• 제목/요약/키워드: Grain Size Distributions

검색결과 96건 처리시간 0.026초

소결법에 의한 다공질 결정화유리의 제조 (Preparation of Porous Glass-Ceramics by the Sintering)

  • 박용완;이준영
    • 한국세라믹학회지
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    • 제31권10호
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    • pp.1218-1230
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    • 1994
  • In manufacturing process of porous glass-ceramics by the filler method, the sintering behaviour of crystallizable glass powder mixed with various salts was studied and also the effects of precipitated crystal phases on the properties of porous glass-ceramics were investigated. Fine-grained crystallizable glass powder was homogeneously mixed with various slat having grain size 100~200 ${\mu}{\textrm}{m}$ and sintered for densification. After washing out the inorganic salt with distilled water, the porous sintered body was heat treated additionly for crystallization. The MgO-Al2O3-SiO2 base glass was used as crystallizable glass powder and the water soluble salts such as K2SO4 and MgSO4 were used as filler. When K2SO4 was used, leucite crystal phase was formed as a result of the ion exchange and porous glass-ceramics which exhibit high temperature resistance and high thermal expansion coefficient of 17$\times$10-6/$^{\circ}C$ could be obtained. On the contrary, when MgSO4 was used, only slight ion exchange is observed and $\mu$-cordierite and $\alpha$-cordierite crystal phases were formed and porous glass-ceramics which exhibit low thermal expansion coefficient schedule were determined with the results of DTA curves, thermal shrinkage curves and XRD patterns analysis. From DTA curves and thermal shrinkage curves, it was found that the sintering densification have been completed at the temperature range of exothermic peak for crystallization. The pore size distributions and pore diameters were measured by mercury porosimeter. The pore diameter of porous glass-ceramics was 10~15 ${\mu}{\textrm}{m}$ when 100~200${\mu}{\textrm}{m}$ grain size of K2SO4 was used and it was 25~30 ${\mu}{\textrm}{m}$ when the same grain size of MgSO4 was used. The porous glass-ceramics K2SO4 used shows bimodal pore size distribution and its porous skeleton structure was ascertained by SEM observation.

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고체 램제트 추진기관 연소실에서의 연소 현상 (Combustion Behavior in a Solid Fuel Ramjet Combustor)

  • Lee, T. H.
    • 한국추진공학회지
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    • 제3권3호
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    • pp.25-30
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    • 1999
  • 본 연구는 보론 카바이드를 함유한 고체 연료를 사용하여 고체 램제트에서 공기 유속량에 따른 연소효율과 입자 크기의 분포를 실험적으로 조사하였다. 입자 분포는 그레인 끝 부분과 노즐 입구에서 MALVERN 2600 HSD를 사용하여 측정하였다. 연소 효율은 공기 유속량이 적을수록 연소 효율이 높은 것으로 나타났으며, 일반적으로 입자 분포는 대략적으로 4, 15와 25$\mu\textrm{m}$, 경우에 따라 2$\mu\textrm{m}$ 보다 적은 크기에서 한 곳을 포함하여 3곳의 피크치 또는 4 곳의 피크치를 나타내는 분포를 보였다. 큰 입자는 주로 재순환 영역에서 표면에서의 입자들의 뭉침의 결과이다. 흡입 공기의 온도가 높으면 연소 효율이 좋았는데 이는 확산 영역에서 연소하는 큰 보론 카바이드 입자의 연소 촉진 결과로 보인다.

