• Title/Summary/Keyword: Grain boundary structure

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Finite Element Analysis of Multi-Stage Deep Drawing Process for High Precision Rectangular Case with Extreme Aspect Ratio (세장비가 큰 사각컵 디프 드로잉의 유한요소 해석)

  • Ku T.W.;Ha B.K.;Song W.J.;Kang B.S.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2002.02a
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    • pp.274-284
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    • 2002
  • Deep drawing process for rectangular drawn section is different with that for axisymmetric circular one. Therefore deep drawing process for rectangular drawn section requires several intermediate steps to generate the final configuration without any significant defect. In this study, finite element analysis for multi-stage deep drawing process for high precision rectangular cases is carried out especially for an extreme aspect ratio. The analysis is performed using rigid-plastic finite element method with an explicit time integration scheme of the commercial program, LS-DYNA3D. The sheet blank is modeled using eight-node continuum brick elements. The results of analysis show that the irregular contact condition between blank and die affects the occurrence of failure, and the difference of aspect ratio in the drawn section leads to non-uniform metal flow, which may cause failure. A series of experiments for multi-stage deep drawing process for the rectangular cases are conducted, and the deformation configuration and the thickness distribution of the drawn rectangular cases are investigated by comparing with the results of the numerical analysis. The numerical analysis with an explicit time integration scheme shows good agreement with the experimental observation.

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Structural and piezoelectric properties of lead-free (1-x)$(Na_{0.5}\;K_{0.5})NbO_3$-xBa($Ti_{0.9}$, $Sn_{0.1}$)$O_3$ ceramics

  • Cha, Yu-Jeong;Nam, San;Kim, Chang-Il;Jeong, Yeong-Hun;Lee, Yeong-Jin;Baek, Jong-Hu
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.05a
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    • pp.33.1-33.1
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    • 2009
  • Lead-free (1-x)$(Na_{0.5}K_{0.5})NbO_3$-xBa($Ti_{0.9}Sn_{0.1})O_3$ [NKN-BTS-100x] ceramics doped with 1 mol% $MnO_2$ have been prepared by the conventional solid state method and their structural and piezoelectric properties were investigated. The NKN-BTS-100x ceramics exhibited a dense and homogeneous microstructure when they were sintered at $1030-1150^{\circ}C$. Grain growth was observed for the specimen sintered at relatively low temperature of $1050^{\circ}C$. A tetragonal/orthorhombic morphotropic phase boundary (MPB) in the perovskite structure was also appeared for the NKN-BTS-100x ceramics (0.04$1050^{\circ}C$. The enhanced piezoelectric properties in the NKN-BTS ceramics with a MPB composition were obtained. Especially, for the NKN-BTS-6 ceramics, a high dielectric constant (${\varepsilon}^T_3/\varepsilon_0=1,400$), piezoelectric constant ($d_{33}=237$) and electromechanical coupling factor ($k_p=0.42$) were obtained.

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Effect of a Matrix Structure on the Initiation of Fatigue Crack and Fatigue Strength in Nodular Graphite Cast Iron (구상흑연 주철재의 피로크랙 발생 및 피로강도에 미치는 기지조직의 영향)

  • Yoon, Myung-Jin;Lee, Kyoung-Mo
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.7 no.5
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    • pp.66-71
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    • 1998
  • It is required the superior materials for the parts of machines or structures, which could be endurable in severe load and environment. According to advancement of casting technology, nodular graphite cast iron is used as suitable for such condition. But nodular graphite cast iron is scattering of fatigue strength and low reliability. Therefore in this study, the effect of matrix structure and number of nodular graphite on the initiation of fatigue crack and fatigue strength. It was found that the material which has relatively high ferrite volume fraction was more easily cracked than other materials and fatigue limit was low. The material which has not found pinhole on the surface, the crack was initiated in graphite went through ferrite and propagated into through graphite, but separated graphite and ferrite grain boundary and combined with other cracks to fro large one.

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Electrical properties of (Na0.5Bi0.5)(Zr0.75Ti0.25)O3 ceramic

  • Lily, Lily;Yadav, K.L.;Prasad, K.
    • Advances in materials Research
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    • v.2 no.1
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    • pp.1-13
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    • 2013
  • Lead-free compound $(Na_{0.5}Bi_{0.5})(Zr_{0.75}Ti_{0.25})O_3$ was prepared using conventional ceramic technique at $1070^{\circ}C$/4h in air atmosphere. X-ray diffraction analysis showed the formation of single-phase orthorhombic structure. Permittivity data showed low temperature coefficient of capacitance ($T_{CC}{\approx}5%$) up to $100^{\circ}C$. Complex impedance studies indicated the presence of grain boundary effect, non-Debye type dielectric relaxation and evidences of a negative temperature coefficient of resistance. The ac conductivity data were used to evaluate the density of states at Fermi level and apparent activation energy of the compound.

Effect of Heat Treatment on Properties of Varistors (바리스터의 물성에 미치는 열처리 효과)

  • 홍경진;민용기;오수홍;조재철
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.07a
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    • pp.955-958
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    • 2001
  • The structure characteristics of varistor of Zn oxide to depend on the breakdown voltage has been investigated to annealing condition by additive material of Sb$_2$O$_3$ system. The breakdown voltage that has not doping Sb$_2$O$_3$ was 235[V]. ZnO varistors was shown ohmic properties when it's applied voltage was below critical voltage. It was shown non-ohmic properties over critical voltage, because current was increased with decreasing resistance. High voltage ZnO varistors had high breakdown voltage, but it had bad electrical stability with various surge. Sb$_2$O$_3$was increased non-linear coefficient in ZnO varistors grain boundary.

