• Journal of the Korean Society for Heat Treatment
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• v.12 no.4
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• pp.294-302
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• 1999

Evaluation of Brinell standard hardness tester was carried out to secure its application as a national standard for Brinell hardness. Accuracies and reliabilities in load application, indenter diameter and indentation measurement were tested through evaluation of these components. The accuracies of load application for various loading conditions were within the limit of ISO and KS specifications. Errors in the indentation measurement due to the difference in personnel characters were successfully removed by utilising automatic indentation measurement system. In overall, the tester and the indentation measuring system were found to be eligible as a national standard of Brinell hardness.

• Journal of the Korean Society for Precision Engineering
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• v.4 no.1
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• pp.65-73
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• 1987

In recent days, the application of ultrasonics has been increased in the field of engineering and medicine. The ultrasonic hardness tester to apply the principle of contact compliance method is entirely different from hardness tester in the past and in the practical use, the more pre- cisive measurement is required because it has a slight change of hardness value due to the difference of resonance frequency. Therefore, in this study, as one type of applicative transducers which can detect the optimum pressure load, ring type load cell was used in the measurement of ultrasonic hardness. From experimental results, it was compared ultrasonic hardness testing method with the other hardness testing methods. Also, the measurement error of ultrasonic hardness tester could be measured within .+-. 0.5 HRC F.S. in the case of 3.0Kg pressure load.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.24 no.6
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• pp.625-631
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• 2015

The hardness of surface treated magnesium alloy was evaluated using laser induced breakdown spectroscopy. The surface of the specimen was hardened mechanically, and the hardness profiles were measured using a traditional measurement technique. A laser beam was irradiated to generate a plasma, and the peaks of the components of the specimen were analyzed. A wavelength of 333.66 nm and 293.65 nm were selected as the atomic and ionic peaks, respectively. The ratios of the ionic peak to the atomic peak were obtained so as to compare the hardness profile. As the depth increased, the ratio decreased. These results are in good agreement with the previous hardness measurement results. It can be considered that this technique could be applied for remote and time-efficient hardness measurement.

• Korean Journal of Materials Research
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• v.21 no.11
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• pp.581-586
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• 2011

This study describes a hydrogen embrittlement evaluation of the subsurface zone in 590DP steel by micro-Vickers hardness measurement. The 590DP steel was designed to use in high-strength thin steel sheets as automotive materials. The test specimens were fabricated to 5 series varying the chemical composition through the process of casting and rolling. Electrochemical hydrogen charging was conducted on each specimen with varying current densities and charging times. The relationship between the embrittlement and hydrogen charging conditions was established by investigating the metallography. The micro-Vickers hardness was measured to evaluate the hydrogen embrittlement of the subsurface zone in addition to the microscopic investigation. The micro-Vickers hardness increased with the charging time at the surface. However, the changing ratio and maximum variation of hardness with depth were nearly the same value for each test specimen under the current density of 150 mA/$cm^2$ and charging time of 50 hours. Consequently, it appears that hydrogen embrittlement in 590DP steel can be evaluated by micro-Vickers hardness measurement.

• Journal of the Korean Society for Heat Treatment
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• v.14 no.5
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• pp.275-281
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• 2001

To improve the reliability of hardness test results, Rockwell hardness round robin test was carried out for 10 laboratories. The test condition was the same with the ISO(International Standards Organization) standards. Korea Research Institute of Standards and Science(KRISS) supplied the hardness standard blocks and an indenter to laboratories for the measurement. The participating laboratories measured hardness of the specified areas on the blocks for 6 times with their own indenter as well as common indenter, respectively, and reported the results to KRISS. The result showed that quite large amount of the differences came from the indenter and it is necessary to change indenter with better quality for improved reliability in hardness measurement.

• Journal of the Korean Society for Heat Treatment
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• v.13 no.1
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• pp.10-15
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• 2000

Evaluation of long term stability of the Brinell standard hardness tester was carried out to secure its application as a national standard in Brinell hardness. Accuracy and repeatability in load application were tested through evaluating errors in hardness measurement of certified reference blocks. All of those requirements in KS as well as ISO specifications were satisfied by this standard hardness tester. In addition to this, long term stability test of automatic indentation measurement system was carried out. The scattering range was almost the same with its error range. To figure out an optimum test condition for better repeatability and long term stability, the effect of load variation, load application speed and time have been studied using orthogonal array experimental plan. It was found that the best combination is $30{\mu}m/s$ of load application speed and 25 seconds of load application time.