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교차롤압연된 Ni-10Cr 합금의 결정립 미세화와 성형성 향상 (Enhancement of Grain Refinement and Formability of Cross-Roll-Rolled Ni-10Cr Alloy)

  • 송국현;김원용;손현택
    • 한국재료학회지
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    • 제22권6호
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    • pp.303-308
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    • 2012
  • This study evaluated the enhancement of microstructural and mechanical properties of a cross rolled Ni-10Cr alloy, comparing with conventionally rolled material. Cold rolling was carried out to 90% thickness reduction and the specimens were subsequently annealed at $700^{\circ}C$ for 30 min to obtain a fully recrystallized microstructure. Cross roll rolling was carried out at a tilted roll mill condition of $5^{\circ}$ from the transverse direction in the RD-TD plane. In order to observe the deformed microstructures of the cold rolled materials, transmission electron microscopy was employed. For annealed materials after rolling, in order to investigate the grain boundary characteristic distributions, an electron back-scattering diffraction technique was applied. Application of cold rolling to the Ni-10Cr alloy contributed to notable grain refinement, and consequently the average grain size was refined from 135 ${\mu}m$ in the initial material to 9.4 and 4.2 ${\mu}m$ in conventionally rolled and cross rolled materials, respectively, thus showing more significantly refined grains in the cross rolled material. This refined grain size led to enhanced mechanical properties such as yield and tensile strengths, with slightly higher values in the cross rolled material. Furthermore, the <111>//ND texture in the CRR material was better developed compared to that of the CR material, which contributed to enhanced mechanical properties and formability.

강가공된 순수 Cu의 미세조직과 기계적 특성 평가 (Evaluation on Microstructure and Mechanical Properties of Severely Deformed Pure Cu)

  • 송국현;손현택;김대근;김한솔;김원용
    • 한국재료학회지
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    • 제21권5호
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    • pp.263-267
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    • 2011
  • The present study was carried out to evaluate the microstructural and mechanical properties of cross-roll rolled pure copper sheets, and the results were compared with those obtained for conventionally rolled sheets. For this work, pure copper (99.99 mass%) sheets with thickness of 5 mm were prepared as the starting material. The sheets were cold rolled to 90% thickness reduction and subsequently annealed at $400^{\circ}C$ for 30 min. Also, to analyze the grain boundary character distributions (GBCDs) on the materials, the electron back-scattered diffraction (EBSD) technique was introduced. The resulting cold-rolled and annealed sheets had considerably finer grains than the initial sheets with an average size of 100 ${\mu}M$. In particular, the average grain size became smaller by cross-roll rolling (6.5 ${\mu}M$) than by conventional rolling (9.8 ${\mu}M$). These grain refinements directly led to enhanced mechanical properties such as Vickers micro-hardness and tensile strength, and thus the values showed greater increases upon cross-roll rolling process than after conventional rolling. Furthermore, the texture development of <112>//ND in the cross-roll rolling processed material provided greater enhancement of mechanical properties relative to the case of the conventional rolling processed material. In the present study, we systematically discuss the enhancement of mechanical properties in terms of grain refinement and texture distribution developed by the different rolling processes.

흙의 다짐에 관한 연구(제4보) -흙의 다짐이 -축골조강동 및 투수계수에 미치는 영향- (Study on the Soil Compaction (Part 4) -The Influence of Soil Compadtion on Unconfined Compressive Strength and Coefficient of Permeability-)

  • 강예묵
    • 한국농공학회지
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    • 제12권3호
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    • pp.2003-2012
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    • 1970
  • In order to the influence of grain size distribution on compressive strength and coefficient of permeability, unconfined compression test and permeability test were performed for seventy samples that have various grain-size distributions. Its results are as follows: 1. Maximum unconfined compressive strength appears at the dry side of optimum moisture content. 2. Unconfined compressive strength is proportional to the increase of percent passing of No. 200 sieve. 3. Precent of deformation in failure increases in proportion to the increase of percent passing of No. 200 sieve, and modulus of No. 200 sieve, and modulus of deformation also increases in proportion to percent passing of No. 200 sieve. 4. Unconfined compressive strength increases in proportion to uniformity coefficient, liquid limit and plastic index, but it decreases gradually according to the increase of coefficient of grading and classification area. 5. Maximum dry density decreases according to the increase of void ratio. 6. Coefficient of permeability decreases according to the increase of percent passing of No. 200 sieve, and when percent of No. 200 sieve, and when percent passing of No. 200 enlarged more than 40%, it becomes less than $10^{-6}cm/sec$ which is the limit of coefficient of permeability of core material for earth dam proposed by Lee. 7. Coefficient of permeability increases according to the increase of coefficient of grading, classification area and index of Talbot formula r, but it was rather decrease by the increase of uniformity coefficient. 8. Coefficient of permeability seems to depend on the size and the shape of the flow path which is a series of void to be concerned by the size and the proprton of soil grain, even though void ratios are same.

