• Title/Summary/Keyword: Hardening heat treatment

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AZ91-0.3Ca-0.2Y 마그네슘 합금 주조재의 시효경화 거동 및 기계적 특성 (Age-hardening Behavior and Mechanical Properties of Cast AZ91-0.3Ca-0.2Y Alloy)

  • 김현지;배준호;김영민;박성혁
    • 소성∙가공
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    • 제32권4호
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    • pp.173-179
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    • 2023
  • In this study, the age-hardening behavior and tensile properties of a cast AZ91-0.3Ca-0.2Y (SEN9) alloy are investigated and compared with those of a commercial AZ91 alloy. Even after homogenization heat treatment, the SEN9 alloy contains numerous undissolved secondary phases, Al8Mn4Y, Al2Y, and Al2Ca, which results in a higher hardness value than the homogenized AZ91 alloy. Under aging condition at 200 ℃, both the AZ91 and SEN9 alloys exhibit the same peak-aging time of 8 h, but the peak hardness of the latter (86.8 Hv) is higher than that of the former (83.9 Hv). The precipitation behavior of Mg17Al12 phase during aging significantly differs in the two alloys. In the AZ91 alloy, the area fraction of Mg17Al12 discontinuous precipitates (DPs) increases up to ~50% as the aging time increases. In contrast, in the SEN9 alloy, the formation and growth of DPs during aging are substantially suppressed by the Ca- or Y-containing particles, which leads to the formation of only a small amount of DPs with an area fraction of ~4% after peak aging. Moreover, the size and interparticle spacing of Mg17Al12 precipitates of the peak-aged SEN9 alloy are smaller than those of the peak-aged AZ91 alloy. The homogenized AZ91 alloy exhibits a higher tensile strength than the homogenized SEN9 alloy due to the finer grains of the former. However, the peak-aged SEN9 alloy has a higher tensile elongation than the peak-aged AZ91 alloy due to the smaller amount of brittle DPs in the former.

액체로켓 연소기용 구리합금의 열/기계적 특성에 관한 실험적 연구 (Experimental Study on the Physical and Mechanical Properties of a Copper Alloy for Liquid Rocket Combustion Chamber Application)

  • 류철성;백운봉;최환석
    • 대한기계학회논문집A
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    • 제30권11호
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    • pp.1494-1501
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    • 2006
  • Mechanical and physical properties of a copper alloy for a liquid rocket engine(LRE) combustion chamber liner application were tested at various temperatures. All test specimens were heat treated with the condition they might experience during actual fabrication process of the LRE combustion chamber. Physical properties measured include thermal conductivity, specific heat and thermal expansion data. Uniaxial tension tests were preformed to get mechanical properties at several temperatures ranging from room temperature to 600$^{\circ}C$. The result demonstrated that yield stress and ultimate tensile stress of the copper alloy decreases considerably and strain hardening increases as the result of the heat treatment. Since the LRE combustion chamber operates at higher temperature over 400$^{\circ}C$, the copper alloy can exhibit time-dependent behavior. Strain rate, creep and stress relaxation tests were performed to check the time-dependent behavior of the copper alloy. Strain rate tests revealed that strain rate effect is negligible up to 400$^{\circ}C$ while stress-strain curve is changed at 500$^{\circ}C$ as the strain rate is changed. Creep tests were conducted at 250$^{\circ}C$ and 500$^{\circ}C$ and the secondary creep rate was found to be very small at both temperatures implying that creep effect is negligible for the combustion chamber liner because its operating time is quite short.

냉간압연접합법에 의해 제조된 AA1050/AA6061/AA1050 층상 복합판재의 미세조직 및 기계적 성질 (Microstructure and Mechanical Properties of AA1050/AA6061/AA1050 Complex Sheet Fabricated by Roll Bonding Process)

  • 안무종;유효상;이성희
    • 한국재료학회지
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    • 제26권7호
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    • pp.388-392
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    • 2016
  • A cold roll-bonding process was applied to fabricate an AA1050/AA6061/AA1050 laminate complex sheet. Two AA1050 and one AA6061 sheets of 2 mm thickness, 40 mm width and 300 mm length were stacked up after surface treatment that included degreasing and wire brushing; material was then reduced to a thickness of 3 mm by one-pass cold rolling. The laminate sheet bonded by the rolling was further reduced to 1.2 mm in thickness by conventional rolling. The rolling was performed at ambient temperature without lubricant using a 2-high mill with a roll diameter of 210 mm. The rolling speed was 5.0 m/sec. The AA1050/AA6061/AA1050 laminate complex sheet fabricated by roll bonding was then hardened by natural aging T4) and artificial aging (T6) treatments. The microstructures of the as-roll bonded and the age hardened Al complex sheets were revealed by optical microscope observation; the mechanical properties were investigated by tensile testing and hardness testing. The strength of the as-roll bonded complex sheet was found to increase by 2.9 times compared to that value of the starting material. In addition, the hardness of the complex sheets increased with cold rolling for AA1050 and age-hardening treatment for AA6061, respectively. After heat treatment, both AA1050 and AA6061 showed typical recrystallization structures in which the grains were equiaxed; however, the grain size was smaller in AA6061 than in AA1050.

