• Title/Summary/Keyword: Hardened Material

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Frictional behaviour of Oxide Films Produced on S45C Steel by Plasma Nitrocarburizing and Post Plasma Oxidation Treatment (플라즈마 질탄화 & 후산화처리로 S45C강에 형성된 산화막의 마찰거동)

  • Jeong, Kwang-Ho;Lee, In-Sup
    • Korean Journal of Materials Research
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    • v.16 no.12
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    • pp.766-770
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    • 2006
  • The frictional behavior of oxide films on top of the plasma nitrocarburized compound layers was investigated in terms of post-oxidation treatment temperatures. The post-oxidation treatment at both temperatures($400^{\circ}C,\;500^{\circ}C$) produced magnetite($Fe_3O_4$) films which led to a significant enhancement in corrosion resistance. However, this process did not result in any improvement in frictional behavior of the nitrocarburized surface. The wear mechanisms were governed predominantly by the abrasive action of the slider on the surface irrespective of the counterface material(SiC and Bearing steel). When the specimen was sliding against a SiC counterface, the oxide films were destroyed during the early stage of the sliding process and the wear debris of the oxide film at the sliding track had a great influence on the friction coefficient. On the other hand, when sliding against a bearing steel counterface, the slider was mainly worn out due to the much higher hardness of the surface hardened layer. The fluctuation of the friction coefficient of $400^{\circ}C$-oxidized/ nitrocarburized specimen is much severer than that of $500^{\circ}C$ specimen, due to the less amount of wear debris.

Analysis of Hydrogen-tightness on the Metal Sealing of a Fuel Pipe for FCEV according to Material Change of the Fitting Body (체결부 재료에 따른 FCEV 연료파이프 메탈 씰링부의 기밀성 분석)

  • Lee, J.M.;Han, E.S.;Chon, M.S.;Lee, H.W.
    • Transactions of Materials Processing
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    • v.28 no.5
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    • pp.266-274
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    • 2019
  • Metal sealing is used to connecting the parts between valves and fuel pipes for a FCEV which utilizes hydrogen gas of 700 bar. Instead of general carbon steel, stainless steel is the primary material used to manufacture fuel pipes due to hydrogen embrittlement. The shape of deformation between metals is an important factor on the air-tightness of the metal to metal contact. Since the stainless steel pipe is hardened using the plastic forming during the tip shaping stage, this work hardening could have an effect on the deformed shape and characteristics of contact surfaces in fastening of pipes. In this paper, the deformation history of the pipe model was considered in order to analyze the hydrogen-tightness on the metal sealing part. The contact distance and the forward displacement for fastening were compared using experimental results and the simulation results. The simulation of the effect of material change on the fitting body demonstrated that the hardness or the strength of the formed tip of the pipe was designed to a proper valued level since the characteristics of the contact surface was exhibited better when the strength of the pipe was lower than that of the fitting body.

A Study on the Diode Laser Surface Hardening Treatment of Cast Iron for Die Material(I) - Characteristics of Surface Hardening by Die Materials - (금형재료용 주철의 다이오드 레이저 표면경화처리에 관한 연구(I) - 금형재료에 따른 표면경화 특성 -)

  • Kim, Jong-Do;Song, Moo-Keun;Hwang, Hyun-Tae
    • Journal of Advanced Marine Engineering and Technology
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    • v.35 no.8
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    • pp.1041-1047
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    • 2011
  • In this study, two types of die material cast iron was treated for surface hardening by using high power diode laser to improve mechanical properties of die which is using as essential production technology in the parts manufacturing in virtually all the infrastructure industries now. First of all, the heat treatment characteristics of FCD550 material which is spheroidal graphite cast iron, and through the heat treatment of HCI350 material which is flake graphite cast iron, the heat treatment characteristics of the two materials were compared. The hardness of hardened zone increased over 3 times over base material for both specimens, but as for required heat input, HCI350 was higher than FCD550 material depending on the heat conductivity of the materials by the content amount and shape of graphite contained in the material.

Study on the Fatigue Resistance of Gray Cast Iron in CO2 Laser Surface Hardening (CO2레이저 표면경화(表面硬化) 처리된 회주철(灰鑄鐵)의 피로특성(疲勞特性)에 관한 연구(硏究))

