• Title/Summary/Keyword: HA coating

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The Development of Double Clad Fiber and Double Clad Fiber Coupler for Fiber Based Biomedical Imaging Systems

  • Ryu, Seon-Young;Choi, Hae-Young;Ju, Myeong-Jin;Na, Ji-Hoon;Choi, Woo-June;Lee, Byeong-Ha
    • Journal of the Optical Society of Korea
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    • v.13 no.3
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    • pp.310-315
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    • 2009
  • We report the fabrication of double clad fiber (DCF) and DCF coupler, suitable for fiber based imaging systems requiring the dual-channel transmission. Unlike the conventional DCF which uses silica for both cladding layers, the proposed DCF uses a low-index polymer for its outer-cladding layer coated over the conventional silica inner-cladding layer. The DCF is drawn with a conventional SMF preform but a low-index polymer coating is used for both jacket and outercladding of the fiber. To achieve the cladding mode coupling, a DCF coupler is fabricated by simply twisting two pieces of the proposed DCF after removing the polymer-coating at contacting regions. A cladding mode coupling ratio of 30% was achieved with a contact length of 16 cm. The proposed DCF and DCF coupler were employed in a composite optical coherence tomography (OCT) and fluorescence spectroscopy (FS) system, and both OCT images and FS signal from a plant tissue are measured simultaneously.

An Electrochemical Evaluation on the Corrosion Property of Metallizing Film (용사 도막의 내식성에 관한 전기화학적 평가)

  • Shin, Joong-Ha;Moon, Kyung-Man
    • Corrosion Science and Technology
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    • v.9 no.6
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    • pp.325-330
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    • 2010
  • Many surface protection methods have been developed to apply for constructional steels used under severe corrosive environment. Thermal spray coating has been known to be an attractive technique due to its relatively high coating speed. Furthermore high corrosion resistance of coated film with thermal spray is required to expand its application. Four types of coated films(DFT:300 um) such as pure zinc, pure aluminum and two Al-Zn alloy (Al:Zn=85:15 and Al:Zn=95:5) onto the carbon steel (SS401) were prepared with arc spray, and the corrosion behavior of their samples were evaluated by electrochemical method in this study. Pure aluminum sample showed high corrosion resistance behavior exposed to sea water solution and pure zinc and alloy (Al:Zn=95:5) samples followed pure aluminum sample. The other alloy(Al:Zn=85:15) so called galvalume coated onto the carbon steel ranks the 4th corrosion resistance in this study. The results of porosity ratio of those samples by observation are well matched with the electrochemical data.

A Study on the Degradation of Isopropyl Alcohol with $TiO_2-Coated$ Plastic Optic Fibers (광촉매 코팅 광섬유의 IPA 분해 특성 연구)

  • Yu Dong-Sik;Joo Hyun-Ku;Ha Jin-Wook
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.6 no.4
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    • pp.337-341
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    • 2005
  • The degradation of IPA according to coating conditions was examined by $TiO_2/P-25-coated$ POF. In the photoactivity of $TiO_2-coated$ POF, ethanol solvent was higher activity than other solvents. Inorganic(KR-400), organic(A-9540) and inorganic$\cdot$organic hybrid(GPTMS, TMOS) resins were used as binder. Organic binder(A-9540) showed the highest activity for degradation of IPA, but organic binder was decomposed by $TiO_2$. Inorganic binder had lower binder ability than others, and lower adhesive than organic binders. In TMOS as inorganic · organic hybrid binder, activity of IPA degradation was decreased by addition of TMOS when the ratio of TMOS and P-25 was changed from 0.05 to 1.

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Surface Discoloration of Ultraviolet (UV)-Irradiated Phyllostachys bambusoides Bamboo

  • Hyoung-Woo LEE;Eun-Ju LEE;Yoon-Jung SHIN;Ha-Yeong JO;Dae-Yeon SONG
    • Journal of the Korean Wood Science and Technology
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    • v.51 no.3
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    • pp.173-182
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    • 2023
  • Color is an attribute of visual perception and can be an important factor that affects the preference of customers toward bamboo and wood products. Solar radiation can discolor bamboo surfaces and initiate cracking. The purpose of this study is to investigate the effects of an ultraviolet (UV)-protective coating on the photodiscoloration of untreated and heat-treated Phyllostachys bambusoides bamboo surfaces. Artificial UVA radiators are set at a UVA irradiance of 2,000 W/m2 to accelerate the aging of the outer surfaces of hot-air-dried and heat-treated bamboo samples. Half of the samples are coated with transparent UV-protective paint. As the UVA radiation progresses, the discoloration prevention efficiency (DPE) of the UV-protective coating on all samples decreases gradually. The DPEs of the hot-air-dried samples are estimated to be 31.4% and 18.8% after 21 and 72 hours of artificial UVA radiation, respectively. The heat-treated samples exhibit similar trends (29.0% after 21 hours and 10.3% after 72 hours). Recoating the UV-protective paint periodically every six months is expected to minimize the discoloration of the bamboo's outer surface.

