• Title/Summary/Keyword: Glass-Ceramics

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In-process Truing of Metal-bonded Diamond Wheels for Electrolytic In-process Dressing (ELID) Grinding

  • Saleh, Tanveer;Biswas, Indraneel;Lim, Han-Seok;Rahman, Mustafizur
    • International Journal of Precision Engineering and Manufacturing
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    • v.9 no.3
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    • pp.3-6
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    • 2008
  • Electrolytic in-process dressing (ELID) grinding is a new technique for achieving a nanoscale surface finish on hard and brittle materials such as optical glass and ceramics. This process applies an electrochemical dressing on the metal-bonded diamond wheels to ensure constant protrusion of sharp cutting grits throughout the grinding cycle. In conventional ELID grinding, a constant source of pulsed DC power is supplied to the ELID cell, but a feedback mechanism is necessary to control the dressing power and obtain better performance. In this study, we propose a new closed-loop wheel dressing technique for grinding wheel truing that addresses the efficient correction of eccentric wheel rotation and the nonuniformity in the grinding wheel profile. The technique relies on an iterative control algorithm for the ELID power supply. An inductive sensor is used to measure the wheel profile based on the gap between the sensor head and wheel edge, and this is used as the feedback signal to control the pulse width of the power supply. We discuss the detailed mathematical design of the control algorithm and provide simulation results that were confirmed experimentally.

Effects of Mixing Chamber Shape on Cutting Performance in AWJ (AWJ에서 혼합챔버 형상이 절단성능에 미치는 영향)

  • Lee, Hyo-Ryeol;Kwak, Yong-Kil;Kim, Hwa-Young;Ahn, Jung-Hwan;Yeo, Myeong-Heon
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.20 no.5
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    • pp.535-540
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    • 2011
  • It is well known that abrasive waterjet (AWJ) was developed as a kind of high-density energy processing technologies. AWJ is used to obtain cutting quality of various materials such as metal, ceramics, glass and composite materials within a short manufacturing time because of the characteristics of heatless and noncontact processing. However, surface roughness and dimension error like round, burr, taper vary severely according to the processing conditions such as pressure, cutting speed, orifice diameter, stand off distance and abrasive flow rate. In this paper, the effect of the shape of mixing chamber on surface quality is studied. Three types of mixing chamber - round, parabolic, elliptical - are suggested and each performance is compared to that of cylindrical mixing chamber experimentally. From the result, is proved to be the optimal mixing chamber in the aspect of surface quality the parabolic one.

Present State and Prospect on Reutilization of Metal - Bearing Solid Wastes in China

  • Chai, Liyuan;Chen, Weiliang;Min, Xiaobo;He, Dewen;Zhang, Chuanfu
    • Proceedings of the IEEK Conference
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    • 2001.10a
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    • pp.183-187
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    • 2001
  • Present states on reutilization of metal-bearing solid wastes in China including metal-containing gangue, red mud, nonferrous metallurgical slag or residue, arsenical slag, steel - iron slag, waste batteries, were described in detail. The wastes pile up at a large quantity, resulting in seriously potential harm to environment. Most of these wastes, however, contain valuable metals, which are regarded as important secondary resources for extracting metals. Waste slag and batteries with a high grade of metals are treated by a hydro-based and / or pyre-based method for extracting valuable metals. While gangue and waste slag with a low grade are as a raw material in architecture field. In the future, a novel technology, such as high-grads magnetization separation technique and biological technique, will be designed to treat these wastes for protecting environment and recycling valuable components. These wastes, furthermore, are synthetically reutilized to produce various architectural materials, including glass and ceramics.

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Effect of $M_2O_3$ on the Sinterbility and Electrical Conductivity of $ZrO_2(Y_2O_3)$ System (I): Ceramics of the:$ZrO_2-Y_2O_3-Bi_2O_3$ System ($ZrO_2(Y_2O_3)$ 계 세라믹스의 소결성과 전기전도도에 대한 $M_2O_3$의 영향 (I):$ZrO_2-Y_2O_3-Bi_2O_3$계 세라믹스)