  • Park, K.W.;Han, Y.H.;Lee, S.Y.
    • Journal of the Korean Society for Heat Treatment
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    • v.8 no.3
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    • pp.169-181
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    • 1995
  • This study has been performed to investigate some effects of the power density and traverse speed of laser beam on the optical microstructure, hardness and fatigue resistance of gray cast iron treated by laser surface hardening technique. Optical micrograph has shown that the dissolution of graphite flakes and the coarsening of lath martensite tend to increase with a small amount of retained austenite as the power density increases under the condition of a given traverse speed. Hardness measurements have revealed that as the power density increases, hardness values of outermost surface layer increases from Hv=620 to Hv=647 in case of traverse speed of 2.0m/min at gray cast iron. Fatigue test has exhibited that the fatigue strength of laser surface hardened specimen is superier compared to that of untreated specimen, showing that values for the fatigue strength at $N_f=10^7$ of gray cast iron laser-surface-hardened at a low power density of $4076w/cm^2$ and a high power density of $8153w/cm^2$ under the condition of a given traverse speed of 2.0m/min are $15kg_f/mm^2$ and $20kg_f/mm^2$, respectively, whereas the fatigue strength of untreated specimen is $11kg_f/mm^2$. Under high stress-low cycle condition a noraml brittleness fracture appears, whereas a ductile fracture with beach mark is observed in the specimen tested under low stress-high cycle condition.

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The Effect of Fluorine Based Emulsion on the Watertightness Properties of Portland Cement (시멘트 수밀성에 대한 불소계 에멀젼의 영향)

  • Kang, Hyun Ju;Song, Myong Shin;Song, Su Jae;Park, Su Haeng
    • Applied Chemistry for Engineering
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    • v.20 no.5
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    • pp.505-510
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    • 2009
  • It is well known that the properties of concrete such as the compressive strength, water permeability, water tightness and durability are affected by micro-structure in hardened cement paste. Especially, for durability of concrete, watertightness of cementitious materials is the most critical property among various properties. Recently, many types of material such as organic and/or inorganic materials are used for watertightness of concrete. In this study, we examined the effect of fluorine-based emulsion on watertightness property. And we also discussed the change of microstructure and formation of hydrates in hardened cement paste by the addition of fluorine-based emulsion. Cement paste with fluorine-based emulsion showed improvement of watertightness by the surface activation of cement paste and by formation of $CaF_2$ fine crystals in cement pore structure.

Short term bond shear stress and cracking control of reinforced self-compacting concrete one way slabs under flexural loading

  • Aslani, Farhad;Nejadi, Shami;Samali, Bijan
    • Computers and Concrete
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    • v.13 no.6
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    • pp.709-737
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    • 2014
  • Fibre-reinforced self-compacting concrete (FRSCC) is a high-performance building material that combines positive aspects of fresh properties of self-compacting concrete (SCC) with improved characteristics of hardened concrete as a result of fibre addition. To produce SCC, either the constituent materials or the corresponding mix proportions may notably differ from the conventional concrete (CC). These modifications besides enhance the concrete fresh properties affect the hardened properties of the concrete. Therefore, it is vital to investigate whether all the assumed hypotheses about CC are also valid for SCC structures. In the present paper, the experimental results of short-term flexural load tests on eight reinforced SCC and FRSCC specimens slabs are presented. For this purpose, four SCC mixes - two plain SCC, two steel, two polypropylene, and two hybrid FRSCC slab specimens - are considered in the test program. The tests are conducted to study the development of SCC and FRSCC flexural cracking under increasing short-term loads from first cracking through to flexural failure. The achieved experimental results give the SCC and FRSCC slabs bond shear stresses for short-term crack width calculation. Therefore, the adopted bond shear stress for each mix slab is presented in this study. Crack width, crack patterns, deflections at mid-span, steel strains and concrete surface strains at the steel levels were recorded at each load increment in the post-cracking range.

Study on ECC Tensile Behavior due to Constrained Drying Shrinkage (구속된 건조수축에 따른 ECC의 인장거동에 관한 연구)

  • Lee, Do-Keun;Lee, Kyoung-Chan;Lee, Chi-Dong;Shin, Kyung-Joon
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.7 no.4
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    • pp.367-374
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    • 2019
  • Drying shrinkage in the hardened cement is known to change in volume by decreasing the moisture content in the hardened body, and it is known that the higher the W / C and the higher the content of the paste, the larger the drying shrinkage. In the case of ECC, more drying shrinkage occurs compared to concrete, since it does not contain coarse aggregate. Since ECC is an important material for tensile performance, the effect of restrained tensile stress on mechanical tensile behavior should be considered. The purpose of this study is to analyze the effect of stress caused by restraint on the tensile behavior of ECC. The mechanical properties of the specimens were tested by uniaxial tension tests with different restraints. As a result, the difference of tensile behavior according to restraint stress was observed and the cause was analyzed.