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NUMERICAL MODELLING OF SEDIMENT TRANSPORT IN CONNECTION WITH ARTIFICIAL GRAIN FEEDING ACTIVITIES IN THE RIVER RHINE

  • Duc Bui Minh;Wenka Thomas
    • Water Engineering Research
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    • 제6권1호
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    • pp.17-30
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    • 2005
  • The bed evolution of the stretch of the River Rhine between km-812.5 and km-821.5 is characterised by general bed degradation as a result of the river training works and dredging activities of the last two centuries. The degradation of the river bed affects the water levels, and so the navigation conditions. To combat the erosion of the river bed with the aim to keep up the shipping traffic and to avoid the ecological system damages due to water level reductions, sand-gravel-mixtures were added to the river (so called artificial grain feeding activities). This paper presents the results of an application of a graded sediment transport model in order to study morpholodynamical characteristics due to artificial grain feeding activities in the river stretch. The finite element code TELEMAC2D was used for flow calculation by solving the 2D shallow water equation on non-structured grids. The sediment transport module SISYPHE has been developed for graded sediment transport using a multiple layer model. The needs to apply such graded sediment transport approaches to study morphological processes in the domain are discussed. The calculations have been carried out for the case of middle water flow and different size-fraction distributions. The results show that the grain feeding process could be well simulated by the model.

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낙동강 하구 신자도 해빈 퇴적물 입도의 시간적인 변화 (Temporal Change of Grain Size of the Beach Sediments in the Sinjado, Nakdong River Estuary)

  • 김백운;이상룡;김부근
    • 한국해안·해양공학회논문집
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    • 제23권4호
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    • pp.304-312
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    • 2011
  • 낙동강 하구 신자도에서 2005년 11월과 2006년 5월에 남쪽 해빈의 상부, 중부 및 하부 조간대에 해당하는 3개의 횡단선(upper, middle 및 lower transect)을 따라 67개 정점에서 총 402개의 표층퇴적물을 채취하여 입도 분석을 실시하였다. 신자도 해빈 퇴적물은 단일 모드의 입도로 구성되었고, 2005년에는 $3.0{\phi}$의 최빈값이 우세하였으며, 2006년에는 $2.5{\phi}$의 최빈값이 우세하였다. 이러한 퇴적물의 조립화는 신자도 해빈의 서쪽 지역과 중부 및 하부 정점들에서 더욱 뚜렷하였다. 이 연구에서는 조위에 의해 구분된 횡단선 자료에 근거하여 퇴적물 입도의 시간적인 변화 특성을 규명하는데 초점을 두었다. 이와 같은 목적을 위하여 횡단선간에 평균입도, 분급도 및 왜도와 같은 퇴적물 조직 변수를 비교할 수 있는 통계적 검정법을 이용하였다. 평균입도는 해빈 중부와 하부 정점들에서, 분급도는 해빈 상부와 하부 정점들에서, 왜도는 해빈 전체에서 통계적으로 유의한 시간적인 변화가 나타났다. 또한, 평균입도와 왜도 사이에 역의 상관관계는 2005년에 비하여 2006년에 더욱 뚜렷하였다. 2005년 11월에서 2006년 5월까지 신자도 해빈 퇴적물의 시간적인 변화는 평균입도와 분급도는 감소하였고, 왜도는 증가하였으며, 평균입도와 왜도 사이에 역의 상관관계가 강화되었다.

