• 대한기계학회논문집A
• /
• 제33권11호
• /
• pp.1274-1278
• /
• 2009

Fracture characteristics for plate and dome shapes of glass filled ceramics using shock tube were carried out. Glass filled ceramics have been considered as a promising candidate material for the dome port cover of air breathing engine. This part of the air breathing engine has an important role as separated membrane between combustion and external air, and needs the frangible characteristics that the particles of fractured glass filled ceramics should not affect the internal components of combustion. The objectives of this study are to evaluate the fracture pressures for various thicknesses and diameters of shock impact area. Also fracture phenomena of separated membrane using a shock tube compare with analytical method. The experimental apparatus consists of a driver, a driven section and a dump tank. The used material is glass filled ceramic made from Corning company. Specimens have the thickness of 3, 4.5 and 6mm. It is expected that the results obtained from this study can be used in the basic data for the dome port cover design of an air breathing engine.

• 한국세라믹학회지
• /
• 제29권12호
• /
• pp.956-962
• /
• 1992

The predominant sintering mechanisms of low firing temperature ceramic substrate which consists of borosilicate glass containing alumina as a filler are the rearrangement of alumina particles and the viscous flow of glass powders. In this system, sintering condition depends on the volume ratio of alumina to glass and on the particle size. When the substrate contains about 35 vol% alumina filler and the average alumina particle size is 4 $\mu\textrm{m}$, the best firing condition is obtained at the temperature range of 900∼1000$^{\circ}C$. The extensive rearrangement behavior occurs at these conditions, and the optimum sintering condition is attained by smaller size of glass particles, too. The formation of cristobalite during sintering causes the difference of thermal expansion coefficient between the substrate and Si chip. This phenomenon degradates the capacity of Si chip. Therefore, the crystallization should be prevented. In the alumina filled borosilicate glass system, the crystallization does not occur. This effect may have some relation with aluminum ions in alumina. For aluminum ions diffuse into glass matrix during sintering, functiong as network former.

• 마이크로전자및패키징학회지
• /
• 제6권1호
• /
• pp.11-21
• /
• 1999

For microelectronic packaging application, the crystallizable glass powder in CaO-$A1_2O_3-SiO_2-B_2O_3$system was mixed with various amounts of alumina inclusions (\approx 4 $\mu \textrm{m}$), and its sintering behavior, crystallization behavior, and dielectric constant were examined in terms of vol% of alumina and the reaction between the alumina and the glass. Sintering of the CASB glass powder alone at $900^{\circ}C$ resulted in full densification (99.5%). Sintering of alumina-filled composite at $900^{\circ}C$ also resulted in a substantial denslfication higher than 97% of theoretical density, In this case, the maximum volume percent of alumina should be less than 40%. XRD analysis revealed that there was a partial dissolution of alumina into the glass. This alumina dissolution, however, did not show the particle growth and shape accommodation. Therefore, the sintering of both the pure glans and the alumina-filled composite was mainly achieved by the viscous flow and the redistribution of the glass. Alumina dissolution accelerated the crystallization initiation time at $1000^{\circ}C$ and hindered the densification of the glass. Dielectric constants of both the alumina-filled glass and the glass-ceramic composites were increased with increasing alumina content and followed rule of mixture. In case of the glass-ceramic matrix composites showed relatively lower dielectric constant than the glass matrix composite. Furthermore, as alumina content increased, crystallization behavior of the glass was changed due to the reaction between the glass and the alumina. As alumina reacted with the glass matrix, the major crystallized phase was shifted from wollastonite to gehlenite. In this system, alumina dissolution strongly depended on the particle size: When the particle size of alumina was increased to 15 $\mu\textrm{m}$, no sign of dissolution was observed and the major crystallized phase was wollastonite.

• 한국추진공학회:학술대회논문집
• /
• 한국추진공학회 2009년도 춘계학술대회 논문집
• /
• pp.103-106
• /
• 2009

Fracture characteristics of plate shape using shock tube for glass filled ceramics was carried out. Glass filled ceramics have been considered as a promising candidate material for the dome port cover of air breathing engine. This part of the air breathing engine has an important role separating solid and liquid fuel, and needs the frangible characteristics that the fracture of a part should not affect the internal components of combustion. The objectives of this study are to evaluate the fracture pressures for various thicknesses and diameters of shock impact area. Also fracture phenomena of separated membrane using a shock tube are observed. The experimental apparatus of shock tube consists of a driver, a driven section and a dump tank. The used material is glass filled ceramic made from Corning company. Specimens are used 3, 4.5 and 6mm thickness. Also diameters of shock wave area are chosen 70, 60 and 50 mm. It is expected that the results obtained from this study can be used in the basic data for the dome port cover design of an air breathing engine.