Characteristics of Bio-Piezoelectric Generator Using Edible Collagen Powder (식용 콜라겐 분말을 적용한 바이오 압전 발전기의 특성)

  • Ha-Young Son;Sang-Shik Park
    • Korean Journal of Materials Research
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    • v.34 no.4
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    • pp.215-222
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    • 2024
  • Because collagen is inherently piezoelectric, research is being actively conducted to utilize it to harvest energy. In this study, a collagen solution was prepared using edible low-molecular-weight peptide collagen powder, and collagen films were fabricated using a dip coating method. The collagen films prepared by dip coating showed a smooth surface without defects such as pinholes or cracks. Dehydrothermal treatment of the collagen films was performed to induce a stable molecular structure through cross-linking. The collagen film subjected to dehydrothermal treatment at 110 ℃ for 24 h showed a thickness reduction rate of 19 %. Analysis of the collagen films showed that the crystallinity of the collagen film improved by about 7.9 % after dehydrothermal treatment. A collagen film-based piezoelectric nanogenerator showed output characteristics of approximately 13.7 V and 1.4 ㎂ in a pressure test of 120 N. The generator showed a maximum power density of about 2.91 mW/m2 and an output voltage of about 8~19 V during various human body movements such as finger tapping. The collagen film-based piezoelectric generator showed improved output performance with improved crystallinity and piezoelectricity after dehydrothermal treatment.

A Proposal for Standardization of Tongue Diagnosis Based on Diagnostic Criteria of Tongue Coating Thickness (설진의 표준화를 위한 제언 : 설태 후박의 진단기준을 중심으로)

  • Son, Ji-Hee;Kim, Jin-Sung;Park, Jae-Woo;Ryu, Bong-Ha
    • The Journal of Internal Korean Medicine
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    • v.33 no.1
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    • pp.1-13
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    • 2012
  • Background : In oriental medicine, the status of the tongue is an important indicator to diagnose the condition of one's health, such as physiological and the clinicopathological changes of internal organs. A tongue diagnosis is not only convenient but also non-invasive, and therefore widely used in Oriental medicine. However, the tongue diagnosis is greatly affected by examination circumstances, patient's posture, and doctor's diagnosis criteria. Objectives : This study was designed to assure the necessity for standardization of tongue diagnosis based on diagnostic criteria of tongue coating thickness (TCT). Methods : Thirty tongue photographs were acquired and analyzed by digital tongue diagnosis system (DTDS) which measured the percentage of TCT on the tongue surface. Fifteen oriental medical doctors evaluated TCT in 30 photographs. Afterward, the 15 assessors were trained for diagnostic criteria of TCT and evaluated the photographs again. The intraclass correlation coefficient (ICC) was used to obtain the agreement rate among the 15 assessors and the agreement rate between assessors' TCT scores and DTDS values. Results : The agreement rate among the 15 assessors after training was higher than before training. The agreement rate between assessors' TCT scores and DTDS values after training was also higher than before training. Furthermore, the difference of the agreement rate between before and after training was significant (p<0.05). Conclusions : The standardization of diagnostic criteria of TCT increased the agreement rate among the assessors and the agreement rate between assessors' TCT scores and DTDS values. Therefore, the standardization of diagnostic criteria is expected to contribute to the objectification and quantification of the tongue diagnosis system.

Reduced Burst Release from ePTFE Grafts: A New Coating Method for Controlled Drug Release

  • Nam, Hye-Yeong;Kim, Dae-Joong;Lim, Hyun-Jung;Lee, Byung-Ha;Baek, In-Su;Park, Sang-Hun;Park, Jong-Sang
    • Bulletin of the Korean Chemical Society
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    • v.29 no.2
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    • pp.422-426
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    • 2008
  • Hemodialysis graft coated with paclitaxel prevents stenosis; however, large initial burst release of paclitaxel causes many negative effects such as drug toxicity and inefficient drug loss. Therefore we developed and tested a novel coating method, double dipping, to provide controlled and sustained release of paclitaxel locally. Expanded polytetrafluoroethylene (ePTFE) grafts were dipped twice into a solution of several different paclitaxel concentrations. In vitro release tests of the double dipping method showed that early burst release could be somewhat retarded and followed by sustained release for a long time. We observed the effect of paclitaxel coating by double dipping in porcine model of arterio-venous (AV) grafts between the common carotid artery and the external jugular vein. 12 weeks after constructing AV grafts, cross sections of the graft venous anastomosis were obtained and analyzed. Paclitaxel coated ePTFE grafts by double dipping were observed to prevent neointimal hyperplasia and therefore reduced stenosis of the arteriovenous hemodialysis grafts, especially at the graft venous anastomosis sites. Our results demonstrate that second dipping of ePTFE graft, which was already coated once with paclitaxel, washes off the drug on a surface of the graft and affects the ratio of paclitaxel on the surface to that of the inner space, possibly by diffusion: thus the early burst of drug can be somewhat reduced.