  • 오영제;정형진;이희수
    • Journal of the Korean Ceramic Society
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    • v.23 no.3
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    • pp.87-93
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    • 1986
  • Yttria-bismuth-stabilized zirconia was investigated with respect to the amount of $Bi_2O_3$ addition in the ran-ge of 0.5~5mol% to the base composition of $(ZrO_2)_{0.92}(Y_2O_3)_{0.08}.Bismuth was introduced into the ma-terial with $Bi_2O_3-SiO_2$ glasses in order to reduce the evaporation of components. The sinterbility evaporation of components phase formation and microstructure were evaluated depending on the amount of $Bi_2O_3-SiO_2$ glass addition. Two probe A. C conductivity measurement was subjected to all the specimens and the result was discussed on the possible substitution of $Bi^{3+}$ for $Zr^{4+}$ and interistial $Si^{4+}$ in the fluorite structure of zirconia crystal there-upon the possible change in the capability of oxygen transference within the material. It was found that the addition of $Bi_2O_3$ could improve the sinterbility of material very much while not so much.oxygen sensing material suitable for relative low temperature firing.

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Evaluation of Ultrasonic Vibration Cutting while Machining Inconel 718

  • Nath, Chandra;Rahman, Mustafizur
    • International Journal of Precision Engineering and Manufacturing
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    • v.9 no.2
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    • pp.63-68
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    • 2008
  • Hard and brittle materials, such as Ni- and Ti-based alloys, glass, and ceramics, are very useful in aerospace, marine, electronics, and high-temperature applications because of their extremely versatile mechanical and chemical properties. One Ni-based alloy, Inconel 718, is a precipitation-hardenable material designed with exceptionally high yield strength, ultimate tensile strength, elastic modulus, and corrosion resistance with outstanding weldability and excellent creep-rupture properties at moderately high temperatures. However, conventional machining of this alloy presents a challenge to industry. Ultrasonic vibration cutting (UVC) has recently been used to cut this difficult-to-machine material and obtain a high quality surface finish. This paper describes an experimental study of the UVC parameters for Inconel 718, including the cutting force components, tool wear, chip formation, and surface roughness over a range of cutting conditions. A comparison was also made between conventional turning (CT) and UVC using scanning electron microscopy observations of tool wear. The tool wear measured during UVC at low cutting speeds was lower than CT. UVC resulted in better surface finishes compared to CT under the same cutting conditions. Therefore, UVC performed better than CT at low cutting speeds for all measures compared.

Effects of Drying Temperature on the Optical Properties of Solution Derived (Pb, La)$TiO_3$ Thin Films

  • Yoon, Dae-Sung;Kim, Sung-Wuk;Koo, Jun-Mo;Jiang, Zhong-Tao
    • The Korean Journal of Ceramics
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    • v.1 no.4
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    • pp.191-196
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    • 1995
  • Using sol-gel processing method, thin films of lathanum modified lead titanate(PLT) on Corning 7059 glass were prepared. A differential thermal analysis (DTA/TG) curve of gel powder and infrared spectra (FT-IR) of the films were measured to estimate residual organices in them. The heat-treated films were characterized by X-ray diffraction(XRD). Microstructures of the films were observed by a scanning electron microscope (SEM). Optical properties of the films were determined by a UV-VIS spectrophotometer. The waveguiding properties and optical attenuation were measured with the end coupling method and the cut back method. Effects of the drying conditions on the transmittance and the propagation loss of the films were investigated. Experimemtal results showed that the content of residual organics in the film decreased as the drying temperature of the film increased. As the La content of the film increased, the grain size decreased and the transmittance increased. The transmittances of the films increased with the increasing of the drying temperature. The propagation losses in the film decreased as the drying temperature increased.

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Analysis of the Coloration Characteristics of Copper Red Glaze Using Raman Microscope (Raman Microscope를 이용한 진사 유약 발색 특성 분석)

  • Eo, Hye-Jin;Lee, Byung-Ha
    • Journal of the Korean Ceramic Society
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    • v.50 no.6
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    • pp.518-522
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    • 2013
  • This study investigatesthe coloration mechanism by identifying the factor that affects thered coloration of copper red glazesin traditional Korean ceramics. The characteristics of the reduction-fired copper red glaze's sections are analyzed using an optical microscope, Raman spectroscopy, scanning electron microscopy (SEM) and energy dispersive x-ray spectroscopy (EDX). The sections observed using an optical microscope are divided into domains of surface, red-bubble, and red band. According to the Raman micro spectroscopy analysis results, the major characteristic peak is identified as silicate in all three domains, and the intensity of $Cu_2O$ increases toward the red band. In addition, it is confirmed that the most abundant CuO exists in the glaze bubbles. Moreover, CuO and $Cu_2O$ exist as fine particles in a dispersed state in the surface domain. Thus, Cu combined with oxygen is distributed evenly throughout the copper red glaze, and $Cu_2O$ is more concentrated toward the interface between body and glaze. It is also confirmed that CuO is concentrated around the bubbles. Therefore, it is concluded that the red coloration of the copper red glaze is revealed not only through metallic Cu but also through $Cu_2O$ and CuO.