• 한국추진공학회:학술대회논문집
• /
• 한국추진공학회 2004년도 제23회 추계학술대회 논문집
• /
• pp.223-226
• /
• 2004

본 연구는 램제트 돔 포트 커버용 글라스 세라믹의 기계적 특성, 정적 및 동적 파괴인성을 평가하기 위해 수행하였다. 램제트 추진기관의 돔 포트 커버의 재료로 MACOR 글라스 세라믹 9658을 선정하였으며, 취성재료인 글라스 세라믹의 파괴인성을 측정하기 위해 노치시편에 대한 정적 및 동적 파괴인성시험을 수행하였다.

• 한국세라믹학회지
• /
• 제40권8호
• /
• pp.735-738
• /
• 2003

고주파용 회로기판으로 사용하는 PTFE 복합체를 woven glass fiber를 사용하여 제조하였다. 유전상수는 PTFE 분산액에 woven glass fiber를 함침하는 횟수 증가에 따라 감소하는 특성을 나타내었으며, 3회 함침 횟수부터는 변화율이 감소하였는데, 이것은 PTFE 미세분말이 woven glass fiber의 기공과 굴곡 사이를 충분히 채우기 때문이다. 또한 함침 횟수 증가에 따라 PTFE의 비율이 증가하면서 유전 상수가 감소하여 회로 기판의 전파 전송속도는 증가하였다.

• 한국추진공학회:학술대회논문집
• /
• 한국추진공학회 2005년도 제24회 춘계학술대회논문집
• /
• pp.112-115
• /
• 2005

본 연구는 램제트 엔진의 돔포트 커버의 소재로 사용 될 첨단 그라스 세라믹(MACOR) 소재에 대한 동적 파괴인성 시험을 목적으로 한다. 다양한 노치반경의 시험편에 대하여 스트레인게이지법을 사용한 정적과 동적 파괴인성 시험을 수행하였다.

• 한국전기전자재료학회:학술대회논문집
• /
• 한국전기전자재료학회 2003년도 하계학술대회 논문집 Vol.4 No.2
• /
• pp.611-615
• /
• 2003

The crystalline and dielectric properties on $Al_2O_3$ filled glass frit ($CaO-Al_2O_3-SiO_2-MgO-B_2O_3$) with admixtures of $TiO_2$ have been investigated. The dielectric constant value of $7.5{\sim}7.8$, quality factor value of 700 were obtained for glass frit : $Al_2O_3$ (50 : 50 wt%) ceramics. As the amount of $TiO_2$ increased, temperature coefficient of dielectric constant were decreased.

• 한국세라믹학회지
• /
• 제35권9호
• /
• pp.939-944
• /
• 1998

실리콘함유 고분자(Polysiloxane)의 세라믹변환과정에서의 부피수축효과를 조절하기 위하여 활성화금속으로 중석을 첨가하여 열분해 및 합성반응을 통해 신 세라믹 복합체를 개발하고 이의 세라믹화 과정이나 물성을 조사하였다. 제조된 시편의 미세조직은 고분자로부터 야기된 $S_{1}$-O-C게열의 Glass기지상과, 분해잔여물(고상,기상)등과 활성화금속과의 반응르로 생성된 고경도의 탄호물로 이루어져 있어 향후 내마모재료로서의 응용을 기대할 수 있을 것이다. 제조된 복합체의 물성은 반응조건에 많이 의존함을 알 수 있었다. 1400~$1500^{\circ}C$에서 열분해 시켜 제조한 복합체의 밀도는 95% 이상의 상대밀도와, 경도 값은 7~8GPa 정도이고 탄성률은 220~230 GPa, 파괴인성응ㄴ 6~6.8$MPam^{1/2}$, 파괴강도는 380~470 MPs정도의 값을 나타내었다.

• 한국세라믹학회지
• /
• 제35권7호
• /
• pp.706-714
• /
• 1998

The MgO-{{{{ { {Al }_{2 }O }_{3 } }}-{{{{ { {SiO }_{2 } }_{ } }}system containing alumina powder was fabricated sintered at various temperature and analyzed in order to study the sintering mechanism and crystallization characteristics. The specimen composed of glass powder with average particle size of 8.27 $\mu\textrm{m}$ and 0-40 vol% alumina powder were sint-ered for 3 hrs at the temperature between 850$^{\circ}C$ and 1350$^{\circ}C$ The sintering mechanism consists of the redis-tribution of particles occuring at 750$^{\circ}C$ and the viscous flow at 850∼950$^{\circ}C$. The degree of crystallization and sintering temperatue were dependent upon the ratio of glass/alumina. The second phase from the reaction between glass and alumina was not observed which was confirmed by XRD and properties analysis. The density dielectric constant and specific resistivity of specimen were 2.30∼3.26g/cm2 5.8∼7.38 at 1 GHz density dielectric constant and specific resistivity of specimen were 2.30∼3.26g/cm3 5.8∼7.38 at 1GHz and 1.23∼4.70${\times}$107 $\Omega$$.$m respectively.