Formation of Uniform SnO2 Coating Layer on Carbon Nanofiber by Pretreatment in Atomic Layer Deposition (전처리를 이용한 탄소 나노 섬유의 균일한 SnO2 코팅막 형성)

  • Kim, Dong Ha;Riu, Doh-Hyung;Choi, Byung Joon
    • Journal of Powder Materials
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    • v.25 no.1
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    • pp.43-47
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    • 2018
  • Carbon nanofibers (CNF) are widely used as active agents for electrodes in Li-ion secondary battery cells, supercapacitors, and fuel cells. Nanoscale coatings on CNF electrodes can increase the output and lifespan of battery devices. Atomic layer deposition (ALD) can control the coating thickness at the nanoscale regardless of the shape, suitable for coating CNFs. However, because the CNF surface comprises stable C-C bonds, initiating homogeneous nuclear formation is difficult because of the lack of initial nucleation sites. This study introduces uniform nucleation site formation on CNF surfaces to promote a uniform $SnO_2$ layer. We pretreat the CNF surface by introducing $H_2O$ or $Al_2O_3$ (trimethylaluminum + $H_2O$) before the $SnO_2$ ALD process to form active sites on the CNF surface. Transmission electron microscopy and energy-dispersive spectroscopy both identify the $SnO_2$ layer morphology on the CNF. The $Al_2O_3$-pretreated sample shows a uniform $SnO_2$ layer, while island-type $SnO_x$ layers grow sparsely on the $H_2O$-pretreated or untreated CNF.

Hydrothermal Coating of Hydroxyapatite on ZrO2 Ceramics

  • Ha, Jung-Soo
    • Journal of the Korean Ceramic Society
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    • v.43 no.8 s.291
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    • pp.463-468
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    • 2006
  • Hydrothermal deposition of hydroxyapatite coatings on two types of $ZrO_2$ substrates (3 mol% $Y_2O_3$-doped and 13 mol% $CeO_2$-doped tetragonal $ZrO_2s$) was studied using aqueous solutions of $Ca(NO_3)_2\;4H_2O$ and $(NH_4)_2HPO_4$ containing EDTA (ethylene diamine tetra acetic acid) disodium salt as a chelating agent for $Ca^{2+}$ ions. For the precipitation of the coatings, the $EDTA-Ca^{2+}$ chelates were decomposed by oxidation with $H_2O_2$ at $90^{\circ}C$. The deposition behavior, morphology, and orientation of the coatings were investigated while varying the solution pH using scanning electron microscopy and X-ray diffractometry. For the two sub-strates, sparse deposition of the coating was obtained at pH 5.5, whereas a uniform deposition was obtained at pH 7.1, 9.8, and 11.4 with a denser microstructure for the higher pH. The coating consisted of thin needle-like or plate-like crystals ($1-2{\mu}m$ length or diameter) at pH 7.1, but fine rod-like crystals ($1-2{\mu}m$ length, $0.1{\mu}m$ diameter) at pH 9.8 and 11.4. The coatings were $1-3{\mu}m$ thick and showed a preferred orientation of the hydroxyapatite crystals with their c axis (i.e., the elongated direction) perpendicular to the substrate surface especially for pH 9.8 and 11.4.

Improvement of Electrical Conductivity of Carbon-Fiber Reinforced Plastics by Nano-particles Coating (나노입자 코팅 탄소섬유 강화 복합재료의 전기전도도 향상)

  • Seo, Seong-Wook;Ha, Min-Seok;Kwon, Oh-Yang;Cho, Heung-Soap
    • Composites Research
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    • v.23 no.6
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    • pp.1-6
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    • 2010
  • The electrical conductivity of carbon-fiber reinforced plastics (CFRP's) has been improved by indium-tin oxide (ITO) nano-particle coating on carbon fibers for the purpose of lightning strike protection of composite fuselage skins. ITO nano-particles were coated on the surface of carbon fibers by spraying the colloidal suspension with 10~40% ITO content. The electrical conductivity of the CFRP has been increased more than three times after ITO coating, comparable to or higher than that of B-787 composite fuselage skins with metal wire-meshes on the outer surface, without sacrificing the tensile property due to the existence of nano-particles at fiber-matrix interface. The damage area by the simulated lightning strike was also verified for different materials and conditions by using ultrasonic C-scan image. As the electrical conductivity of 40% nano-ITO coated sample surpass that of the B-787 sample, the damage area by lightning strike also appeared comparable to that of the materials currently employed for composite fuselage construction.