• Journal of the Korean Society for Precision Engineering
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• v.31 no.2
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• pp.141-148
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• 2014

In this work, effects of plasma on different hardness of welding steel using laser-induced breakdown spectroscopy were investigated. The ratios of ionic to atomic spectrum peaks were related to its material hardness. The major spectrum peak (Fe) and minor spectrum peak (Mn) were considered as monitoring elements. The stronger repulse plasma was generated, the harder material it was. The ratios of ionic to atomic spectrum peaks increased with respect to the material hardness as well. The correlation of minor spectrum peaks was stronger than that of major spectrum peaks. However, the major spectrum peaks indicated a similar trend, which could be used to estimate the hardness, too. Based on this result, the method could be used as a non-contact remote measurement of material properties.

• Journal of the Korean institute of surface engineering
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• v.54 no.4
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• pp.171-177
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• 2021

This paper is concerned with the surface hardness measurement of NiP-coated AA7050 using different loads from 10 to 100 g. The surface hardness was observed to increase from 180 to 600 H_v with increasing NiP layer thickness, depending on the load applied for indentation. When NiP coating thickness is thinner than 2 ㎛, the surface hardness of NiP-coated AA7050 was mainly determined by AA7050 substrate, while it was significantly increased by NiP coating layer when NiP coating thickness is thicker than 2 ㎛. Hardness of AA7050 substrate itself was not dependent on the applied load but the hardness of NiP-coated AA7050 was largely influenced by the load applied for indentation. The largest difference of hardness between 10 g and 100g of applied loads, was obtained at the NiP thickness of about 8 ㎛ above which the measured hardness at 10 g reached a maximum value of about 600 H_v. It was also observed that indentation-induced plastic deformation next to the indented zone occurs when NiP layer is 5.64 times thicker than the depth of impression formed by indentation.

• Journal of the Korean Vacuum Society
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• v.19 no.5
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• pp.360-364
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• 2010

Most research groups used two analysis methods (spectroscopy and nanotribology) to measure the mechanical properties of nano-materials: NMR (Nuclear Magnetic Resonance), IR (Infrared Spectroscopy), Raman Spectroscopy as the spectroscopy method and AFM (Atomic Force MicroScope), EFM (Electrostatic Force Microscope), KFM (Kelvin Force Microscope), Nanoindenter as the nanotribological one. Among these, the nano-indentation technique particularly has been recognized as a powerful method to measure the elastic modulus and the hardness. However, this technique are prone to considerable measurement errors with pressure conditions during measurement. In this paper, we measured the change of elastic modulus and hardness of an Al single crystal with the change of load, hold, and unload time, respectively. We found that elastic modulus and hardness significantly depend on load, hold, and unload time, etc. As the indent time was shortened, the elastic modulus value decreased while the hardness value increased. In addition, we found that elastic modulus value was more sensitive to indent load, hold, and unload time than the hardness value. We speculate that measurement errors of the elastic modulus and the hardness originate from the residual stress during indenting test. From our results, the elastic modulus was more susceptible to the residual stress than the hardness. Thus, we find that the residual stress should be controlled for the minimum measurement errors during the indenting test.

• Polymer(Korea)
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• v.29 no.6
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• pp.536-542
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• 2005

The effect of lime-related parameters such as loading velocity, load application time, gauge reading time on Rockwell hardness measurement was investigated for PE, PP PVC, and PMMA. It was found that keeping the specific requirements in the same condition is very important to obtain reliable and repeatable darn in polymer hardness measurement. The optimum condition for hardness measurement was 4 sec for load application time,15 sec for test load application net time, and 15 sec for gauge reading time after unloading. Using thess conditions, round robin test was carried out for 6 laboratories and it was shown that the testing machine should be one in which time-related variables are controllable. Indirect verification of hardness tester using brass reference block was not enough to guarantee the test results for polymer.