• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2006년 추계학술발표대회 개요집
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• pp.123-124
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• 2006

This study aimed at exploiting low heat input characteristic of laser welding to effectively control grain coarsening in the fusion zone(FZ) and heat affected zone(HAZ) of 1.5mm thick 18wt% Cr ferritic stainless steel weld. The study demonstrated that as compared with gas tungsten arc welding(GTAW), laser welding brought about significant grain refinement in the FZ and HAZ. However, the impact absorbed energy of GTA weld was superior than that of laser weld because the strengthening effect during welding and cooling stage was higher In laser weld than that in GTA weld. The coarser grains in each weld than base metal resulted in an inferior toughness.

• 한국주조공학회지
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• 제10권2호
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• pp.162-170
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• 1990

The major effects of RSP sre 1) extension of solid solubilities, 2) formation of metastable phaeses, 3) microstructural refinement 4) segregationless. The main trust of this study was to investigate the effects of superimposing RSP on the structure and properties of HSLA steels. Powder was made by NGA (Nitrogen Gas Atomization) process, and consolidated by HIP. The high grain-coarsening resistance of NGA-HIP steels was attributed to a fine dispersion of oxide precipitates. The average grain size for the NGA-HIP steels was somewhat finer than that for the conventional HSLA steels, The impact properteis of NGA-HIP steels were improved over those of the conventional HSLA steels.

• 한국공작기계학회:학술대회논문집
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• 한국공작기계학회 2000년도 추계학술대회논문집 - 한국공작기계학회
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• pp.369-374
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• 2000

This study has been achieved on the characteristics of ultrasonic wave in 2.25Cr-1Mo steel to evaluate the feasibility of ultrasonic nondestructive technique on the assessment of aging degradation. The measured values were used find a relationship between the ultrasonic propagation properties and degradation such as coarsening of carbides and precipitates. The ultrasonic attenuation coefficient was mainly affected by the grain size of prior austenitic phase as well as degradation. In this results, degradation and grain size in 2.25Cr-1Mo steel was able to cope with the changes in ultrasonic wave properties by applying the nondestructive evaluation method

• 한국분말재료학회지
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• 제1권2호
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• pp.208-216
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• 1994

A radically new approach to the in situ synthesis of the consituent phases of a composite structure has enabled the production of a new WC/Co materials with an ultrafine microstructure. The process for synthesizing nanophase WC/Co powders consists of spray drying from solution to form a homogeneous precursor powder, and thermochemical conversion of the precursor powder to the nanophase WC/Co powder. Near theoretical density of pure nanophase WC-10 wt%Co has been obtained in only 30 sec at 140$0^{\circ}C$. But WC particles were grown up very rapidly with longer sintering time to get full density. To overcome coarsening of WC particle during sintering, VC, TaC and VC/TaC were used as the grain growth inhibitor with different amount respectively. VC/TaC doped WC-10 wt%Co was shown superior hardness and TRS and microstructure was maintained ultrafine scale (average WC size is less than 0.1 ${\mu}{\textrm}{m}$).

• 한국산학기술학회논문지
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• 제18권11호
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• pp.124-129
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• 2017

본 연구에서는 철도차량의 경량 차체 소재로 주로 사용되는 알루미늄 합금 (Al-6005-T6) 압출재에 대한 마찰교반접합 적용 연구를 수행하였다. 용접속도를 300 mm/min으로 고정시킨 채 회전 공구의 회전속도를 600, 900, 1200, 1600 rpm으로 변화시킬 때 미세구조 및 기계적 특성의 변화에 대해 평가하였다. 특히, 동일 소재에 대해 전통적인 용접방법인 MIG 용접된 시편과의 비교를 통해 마찰교반접합법의 철도차량 적용성에 대해 논하였다. MIG 용접방법과는 달리, 마찰교반접합부에는 미세기공이 발견되지 않았으며, 경도 측정 결과 공구의 회전속도가 빨라질수록 높아진 입열량에 따라 heat affected zone (HAZ)의 범위가 넓어지고 결정립 조대화에 따라 HAZ의 경도 또한 낮아지는 것을 확인하였다. 인장시험 결과 HAZ지역에서 파단이 발생하였으며, 본 연구에서 설정한 공구의 회전속도 범위에서는 nugget 부의 경도 변화는 발견되지 않았으나 rpm이 올라갈수록 인장강도와 항복강도가 떨어지는 경향을 보였으며 이는 경도 시험에서와 같이 HAZ지역의 결정립 크기의 증가로 인한 현상으로 판단된다.