용접(鎔接) 강부재(鋼部材)의 피로균열성장(疲勞龜裂成長)에 대한 잔류응력특성(殘留應力特性)에 관한 연구(硏究) (Experimental Investigation of the Residual Stress on Fatigue Crack Growth of Welded Steel Members)

  • 장동일;김두환
    • 대한토목학회논문집
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    • 제7권2호
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    • pp.99-106
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    • 1987
  • 용접(鎔接) 강구조물(鋼構造物)의 피로균열성장거동(疲勞龜裂成長擧動)에 관(關)한 용접잔류응력(鎔擬殘留應力)의 거동(擧動)을 파악(把握)키 위하여 열처리(熱處理)를 실시(實施)하고 피로균열성장(疲勞龜裂成長) 및 검토(檢討)한 결과(結果) 용접부(鎔接部)는 경화(硬化)되어 늑성(勒性)이 감소(減少)되므로 소재부(素材部)보다 피로균열성장율(疲勞龜裂成長率)이 높았으며 이를 열처리(熱處理)한 결과(結果) 경도(硬度)나 저항력(抵抗力)이 증가(增加)되어 개선(改善)되었으며 $650^{\circ}C$ 정도(程度)에서 가장 이상적(理想的) 이었다. Elber 식(式)은 Paris-Erdogan 식(式)에 비(比)해 균열(龜裂)닫힘현상(現狀)을 고려(考廬)하므로 더 낮은 균열성장율(龜裂成長率)을 가지며 각(各) 열처리(熱處理)에 의한 곡선(曲線)들이 서로 비슷하므로 잔류응력(殘留應力)의 효과(効果)를 고려(考慮)할 수 없었다. 균열(龜裂)길이에 따른 개구하중(開口荷重)은 경도(硬度)가 높을수록 큰 값을 가지나 열처리(熱處理) 후(後)는 경도(硬度)값의 저하(低下)로 피로균열(疲勞龜裂) 성장율(成長率)이 낮아지며 흡수(吸收)에너지와 파괴늑성(破壞勒性)을 증대(增大)시켜 균열저지능력(龜裂沮止能力)을 가져 파괴(破壞)의 위험성(危險性)을 감소(減少)시킨다.

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사출금형기계용 앵귤러핀의 충격시험에 따른 파손분석과 와이블 통계 해석 (Failure Analysis and Weibull Statistical Analysis according to Impact Test of the Angular Pin for Injection Molding Machines)

  • 김철수;남기우;안석환
    • 동력기계공학회지
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    • 제21권3호
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    • pp.37-44
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    • 2017
  • In this study, failure analysis of the angular pin for molding machines to aluminum component molding was carried out. SM45C steel was used for the angular pin, it was surface hardened by the induction surface hardening heat treatment. The cross section of damaged angular pin was observed, and micro Vickers hardness value from the fractured part was measured. Brittle fracture was occurred from the fracture surface of angular pin, therefore, impact toughness value was evaluated by V-notch Charpy impact test. It was confirmed that the impact absorption energy was high when was tempered at a high temperature for a long time, and the toughness was slightly increased. Also, 2-parameter Weibull statistical analysis was investigated in order to evaluate the reliability of the measured micro Vickers hardness values and absorbed energy. The micro Vickers hardness and absorbed energy well followed a two-parameter Weibull probability distribution, respectively. The reverse design against angular pin was proposed as possible by using test results.

전기방전소결에 의해 제조된 다공성 Titanium 임플란트의 기계적 특성 (Mechanical Properties of Electro-Discharge-Sintered Porous Titanium Implants)

  • 현창용;허재근;이원희
    • 한국재료학회지
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    • 제16권3호
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    • pp.173-177
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    • 2006
  • Porous surfaced Ti implant compacts were fabricated by electro-discharging-sintering (EDS) of atomized spherical Ti powders. Powders of $50-100{\mu}m$ in diameter were vibratarily settled into a quarts tube and subject to a high voltage and high density current pulse in Ar atmosphere. Single pulse of 0.7 to 2.0 kJ/0.7 gpowder, from 150, 300, and $450{\mu}F$ capacitors was applied in less than $400{\mu}sec$ to produce twelve different porous-surfaced Ti implant compacts. The solid core formed in the center of the compact shows similar microstructure of cp Ti which was annealed and quenched in water. Hardness value at the solid core was much higher than that at the particle interface and particles in the porous layer, which can be attributed to both heat treatment and work hardening effects induced by EDS. Compression tests were made to evaluate the mechanical properties of the EDS compacts. The compressive yield strength was in a range of 12 to 304MPa which significantly depends on input energy. Selected porous-surfaced Ti-6Al-4V dental implant compacts with a solid core have much higher compressive strengths compared to the human teeth and sintered Ti dental implants fabricated by conventional sintering process.