Microstructure and Mechanical Properties of AA6061/AA5052/AA6061 Complex Sheet Fabricated by Cold-Roll Bonding Process (냉간압연접합법에 의해 제조된 AA6061/AA5052/AA6061 복합판재의 미세조직 및 기계적 성질)

  • Hwang, Ju-Yeon;Lee, Seong-Hee
    • Korean Journal of Materials Research
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    • v.29 no.6
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    • pp.392-397
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    • 2019
  • A cold roll-bonding process is applied to fabricate an AA6061/AA5052/AA6061 three-layer clad sheet. Two AA6061 and one AA5052 sheets of 2 mm thickness, 40 mm width, and 300 mm length are stacked, with the AA5052 sheet located in the center. After surface treatment such as degreasing and wire brushing, sample is reduced to a thickness of 1.5 mm by multi-pass cold rolling. The rolling is performed at ambient temperature without lubricant using a 2-high mill with a roll diameter of 400 mm at rolling speed of 6.0 m/sec. The roll bonded AA6061/AA5052/AA6061 complex sheet is then hardened by natural aging(T4) and artificial aging(T6) treatments. The microstructures of the as-roll bonded and age-hardened Al complex sheets are revealed by optical microscopy; the mechanical properties are investigated by tensile testing and hardness testing. After rolling, the roll-bonded AA6061/AA5052/AA6061 sheets show a typical deformation structure in which grains are elongated in the rolling direction. However, after T4 and T6 aging treatment, there is a recrystallization structure consisting of coarse equiaxed grains in both AA5052 and AA6061 sheets. The as roll-bonded specimen shows a sandwich structure in which an AA5052 sheet is inserted into two AA6061 sheets with higher hardness. However, after T4 and T6 aging treatment, there is a different sandwich structure in which the hardness of the upper and lower layers of the AA6061 sheets is higher than that of the center of the AA5052 sheet. The strength values of the T4 and T6 age-treated specimens are found to increase by 1.3 and 1.4 times, respectively, compared to that value of the starting material.

Microstructure and Mechanical Properties of Cold Roll-Bonded Layered AA6061/AA5052/AA6061/AA5052 Aluminum Alloy Sheet (냉간압연접합된 층상 AA6061/AA5052/AA6061/AA5052 알루미늄합금판재의 미세조직 및 기계적 성질)

  • Jo, Sang-Hyeon;Park, Bo-Bae;Lee, Seong-Hee
    • Korean Journal of Materials Research
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    • v.32 no.3
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    • pp.161-167
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    • 2022
  • A cold roll-bonding process is applied to fabricate an AA6061/AA5052/AA6061/AA5052 layered sheet. Two AA6061 and one AA5052 sheets of 2mm thickness, 40mm width and 300mm length are alternately stacked, then reduced to a thickness of 2.0 mm by multi-pass cold rolling after surface treatment such as degreasing and wire brushing. The rolling is performed at ambient temperature without lubricant using a 2-high mill with a roll diameter of 400 mm at a rolling speed of 6.0 m/sec. The roll-bonded AA6061/AA5052/AA6061/AA5052 layered sheet is then hardened by natural aging (T4) and artificial aging (T6) treatments. The microstructure of the as-roll bonded and the age-hardened Al sheets was revealed by SEM observation; the mechanical properties were investigated by tensile testing and hardness testing. After T4 and T6 aging treatment, the specimens had a recrystallization structure consisting of coarse equiaxed grains in both AA5052 and AA6061 regions. The as-roll-bonded specimen showed a clad structure in which the hardness of AA5052 regions was higher than that of AA6061 regions. However, after T4 and T6 aging treatment, specimens exhibited different structures, with hardness of AA6061 regions higher than that of AA5052 regions. Strengths of T6 and T4 age-treated specimens were found to increase by 1.55 and 1.36 times, respectively, compared to the value of the starting material.

The Effects of Heat-treatment on the Mechanical Properties of High Chromium Cast Irons (고크롬 주철의 기계적 특성에 미치는 열처리 영향)

  • Kim, Sug-Won;Kim, Ki-Kon;Park, Jin-Sung;Kim, Dong-Keun;Yoon, Young-Gap
    • Journal of Korea Foundry Society
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    • v.25 no.1
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    • pp.23-29
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    • 2005
  • Mechanical characteristics of Hi-Cr cast irons containing 16.8%Cr and 3.0%C were studied with various heat treatments. After as-cast Y-block ingots were annealed fully, the ingots were machined into cylinderical specimens with the size of 9mm in diameter and 20mm in length in order to investigate the effect of heat-treatments on mechanical characteristics of high Cr cast irons. All specimens were heat-treated by quenching- tempering, austempering and cyclic heat at the various temperatures(950, 1000, 1050 and $1100^{\circ}C$) respectively. The wear amount was measured for each heat-treated specimens against the counterpart of a hardened SKD11 steel at the following conditions; wearing velocity: 0.7 m/s, load: 100N and sliding distance: 70 km. After as-cast specimens were annealed, fine $M_{3}C$ carbides were formed, which affected the hardness and the wear resistance of Hi-Cr specimens. High hardness and good wear resistance were appeared on the specimens treated at 950 and $1000^{\circ}C$ and the austempered specimens show excellent wear resistance as well as high hardness.