• 한국환경과학회지
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• 제28권12호
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• pp.1085-1099
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• 2019

We investigated the spatial and temporal variation in characteristics and pollution assessment of sediments in the watersheds of Andong-Dam and Imha-Dam, in Korea. Surface sediments were collected from six sites once a year for three years (2015-2017), and analyzed for organic matter (water content, IL, COD, TOC, TN, and TP), grain size, and concentration of trace metals (Al, Li, Zn, Cr, Pb, Cu, Ni, and As). Organic matter generally tended to increase, and was higher in the Andong watershed compare to Imha watershed. Surface sediments were mainly composed of silt. Coarse sediments were mainly distributed at the site adjacent to Andong-Dam, and showed fining after coarsening. Fine sediment were mainly distributed at the site adjacent to Imha-Dam, and were gradually coarsening. Concentration of trace metals generally tended to increase, and was higher for sites in watershed of Andong watershed (PLI > 1) than for sites in Imha watershed (PLI < 1). Trace metals in the study area were considered to be affected by fine sediment (silt), and contamination of trace metals was somewhat affected by Pb, and greatly affected by Zn and As.

• Journal of Welding and Joining
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• 제33권6호
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• pp.6-12
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• 2015

Thermal fatigue life of the automobile exhaust manifold is directly affected by the restraint force according to the structure of exhaust system and bead shape of the welded joints. In the present study, the microstructural changes and precipitation behavior during thermal fatigue cycle of the 18wt% Cr ferritic stainless steel weld heat affected zone (HAZ) considering restraint stress were investigated. The simulation of weld HAZ and thermal fatigue test were carried out using a metal thermal cycle simulator under complete constraint force in the static jig. The change of the restraint stress on the weld HAZ was simulated by changing the shape of notch in the specimen considering the stress concentration factor. Thermal fatigue properties of the weld HAZ were deteriorated during cyclic heating and cooling in the temperature range of $200^{\circ}C$ to $900^{\circ}C$ due to the decrease of Nb content in solid solution and coarsening of MX type precipitates, laves phase, $M_6C$ with coarsening of grain and softening of the matrix. As the restraint stress on the specimen increased, the thermal fatigue life was decreased by dynamic precipitation and rapid coarsening of the precipitates.

• Applied Microscopy
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• 제43권4호
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• pp.164-172
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• 2013

In this work, microstructural and hardness evolution of the X20 steel upon short-term creep test ($550^{\circ}C$ to $650^{\circ}C$, $180^{\circ}C$ to 60 MPa) was studied by using scanning electron microscope, electron backscattered diffraction, and transmission electron microscope, microhardness tester. After creep rupture, gauge and grip part of the specimens were microstructurally analyzed. Creep at the $650^{\circ}C$/60 MPa resulted in a rupture at 1,460 hours with growth of lath width from 1.31 to $2.87{\mu}m$ and a grain growth with a more equiaxed feature. There is a close relationship between Microhardness and lath width. The formation and coarsening of Laves phase, which was observed up to $600^{\circ}C$ of creep temperature, was accelerated by the applied stress. Slight coarsening of the $M_{23}C_6$ was observed in the $550^{\circ}C$ and $600^{\circ}C$ crept or aged specimens. The coarsening of $M_{23}C_6$ depended on the temperature, where specimens crept at $650^{\circ}C$ showed higher growth rate. The microstructural evolution of X20 after short-term creep test was extensively discussed in relation to the long-term creep/aging test reported in literatures.

• 열처리공학회지
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• 제21권2호
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• pp.87-93
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• 2008

A variety of minor alloying elements such as Zr, Sr, Y, and Gd were added to Mg-3%Zn-0.5%Sn base alloy to form various fine precipitates and their effects on the microstructure, tensile properties, and sheet metal formability were investigated. Various very fine precipitates along with fine second phases were observed by the additions. It was found that Zr or Gd additive has a role to suppress the grain coarsening of alloy sheets during the hot working process. The Zr-added alloy showed the highest tensile elongation at $250^{\circ}C$ whereas the Gd-added alloy exhibited the best sheet metal forming characteristics in terms of CCV (conical cup value) and spring-back tendency.

• Journal of Welding and Joining
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• 제20권4호
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• pp.517-524
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• 2002

An overlaying of the seating surfaces of engine valves by OAW, GTAW or PTA weldings are common practice. The OAW method of a lower torch energy density compared to GTAW and PTA methods produces smoother deposits but the pain size at the vicinity of the interface is increased remarkably up to $30~50{\mu\textrm{m}}$ (that of base metal is about $10\mu\textrm{m}$). It's grain coarsening and the solute dilution are related to the decarburizing during OAW could be minimized by reducing the preheating temperature and by maintaining the carbide precipitates in base metal prior to welding. The formation of columnar structures and carbide precipitation zone in the vicinity of the GTAW welded interface, because of the high heat concentration, causes weakened zone on the valve seat face. The width of the reaction boundary zone is about $50\mu\textrm{m}$ for PTA and GTAW overlaying, and about $150\mu\textrm{m}$ for OAW welding. The smaller width of the reaction boundary zone is the less the solute-dilution rate. Thereby PTA welding may be recommended for overlaying of the seating surfaces.