Grain Growth Revealed by Multi-wavelength Analysis of Non-axisymmetric Substructures in the Protostellar Disk WL 17

  • Han, Ilseung;Kwon, Woojin;Aso, Yusuke
    • 천문학회보
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    • 제45권1호
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    • pp.59.2-59.2
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    • 2020
  • Disks around protostars are the birthplace of planets. The first step toward planet formation is grain growth from ㎛-sized grains to mm/cm-sized grains in a disk, particularly in dense regions. In order to study whether grains grow and segregate at the protostellar stage, we investigate the ALMA Band 3 (3.1 mm) and 7 (0.87 mm) dust continuum observations of the protostellar disk WL 17 in ρ Ophiuchus L1688 cloud. As reported in a previous study, the Band 3 image shows substructures: a narrow ring and a large central hole. On the other hand, the Band 7 image shows different substructures: a non-axisymmetric ring and an off-center hole. The two-band observations provide a mean spectral index of 2.3, which suggests the presence of mm/cm-sized large grains. Its non-axisymmetric distribution may imply dust segregation between small and large grains. We perform radiative transfer modeling to examine the size and spatial distributions of dust grains in the WL 17 disk. The best-fit model suggests that large grains (>1 cm) exist in the disk, settling down toward the midplane, whereas small grains (~10 ㎛) well mixed with gas are distributed off-center and non-axisymmetrically in a thick layer. The low spectral index and the modeling results suggest that grains rapidly grow at the protostellar stage and that grains differently distribute depending on sizes, resulting in substructures varying with observed wavelengths. To understand the differential grain distributions and substructures, we discuss the effects of the protoplanet(s) expected inside the large hole and the possibility of gravitational instability.

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목포-해남 연안 조간대 퇴적물중 유기물 및 미량금속 분포 특성 (Distributions of Organic Matter and Trace Metals in Intertidal Surface Sediment from the Mokpo-Haenam Coast)

  • 황동운;김평중;정래홍;윤상필
    • 한국수산과학회지
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    • 제46권4호
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    • pp.454-466
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    • 2013
  • To evaluate the organic matter and trace metal pollution in intertidal sediment of the coastal zone, various geochemical parameters (grain size, ignition loss [IL], chemical oxygen demand [COD], acid volatile sulfide [AVS], and metals [Al, Fe, Cu, Pb, Zn, Cd, Cr, Mn, Hg, and As]) were measured for the intertidal surface sediment of the mainland and islands between Mokpo and Haenam in the southwestern coast of Korea. The surface sediments consist mainly of finer sediments, such as mud and silt. The concentrations of IL, COD, and trace metals in intertidal sediment were relatively high in the shoreline of the mainland than in that of islands and those in some stations exceeded the sediment quality guidelines (SQGs). Moreover, the concentrations of IL, COD, and trace metals (except As) in sediment showed relatively good positive correlations with mean grain size, indicating that the concentrations of organic matter and trace metals in intertidal sediment of the study region are dependent on grain size of sediment. Pollution evaluation for trace metals using geochemical assessment techniques, such as enrichment factor, geoaccumulation index, and SQGs, suggested that the intertidal sediments in the study region show light pollution with Cr and moderate pollution with As. More extensive interdisciplinary studies are required to determine the potential causes of As pollution in intertidal sediment.

대형 오이도미터 시험을 통한 Rockfill 재료의 압축성 평가 (Evaluation of Compressibility of Rock Fill Materials by Large-Scale Oedometer Tests)

  • 김범주;신동훈;전제성;임정열
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2005년도 춘계 학술발표회 논문집
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    • pp.627-632
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    • 2005
  • In this study, a series of large-scale oedometer tests was performed to investigate the compressibility of rock fill materials. The testing samples were prepared to have three different grain size distributions and for each distribution, exist in two different states(dried and saturated). The test results indicated that particle breakages occurred mainly for the particles larger than 4.75mm in size and increased with increasing grain sizes. Also, it was found that, for a dry sample as it became well-graged, its compressibility decreased and accordingly, its tangent constrained modulus increased. A comparion between the samples in dry and saturated states revealed that compressibility of the materials increases with increasing water content. The values of tangent constrained modulus calculated for the tested dry samples were larger by about 10 to 20%, on average, than those for the saturated samples.

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