presented in the guideline for the design and construction of concrete-filled steel pipe structure. and evaluated the performance of super-high strength concrete according to the shape and size of the aperture ratio of diaphragm.

• Carbon letters
• /
• 제8권3호
• /
• pp.177-183
• /
• 2007

[ $TiO_2$ ]ACF composites were prepared by the electrochemical method with Titanium (IV) n-butoxide (TNB) electrolyte under different electrochemical operation time. The BET surface area for $TiO_2$/ACF composites decrease with the increase of electrochemical operation time. There is a single crystal structure which is anatase in all of the samples from the data of XRD. The SEM micrphotographs of $TiO_2$/ACF composites show that the $TiO_2$ particles were well mixed with the ACF. There are O and P with strong C and Ti peaks in all samples from EDX results, and it also shows that a decrease of the C content with a increasing of Ti content with increasing of the electrochemical operation time in the over all composites. DSC cures show that the exothermic peak of all composites at $560^{\circ}C$ represents the transformation heat of amorphous parts to anatase phase and the discontinuous grain growth of the transformed anatase particles. Finally, the excellent photoactivity of $TiO_2$/ACF composites (especially, ACFT10) could be attributed that the decrease of concentration of MB can be concluded to be much faster for the adsorption by ACF than for photocatalytic decomposition by $TiO_2$.

• 한국분말재료학회지
• /
• 제17권6호
• /
• pp.482-488
• /
• 2010

In this study, $FeSi_2$ as high temperature performance capable thermoelectric materials was manufactured by powder metallurgy.The as-casted Fe-Si alloy was annealed for homogenization below $1200^{\circ}C$ for 3 h. Due to its high brittleness, the cast alloy transformed to fine powders by ball-milling, followed by subsequent compaction (hydraulic pressure; 2 GPa) and sintering ($1200^{\circ}C$, 12 h). In order to precipitate ${\beta}-FeSi_2$, heat treatment was performed at $850^{\circ}C$ with varying dwell time (7, 15 and 55 h). As a result of this experiment thermoelectric phase ${\beta}-FeSi_2$ was quickly transformed by powder metallurgical process. There was not much change in powder factor between 7h and 55h specimens.

• 조명전기설비학회논문지
• /
• 제17권4호
• /
• pp.50-56
• /
• 2003

본 논문에서는 유입변압기 진단을 목적으로 부분방전시 발생하는 여러 가지 물리적 화학적 현상중 초음파를 검출하기 위하여 광섬유 Mach-Zehnder 간섭계를 구성하였다. 구성된 광섬유 센서의 초음파 검출 평가 실험을 실시하고, 절연유 중에 배치한 침-평판전극에 교류 고전압을 인가하여 방전시 발생하는 초음파를 측정하고 퓨리에 변환 및 wavelet 변환을 이용한 데이터 분석 결과를 나타냈다.