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Fatigue Crack Retardation and Retardation Mechanism in Variable Loading (The Effects of Crack Tip Branching in Crack Growth Retardation)

  • Song, Sam-Hong;Kwon, Yun-Ki
    • International Journal of Precision Engineering and Manufacturing
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    • v.3 no.3
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    • pp.76-81
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    • 2002
  • In order to study the fatigue crack and retardation mechanism in variable loading, the effects of crack tip branching in crack growth retardation were examined. The characteristics of crack tip branching behavior were considered with respect to microstructure and crack tip branching angle was examined. Crack tip branching was observed along the grain boundary of finite and pearlite structure. It was found that the branching angle ranges from 25 to 53 degrees. Using the finite element method, the variable of crack driving farce to branching angle was examined. The effective crack driving farce (K$\_$eff/) decreased as the branching angle increased. The rate of decrease was 33% for kinked type and 29% for forked one. It was confirmed that the effect of crack tip branching is a very important factor in crack growth retardation. Therefore, crack branching effect should be considered in building the hypothetical model to predict crack growth retardation.

Numerical Simulationof Plaster Casting with Pressurized Vibration (진동을 부가한 저압의 석고주조 공정 해석)

  • Kim, Gi-Don;Yang, Dong-Yeol;Jeong, Jun-Ho
    • Journal of the Korean Society for Precision Engineering
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    • v.18 no.9
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    • pp.101-109
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    • 2001
  • The simulated die casting process in which the traditional plaster casting process is combined with rapid prototyping technology is being used to produce Al, Mg and Zn die casting prototypes. Because of lower mechanical properties induced by the large grain structure and incomplete filling, conventional plaster casting is not suitable for the simulated die casting process. A plaster casting process with pressurized vibration was developed for the simulated die casting process[5]. In this paper, numerical simulation for the filling stage of the process has been performed to show the effect of the pressurized vibration for complete filling. Treatment of boundary condition based on the finite element method has been proposed for imparted pressurized vibration in the plaster casting process.

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Effect of $Mo_2C$ Content on the Microstructure and Properties of Ti(CN)-$Mo_2C$ Ceramics

  • Park, Dong-Soo;Lee, Yang-Doo;Taejoo Jung
    • The Korean Journal of Ceramics
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    • v.5 no.3
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    • pp.230-234
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    • 1999
  • Ti(CN)-0.3mole% $Mo_2C$ ceramics were prepared by pressureless sintering. $Mo_2C$ dissolved in Ti(CN) more easily in a nitrogen environment than in the other environment because nitrogen forced Mo to form a solid solution, (Ti, No)(C, N). A "core-rim" structure developed within the grains. The boundary between the "core" and the rim was delineated by thermal etching in the sample with more than 2 mole% $Mo_2C$. The rim thickness and the grain size decreased as the $Mo_2C$ content increased. The hardness and the flexural strength showed maxima of 18.2 GPa and 1.23 GPa, respectively when the $Mo_2C$ content was 2 mole%. The post-sintering heat treatments improved the properties.oved the properties.

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Reaction diffusion and formation of$Ni_3Al$ phase at the Ni-NiAl diffusion couple (Ni-NiAl 확산대에서 $Ni_3Al$ 상의 형성과 반응확산)

  • 정승부
    • Journal of Welding and Joining
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    • v.15 no.3
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    • pp.128-135
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    • 1997
  • Reaction diffusion and formation of $Ni_3Al$phase with $L1_2$ structure have been studied in temperature range of 1432K to 1573K using the diffusion couple of (Ni-40, 5at%Al)/(Ni-14, 1at%Al) and (Ni-49, 2at%Al)/ (Nickel). The layer growth of Ni$_{3}$Al pyhase in the annealed diffusion couple was measured by optical microscope and electron probe microanalyzer (EPMA). The layer growth of $Ni_3Al$phase in diffusion zone obeyed the parabolic law without any indication of grain boundary effects. The layer growth of $Ni_3Al$phase in temperature range of 1423K to 1573K was mainly controlled by the volume diffusion mechanism. The rate of layer growth of $Ni_3Al$phase was found to be colsely related to the composition of intermetallic compound NiAl phase. The activation energy for layer growth of $Ni_3Al$phase was calculated to be 127kJ/mol.

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Thermal Residual Stress Relaxation Behavior of Alumina/SiC Nanocomposites (Alumina/SiC 나노복합재료에서의 잔류 열응력 완화거동에 관한 연구)

  • Choa, Y.H.;Niihara, K.;Ohji, T.;Singh, J.P.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2002.04b
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    • pp.11-11
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    • 2002
  • Plastic deformation was observed by TEM around the intragranular SiC particles in the $Al_2O_3$ matrix for $Al_2O_3/SiC$ nanocomposite system. The dislocations are generated at selected planes and there is a tendency for the dislocations to form a subgrain boundary structure with low-angel grain boundaries and networks. In this study, dislocation generated in the $Al_2O_3$ matrix during cooling down from sintering temperatures by the highly localized thermal stresses within and/or around SiC particles caused from the thermal expansion mismatch between $Al_2O_3$ matrix and SiC particle was observed. In monolithic $Al_2O_3$ and $Al_2O_3/SiC$ microcomposite system. These phenomena is closely related to the plastic relaxation of the elastic stress and strain energy associated with both thermal misfitting inclusions and creep behaviors. The plastic relaxation behavior was explained by combination of yield stress and internal stress.

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