나노/마이크로 프로브 기술을 통한 틱소/레오 캐스트의 시효경화 특성 조사 (Investigation on Age-hardening characteristic of thixo and rheocast by using Nano/Micro-probe Technology)

  • 조상현;이창수;강충길
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2006년도 춘계학술대회 논문집
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    • pp.322-325
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    • 2006
  • The nano/microstructure and mechanical properties of the eutectic regions in thixo and rheo cast A356 alloy parts were investigated using nano/micro-indentation and mechanical scratching, combined with optical microscopy and atomic force microscope (AFM).Most eutectic Si crystals in the A356 alloy showed a modified morphology as fine-fibers, however Si particles of network in eutectic region was formed quickly with aging time increase in thixo-cast. The aging responses of the eutectic regions in both the thixo and rheo cast A356 alloys aged at $150^{\circ}C$ for different times (0, 2, 4, 8, 10, 16, 24, 36, and 72 h) were investigated. Both Vickers hardness ($H_V$) and indentation ($H_{IT}$) test results showed almost the same trend of aging curves, the peak was obtained at the same aging time of 10 h.

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Electrodes for contact electric welding of aluminium alloys

  • Bondar, M.P.;Moon, J.G.
    • 대한용접접합학회:학술대회논문집
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    • 대한용접접합학회 1997년도 특별강연 및 추계학술발표 개요집
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    • pp.184-193
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    • 1997
  • Aluminium and aluminium alloys have the high electrical and heat conductivity. It gives rise to difficulties for a choice of electrodes material for their contact electric welding. This paper describes the investigations performed to solve the above problem. The purpose of this investigation was to obtain dispersion-hardening alloys by the internal oxidation method, to optimize their contents and treatment modes, to produce electrodes of these alloys and to test them. The strengthing effect of alloys with oxide particles depends on their size stability at high temperatures. Despite of the fact, that oxides are the most stable of all the non-metallic phases their coagulation takes place. Based on the early results, we chose two types of alloys, first No. 1 Cu - 0,4%Al and second No. 2 Cu - 0,2%Be for production of electrodes. These alloys had not additional alloying elements. These alloys were prepared as 1 mm plates and flake-formed 200 m thick, and also No. 1 as a powder of size 100 mkm (received from Korea). The large samples for electrodes were produced by three methods : explosive welding method, dynamic one including the explosion compression of electrode blank and the quasi-dynamic method including the high-speed compression of dense briquest and the further hot extrusion of a rod.

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레이저 빔에 의한 박판금속의 강화특성 (Characteristics of Strengthening for Thin Metals by Laser Beam)

  • 양세영;최성대;김기만;전재목;공병채
    • 한국생산제조학회지
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    • 제19권2호
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    • pp.216-223
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    • 2010
  • The general way to process the surface by means of the laser was heat treatment for strengthening the surface hardness. They have used the laser for changing the property of the surface, especially for metal. Generally, it is recent increasing tendency to use the thin plate panel for making things smaller and lightweight. However, thin plate should be strengthened or let the thin plate panel have moment of inertia by means of engraving the groove or wave on them for lightweight and strengthening. Therefore it is expected that the thin plate panel can be harder and more stable through processing the metal surface by laser beam irradiation and the hardness of thin plate possibly can be also changed how many parts of them are harden. Through this research, it can be grasped how the hardness and mechanical characteristic changes according to width and depth of groove by laser affect the max stress by the ratio of $A_H/A_T$ (hardening area/total area) and characteristic of displacement and structural characteristic for making the thin plate harder by the strengthening metal surface of thin plate by laser through the experiment and analysis of FEA can be presented.

고온초전도 PIT 장선재 제조 및 특성 평가 (Fabrication and evaluation of superconducting properties of HIS PIT long tapes)

  • 하홍수;이동훈;양주생;황선역;최정규;김상철;하동우;오상수;권영길
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2003년도 하계학술대회 논문집 Vol.4 No.1
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    • pp.597-600
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    • 2003
  • Bi-2223/Ag HTS wires have been fabricated by the PIT(powder in tube)process. Intermediate annealing was carried out to increase the homogenization and uniformity of the superconducting filaments embedded in the silver matrix during the deformation process that is important to sustain the engineering critical current density in long superconducting wire. Intermediate annealing act to release the deformation hardening of the superconducting wires during drawing process. Rolling parameters were investigated to roll the superconducting tapes with uniform thickness, width and winding tensions. Critical current of 60 m long superconducting tapes was measured 54.3 A continuously after final sintering heat treatment. The phase analysis of Bi-2223/Ag superconducting tapes are examined by the XRD.

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