Structural and Optical Properties of SiO2 Thick Films by Aerosol Deposition Process (에어로졸 데포지션 법을 이용하여 제조한 SiO2 후막의 구조 및 광학 특성)

  • Jang, Chan-Ik;Koh, Jung-Hyuk
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.26 no.1
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    • pp.6-12
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    • 2013
  • Aerosol deposition(AD) coating that enable fabricate films at low temperature have begun to be widely researched for the integration of ceramics as well to realize high-speed deposition rates. For application of ceramic thick film by AD to display and electronic ceramic industry, fabrication of dense structure with a no cracking is required. In this study, to fabricate dense ceramic thick film, the effect of crystal phase of starting powder was investigated. For this study, amorphous and crystalline $SiO_2$ powders were used as starting powders. Two types of $SiO_2$ powders were deposited on glass substrate by AD. In the case of amorphous $SiO_2$ powder, the deposited films had extremely incompact and opaque layer, irrespective of particle size. In contrast to amorphous powder, in the case of crystalline powder, porous structure layer and dense microstructure with no cracking layer were fabricated depending on the particle size. The optimized starting powder size for dense coating layer was $1{\sim}2{\mu}m$. The transmittance of film reached a maximum of 76% at 800 nm.

Design of piezoelectric transducer arrays for passive and active modal control of thin plates

  • Zenz, Georg;Berger, Wolfgang;Gerstmayr, Johannes;Nader, Manfred;Krommer, Michael
    • Smart Structures and Systems
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    • v.12 no.5
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    • pp.547-577
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    • 2013
  • To suppress vibration and noise of mechanical structures piezoelectric ceramics play an increasing role as effective, simple and light-weighted damping devices as they are suitable for sensing and actuating. Out of the various piezoelectric damping methods this paper compares mode based active control strategies to passive shunt damping for thin plates. Therefore, a new approach for the optimal placement of the piezoelectric sensors/actuators, or more general transducers, is proposed after intense theoretical investigations based on the Kirchhoff kinematical hypotheses of plates; in particular, modal and nilpotent transducers are discussed in detail. Based on the proposed distribution a discrete design for modal transducers is implemented, tested and verified on an experimental setup. For active control the modal sensors clearly identify the eigenmodes, whereas the modal actuators impose distributed eigenstrains in order to reduce the transverse plate vibrations. In contrast to the modal control, passive shunt damping works without requiring additional actuators or auxiliary power and can therefore act as an autonomous system, but it is less effective compensating the flexible vibrations. Exemplarily, an acryl glass plate disturbed by an arbitrary force initialized by a loudspeaker is investigated. Comparing the different methods their specific advantages are highlighted and a significant broadband reduction of the vibrations of up to -20dB is obtained.

Application of Inverse Pole Figure to Rietveld Refinement: III. Rietveld Refinement of $SnO_2$ Thin Film using X-ray Diffraction Data

  • Kim, Yong-Il;Jung, Maeng-Joon;Kim, Kwang-Ho
    • The Korean Journal of Ceramics
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    • v.6 no.4
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    • pp.354-358
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    • 2000
  • The SnO$_2$film was deposited on a corning glass 1737 substrate by plasma enhanced chemical vapor deposition using a gas mixture of SnCl$_4$, $O_2$, and Ar. The film thickness was measured using $\alpha$-step and was about 9400$\AA$. The conventional X-ray diffractometry and pole figure attachment were used to refine the crystal structure of SnO$_2$ thin film. Six pole figures, (200), (211), (310), (301), (321), and (411), were measured with CoK$_\alpha$ radiation in reflection geometry. The X-ray diffraction data were measured at room temperature using CuK$_\alpha$ radiation with graphite monochromator. The agreement between calculated and observed patterns for the normal direction of SnO$_2$ thin film was not satisfactory due to the severely preferred orientation effect. The Rietveld refinement of heavily textured SnO$_2$ thin film was successfully achieved by adopting the pole density distribution of each reflection obtained from the inverse pole figure as a correction factor for the preferred orientation effect. The R-weighted pattern, R$_wp$, was 15.30%.

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